The characterization of microstructure evolution in friction stir welded aluminum alloy was carried out by optical microscopy (OM) and transmission electron microscopy (TEM) and electron backscatter diffraction (...The characterization of microstructure evolution in friction stir welded aluminum alloy was carried out by optical microscopy (OM) and transmission electron microscopy (TEM) and electron backscatter diffraction (EBSD). The weld nugget consisted of very fine equiaxed grains and experienced dissolution of nearly half of metastable precipitates into the matrix during welding. Thermomechanically affected zone (TMAZ) also experienced dissolution of precipitates but to a lesser extent whereas coarsening of precipitates was observed in heat affected zone (HAZ). Grain boundary misorientation measurements using EBSD indicated continuous dynamic recrystallization as the underlying mechanism for the fine equiaxed nugget grains. The yield and tensile strength of the weld decreased with comparison to base material. But due to the decrease of grain size and the dissolution of second phase precipitates, an increased Charpy energy value was observed in the weld n u gget.展开更多
针对牙科钴铬合金(remanium star CL)进行选择性激光熔融(SLM)成形实验,测试分析钴铬合金成形件微观组织及表面质量,研究激光功率、扫描速度、扫描间距及其综合作用下的激光能量密度对钴铬合金件表面粗糙度、相对密度及维氏硬度的...针对牙科钴铬合金(remanium star CL)进行选择性激光熔融(SLM)成形实验,测试分析钴铬合金成形件微观组织及表面质量,研究激光功率、扫描速度、扫描间距及其综合作用下的激光能量密度对钴铬合金件表面粗糙度、相对密度及维氏硬度的影响。研究结果表明,相同激光能量密度下,不同的激光功率、扫描速度、扫描间距也会导致不同的表面粗糙度。SLM成形钴铬合金件相对密度随激光功率的增加而增大且变化速率逐渐缓慢;扫描速度在80~100 mm/s时,钴铬合金SLM成形相对密度最大值达94.95%。随着激光扫描间距的增大,钴铬合金件的相对密度下降。试件维氏硬度随激光功率和扫描速度的增大均呈现先增大后减小的变化规律。此外,激光功率从50 W变为100 W时,网状晶粒平均尺寸由0.8μm增大到2μm左右,然而过大的激光功率将导致晶粒尺寸过大使硬度降低。SLM成形钴铬合金件维氏硬度平均硬度为392 HV,在合理范围内略高于标准值。展开更多
文摘The characterization of microstructure evolution in friction stir welded aluminum alloy was carried out by optical microscopy (OM) and transmission electron microscopy (TEM) and electron backscatter diffraction (EBSD). The weld nugget consisted of very fine equiaxed grains and experienced dissolution of nearly half of metastable precipitates into the matrix during welding. Thermomechanically affected zone (TMAZ) also experienced dissolution of precipitates but to a lesser extent whereas coarsening of precipitates was observed in heat affected zone (HAZ). Grain boundary misorientation measurements using EBSD indicated continuous dynamic recrystallization as the underlying mechanism for the fine equiaxed nugget grains. The yield and tensile strength of the weld decreased with comparison to base material. But due to the decrease of grain size and the dissolution of second phase precipitates, an increased Charpy energy value was observed in the weld n u gget.