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大塑性变形制备超细晶复合材料的研究进展 被引量:17
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作者 郭炜 王渠东 《锻压技术》 CAS CSCD 北大核心 2010年第1期4-9,共6页
介绍了等径角挤压(ECAP)、往复挤压(CEC)、高压扭转(HPT)和累积叠轧(ARB)4种技术的加工原理,系统阐述了大塑性变形(SPD)制备铝基、镁基、铜基超细晶(UFG)复合材料的研究进展,指出SPD技术是细化复合材料基体、均匀弥散增强相从而提高强... 介绍了等径角挤压(ECAP)、往复挤压(CEC)、高压扭转(HPT)和累积叠轧(ARB)4种技术的加工原理,系统阐述了大塑性变形(SPD)制备铝基、镁基、铜基超细晶(UFG)复合材料的研究进展,指出SPD技术是细化复合材料基体、均匀弥散增强相从而提高强度、硬度和塑性的有效手段,并展望了其研究范围将由有色金属基复合材料拓宽到铁基、陶瓷基、聚合物基等复合材料。 展开更多
关键词 大塑性变形 超细晶 复合材料 力学性能
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Bimodal microstructure – A feasible strategy for high-strength and ductile metallic materials 被引量:10
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作者 Min Zha Hong-Min Zhang +4 位作者 Zhi-Yuan Yu Xuan-He Zhang Xiang-Tao Meng Hui-Yuan Wang Qi-Chuan Jiang 《Journal of Materials Science & Technology》 SCIE EI CAS CSCD 2018年第2期257-264,共8页
Introducing a bimodal grain-size distribution has been demonstrated an efficient strategy for fabricating high-strength and ductile metallic materials, where fine grains provide strength, while coarse grains enable st... Introducing a bimodal grain-size distribution has been demonstrated an efficient strategy for fabricating high-strength and ductile metallic materials, where fine grains provide strength, while coarse grains enable strain hardening and hence decent ductility. Over the last decades, research activities in this area have grown enormously, including interesting results onfcc Cu, Ni and Al-Mg alloys as well as steel and Fe alloys via various thermo-mechanical processing approaches. However, investigations on bimodal Mg and other hcp metals are relatively few. A brief overview of the available approaches based on thermo- mechanical processing technology in producing bimodal microstructure for various metallic materials is given, along with a summary of unusual mechanical properties achievable by bimodality, where focus is placed on the microstructure-mechanical properties and relevant mechanisms. In addition, key factors that influencing bimodal strategies, such as compositions of starting materials and processing parameters, together with the challenges this research area facing, are identified and discussed briefly. 展开更多
关键词 Nanocrystalline and ultrafine-grained metals Mechanical milling Severe plastic deformation Bimodal microstructure Strength and ductility
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等通道转角挤压——提高材料性能的有效方法 被引量:6
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作者 孙爱民 《上海钢研》 2004年第1期19-25,共7页
等通道转角挤压法是能使块体材料得到超细晶粒的一种新的材料加工方法,目前受到材料研究者的广泛关注。简要介绍等通道转角挤压法(ECAE)的基本原理及通过该方法得到的有效应变量的主要影响因素。综述等通道转角挤压法研究和应用现状,同... 等通道转角挤压法是能使块体材料得到超细晶粒的一种新的材料加工方法,目前受到材料研究者的广泛关注。简要介绍等通道转角挤压法(ECAE)的基本原理及通过该方法得到的有效应变量的主要影响因素。综述等通道转角挤压法研究和应用现状,同时展望该方法的应用前景。 展开更多
关键词 等通道转角挤压 超细晶粒 有效应变量 ECAE 晶粒细化 金属材料
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Al-Zn-Mg合金超低温高速大变形中超细晶组织演化行为的研究 被引量:7
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作者 卢剑 殷京瓯 +1 位作者 何瑜 丁宝峰 《稀有金属材料与工程》 SCIE EI CAS CSCD 北大核心 2005年第5期742-745,共4页
利用透射电子显微镜研究了Al-Zn-Mg铝合金在低温(液氮)高速多向大变形条件下的显微组织演化,分析了合金在不同变形条件下的变形及组织形貌特征,讨论了低温及几何动态再结晶对显微组织演化过程的影响。结果表明:在超低温、高速、大形变... 利用透射电子显微镜研究了Al-Zn-Mg铝合金在低温(液氮)高速多向大变形条件下的显微组织演化,分析了合金在不同变形条件下的变形及组织形貌特征,讨论了低温及几何动态再结晶对显微组织演化过程的影响。结果表明:在超低温、高速、大形变量、约束变形条件下,7075铝合金能够不经过退火实现连续的大变形而不会失效,并且获得了均匀的超细晶组织,晶粒尺寸小于200nm;超细晶组织随着变形量增加而明显细化,相邻晶粒的取向差增大。 展开更多
关键词 多向锻造:低温 超细晶 几何动态再结晶 渐进转动动态再结晶 7075铝合金
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Fabrication of ultrafine-grained AA1060 sheets via accumulative roll bonding with subsequent cryorolling 被引量:7
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作者 Qing-lin DU Chang LI +2 位作者 Xiao-hui CUI Charlie KONG Hai-liang YU 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2021年第11期3370-3379,共10页
Ultrafine-grained(UFG)AA1060 sheets were fabricated via five-cycle accumulative roll bonding(ARB)and subsequent three-pass cold rolling(298 K),or cryorolling(83 K and 173 K).Microstructures of the aluminum samples wer... Ultrafine-grained(UFG)AA1060 sheets were fabricated via five-cycle accumulative roll bonding(ARB)and subsequent three-pass cold rolling(298 K),or cryorolling(83 K and 173 K).Microstructures of the aluminum samples were examined via transmission electron microscopy,and their mechanical properties were measured via tensile and microhardness testing.Results indicate that ultrafine grains in ARB-processed sheets were further refined by subsequent rolling,and the grain size became finer with reducing rolling temperature.The mean grain size of 666 nm in the sheets subjected to ARB was refined to 346 or 266 nm,respectively,via subsequent cold rolling or cryorolling(83 K).Subsequent cryorolling resulted in ultrafine-grained sheets of higher strength and ductility than those of the sheets subjected to cold rolling. 展开更多
关键词 microstructure AA1060 sheet ultrafine-grained materials CRYOROLLING accumulative roll bonding
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超细晶镁合金的腐蚀与防护进展 被引量:3
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作者 程青鹏 黄秀玲 张凡 《表面技术》 EI CAS CSCD 北大核心 2023年第4期112-123,共12页
总结了近年来经剧烈塑性变形加工后的超细晶镁合金的腐蚀与防护研究。镁合金的初始成分可能对剧烈塑性变形加工后样品耐蚀性的变化起主导性作用。对于纯镁及含有铝或稀土等致钝性元素的合金,如AZ系和WE系镁合金,绝大多数剧烈塑性变形加... 总结了近年来经剧烈塑性变形加工后的超细晶镁合金的腐蚀与防护研究。镁合金的初始成分可能对剧烈塑性变形加工后样品耐蚀性的变化起主导性作用。对于纯镁及含有铝或稀土等致钝性元素的合金,如AZ系和WE系镁合金,绝大多数剧烈塑性变形加工会促进生成更致密的保护膜,因而可以提升镁合金的耐蚀性。对于不含此类元素的镁合金体系,如Mg-Zn系合金,由于生成了更多的腐蚀微电偶,等通道转角挤压或高压扭转加工引起的第二相颗粒的细化和分布会加速镁合金的腐蚀,但多轴等温锻造可以提升此类合金的耐蚀性,该技术值得更多的关注。在成分相似的情况下,组织的均匀性或者第二相变化情况的影响可能较晶粒尺寸和织构演变的影响更大。对加工后的镁合金进行热处理或者表面改性是进一步提升其耐蚀性的有效手段。相对于粗晶基体,超细晶基体表面改性后的涂层的耐蚀性往往更好,值得更多的研究关注。 展开更多
关键词 镁合金 超细晶 剧烈塑性变形 表面改性 耐蚀性 腐蚀与防护
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晶粒长大抑制剂对WC-9%Co超细晶硬质合金组织及性能的影响 被引量:7
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作者 雍薇 彭晖 +1 位作者 刘益兴 王晓灵 《硬质合金》 CAS 2018年第5期338-343,共6页
本文采用常规粉末冶金方法,通过单独或复合添加Cr_3C_2、VC、TiC等晶粒长大抑制剂的方法,制备了WC-9%Co超细晶硬质合金,试验对比了其显微组织和力学性能。结果显示:抑制剂的加入均可显著细化合金组织,提高硬度,但合金的断裂韧性(K_(IC)... 本文采用常规粉末冶金方法,通过单独或复合添加Cr_3C_2、VC、TiC等晶粒长大抑制剂的方法,制备了WC-9%Co超细晶硬质合金,试验对比了其显微组织和力学性能。结果显示:抑制剂的加入均可显著细化合金组织,提高硬度,但合金的断裂韧性(K_(IC))有所降低,抗弯强度(TRS)与所添加的抑制剂种类有关。其中VC抑制晶粒长大的效果最显著,其次是Cr_3C_2,再次是TiC。在本实验条件下,复合添加Cr_3C_2+VC的合金硬度最高,强韧性最差;复合添加Cr_3C_2+TiC的合金具有最好的综合力学性能。 展开更多
关键词 硬质合金 超细晶 晶粒长大抑制剂 显微组织 力学性能
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Martensite decomposition under thermal-mechanical coupling conditions to fabricate an ultrafine-grained Ti6Al4Mo4Zr1W0.2Si alloy
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作者 Taoyu Zhou Jiuxu Yang +4 位作者 Nan Li Hao Sun Bohua Zhang Zibo Zhao Qingjiang Wang 《Journal of Materials Science & Technology》 SCIE EI CAS CSCD 2024年第1期157-168,共12页
The fabrication of ultrafine-grained microstructures(grain size below 1μm)in titanium alloys is beneficial for improving their mechanical properties at room temperature and medium tempera-tures(400-550°C).Howeve... The fabrication of ultrafine-grained microstructures(grain size below 1μm)in titanium alloys is beneficial for improving their mechanical properties at room temperature and medium tempera-tures(400-550°C).However,a long-standing challenge involves the low-cost manufacturing of bulk ultrafine-grained titanium alloys.In this work,we developed a facile strategy through martensite de-composition at thermal-mechanical coupling conditions,to fabricate an equiaxed microstructure in a Ti6Al4Mo4Zr1W0.2Si model alloy with an averageαgrain size of 315±62 nm.The formation of the ultrafine-grained microstructure was because the lattice strain stored in the martensitic initial mi-crostructure enhanced the nucleation rate of dynamic recrystallization,meanwhile,the pinning role of martensite decomposition productsβand(Ti,Zr)_(5)Si_(3)phases suppressed grain coarsening at high tem-peratures.Compared to conventional(α+β)alloys,the tensile strength of this alloy improved by 20%-30%at both room temperature and 550°C,without decreasing its ductility.In situ SEM observations revealed that the ultrafine-grained microstructure would not only suppress dislocation motions but also contribute to the homogenous deformation in the matrix of the material,therefore,it resulted in higher mechanical performance.The research results may be of great significance to the development of next-generation aviation titanium alloys. 展开更多
关键词 ultrafine-grained Titanium alloy In situ observation Deformation mechanism Thermostability
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微合金化对超细晶中厚板显微组织的影响 被引量:6
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作者 王立军 姚连登 +1 位作者 任海鹏 刘春明 《东北大学学报(自然科学版)》 EI CAS CSCD 北大核心 2007年第4期510-513,521,共5页
在Gleeble 1500热模拟机上,通过820-790℃温度范围内的多道次热压缩变形模拟了中厚板的精轧工艺,考察了不同铌、钒(氮)含量的低碳钢的组织演变过程、微合金元素的碳氮化物的析出行为和对形变诱导铁素体相变(DIFT)的影响.结果表明:... 在Gleeble 1500热模拟机上,通过820-790℃温度范围内的多道次热压缩变形模拟了中厚板的精轧工艺,考察了不同铌、钒(氮)含量的低碳钢的组织演变过程、微合金元素的碳氮化物的析出行为和对形变诱导铁素体相变(DIFT)的影响.结果表明:变形过程中有部分奥氏体转变为铁素体,依变形的温度不同在变形间隔时间内有逆相变或亚动态相变发生;变形后快速冷却得到平均晶粒直径低于5μm的超细晶组织.单独添加钒对DIFT具有抑制作用,可以细化显微组织;钒-氮复合添加促进DIFT,但使组织粗化;添加铌基本不会抑制DIFT,能显著细化显微组织.变形后冷速越小,钢种间差距越明显.微合金化元素的作用与其在变形过程中的溶解析出行为有关. 展开更多
关键词 微合金化 中厚板 超细晶粒 形变诱导铁素体相变 碳氮化物
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Effect of magnetic field on dislocation morphology and precipitation behaviour in ultrafine-grained 7075 aluminium alloy 被引量:5
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作者 Jun Luo Hongyun Luo +1 位作者 Tianshu Zhao Runze Wang 《Journal of Materials Science & Technology》 SCIE EI CAS CSCD 2021年第34期128-146,共19页
The influence of magnetic field(1 T)on dislocation morphology and precipitation behaviour of ultrafinegrained(UFG)Al 7075 alloy was investigated after ageing from 90 to 200℃ via wide angle X-ray scattering(WAXS),smal... The influence of magnetic field(1 T)on dislocation morphology and precipitation behaviour of ultrafinegrained(UFG)Al 7075 alloy was investigated after ageing from 90 to 200℃ via wide angle X-ray scattering(WAXS),small angle X-ray scattering(SAXS),and transmission electron microscopy(TEM).Experimental results reveal that the improved precipitation kinetics of alloys in the thickness plane(denoted as sample II)as compared to those in the rolling plane(denoted as sample I),which arises due to a higher dislocation density(morphology of dislocation cells)of the thickness plane than that of the rolling plane(morphology of dislocations and dislocation tangles).Specifically,because of different dislocation morphologies,the magnetic field positively and negatively affects the dislocation activity in samples I and II,leading to enhanced and suppressed precipitation behaviors,respectively.Interestingly,nucleation of theηphase is facilitated in the UFG alloy at the critical temperature(140℃)because it affords a faster rate of atom diffusion and a higher dislocation density as compared to those exhibited by its coarse-grained alloy.This systematic and comprehensive study provides new insights into dislocation morphology and precipitation behaviour of the UFG 7075 Al alloy,while enabling the optimization of precipitation kinetics. 展开更多
关键词 ultrafine-grained Al alloy Precipitation behaviors Magnetic field Dislocation morphology Critical temperature
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大塑性变形制备超细晶生物医用钛合金的研究进展 被引量:5
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作者 林正捷 王立强 +2 位作者 吕维洁 覃继宁 张荻 《材料与冶金学报》 CAS 北大核心 2014年第3期206-211,共6页
生物医用钛合金具有高强度、良好的耐蚀性能、较低的弹性模量、优异的生物相容性,已成为具有广阔应用前景的医用金属材料之一.与传统医用钛合金相比,超细晶医用钛合金具有更高的强度与更好的疲劳性能以及耐腐蚀性能.此外,超细晶钛合金... 生物医用钛合金具有高强度、良好的耐蚀性能、较低的弹性模量、优异的生物相容性,已成为具有广阔应用前景的医用金属材料之一.与传统医用钛合金相比,超细晶医用钛合金具有更高的强度与更好的疲劳性能以及耐腐蚀性能.此外,超细晶钛合金可诱导骨组织向内生长,增加界面结合强度,加快骨修复进程,在硬组织修复材料领域具有广阔的应用前景.阐述了各种大塑性变形(Severe Plastic Deformation)法制备超细晶生物医用钛合金的研究状况与最新进展,指出了SPD法制备医用钛合金中存在的技术问题和发展方向,并展望了利用SPD法对生物医用钛合金改性将成为生物医用材料的研究热点. 展开更多
关键词 大塑性变形 超细晶 医用钛合金
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Resolving the sintering conundrum of high-rhenium tungsten alloys
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作者 Zhongyou Que Xingyu Li +8 位作者 Lin Zhang Xuanhui Qu Zichen Wei Chenguang Guo Haishen Sun Mingli Qin Gang Chen Peinan Du Yanhao Dong 《Journal of Materials Science & Technology》 SCIE EI CAS CSCD 2023年第35期78-85,共8页
Tungsten-rhenium(W-Re)alloys with high-Re contents are the preferred refractory metal materials in many applications because of the improved ductility and processability over pure W and low-Re tung-sten alloys.However... Tungsten-rhenium(W-Re)alloys with high-Re contents are the preferred refractory metal materials in many applications because of the improved ductility and processability over pure W and low-Re tung-sten alloys.However,the sintering concurrently becomes increasingly more difficult with increasing Re contents.Here we proposed that the sintering conundrum is caused by the lowered crystal symmetry and the wider dihedral angle distribution when body-center-cubic(BCC)W is alloyed with more hexagonal-close-packed(HCP)Re,which results in inefficient pore removal in the final stage sintering.We showed that the conundrum can be resolved by pressureless two-step sintering(TSS)which suppresses acceler-ating final-stage grain growth,and our proposal is supported by the data of the critical densityρc that is required to start the second step for successful TSS at different W-Re compositions.Dense ultrafine-grained W-Re alloys with∼300 nm average grain size and up to 25 wt%Re were successfully produced.Our work demonstrates the unique opportunities offered by two-step sintering to advance the scientific understanding and technological practices in powder metallurgy and related fields. 展开更多
关键词 W-Re alloys Two-step sintering grain growth ultrafine-grained materials
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超细WC-6Co硬质合金注射参数的优化 被引量:4
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作者 谢兴铖 林晨光 +1 位作者 贾成厂 曹瑞军 《稀有金属材料与工程》 SCIE EI CAS CSCD 北大核心 2015年第12期3202-3207,共6页
采用正交实验方法研究了注射温度、注射压力、注射速度、保压压力及其交互作用对超细WC-6Co硬质合金注射成形坯质量的影响。通过直观分析和方差分析,比较了各因素影响注射坯质量的显著程度,优化了注射成形参数。结果表明:注射温度与注... 采用正交实验方法研究了注射温度、注射压力、注射速度、保压压力及其交互作用对超细WC-6Co硬质合金注射成形坯质量的影响。通过直观分析和方差分析,比较了各因素影响注射坯质量的显著程度,优化了注射成形参数。结果表明:注射温度与注射压力的交互作用、注射温度与保压压力的交互作用、注射温度和注射速度对注射坯密度的影响显著;注射温度与保压压力的交互作用、注射温度与注射压力的交互作用和注射速度对注射坯抗弯强度的影响显著;台阶状圆棒的最佳注射参数组合为注射温度为100℃,注射压力为60 MPa,注射速度为40%,保压压力为20 MPa。 展开更多
关键词 超细 硬质合金 注射参数 正交实验
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Tension-Compression Asymmetry in Ultrafine-grained Commercially Pure Ti Processed by ECAP
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作者 刘晓燕 LI Shuaikang +1 位作者 YANG Xirong LUO Lei 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS CSCD 2023年第3期689-694,共6页
A homogenous microstructure of ultrafine-grained (UFG) commercially pure (CP) Ti characterized by equiaxed grains/subgrains with an average grain size of about 150 nm and strong prismatic fiber texture were obtained a... A homogenous microstructure of ultrafine-grained (UFG) commercially pure (CP) Ti characterized by equiaxed grains/subgrains with an average grain size of about 150 nm and strong prismatic fiber texture were obtained after 4 passes of equal channel angular pressing (ECAP).Tension–compression asymmetry in yield and work hardening behavior of UFG CP Ti were investigated by uniaxial tension and compression tests.The experimental results reveal that UFG CP Ti exhibits a relatively obvious tensioncompression asymmetry in yielding and work hardening behavior.The basal and prismaticslip are suppressed either for tension or compression,which is the easiest to activate.The tension twin system{1012}<1011> easily activated in compression deformation due to the prismatic fiber texture based on the Schmidt factor,consequently resulting in a lower yield strength under compression than tension.ECAP can improve the tension-compression asymmetry of CP Ti due to grain refinement.The interaction among the dislocations,grain boundaries and deformation twins are the main work hardening mechanisms for compression deformation,while the interaction between the dislocations and grain boundaries for tension deformation.Deformation twins lead to the higher work hardening under compression than tension. 展开更多
关键词 ultrafine-grained commercially pure Ti equal channel angular pressing tensioncompression asymmetry texture TWINNING
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大塑性变形制备超细晶钛及其合金的腐蚀行为研究进展
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作者 谷艳霞 马爱斌 +3 位作者 江静华 吴浩然 陆李和 桑俊锋 《现代交通与冶金材料》 CAS 2023年第3期61-65,共5页
通过大塑性变形技术,可以细化晶粒,获得超细晶钛及其合金,明显提高其强度,但也会影响其耐腐蚀性能。综述了超细晶钛及其合金腐蚀行为的研究现状,讨论了晶粒尺寸、织构、位错密度、氧化膜厚度结构、组织均匀程度、晶界特征分布等因素对... 通过大塑性变形技术,可以细化晶粒,获得超细晶钛及其合金,明显提高其强度,但也会影响其耐腐蚀性能。综述了超细晶钛及其合金腐蚀行为的研究现状,讨论了晶粒尺寸、织构、位错密度、氧化膜厚度结构、组织均匀程度、晶界特征分布等因素对超细晶纯钛耐蚀性的影响。其中,最主要的影响因素是晶粒尺寸和织构。但是超细晶钛及其合金的耐蚀性受到多种因素的共同影响,各影响因素之间存在竞争关系。此外,基于当前的耐蚀化进展,对其未来的研究方向进行了展望。 展开更多
关键词 钛合金 超细晶 腐蚀 大塑性变形
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A crystal plasticity based approach to establish role of grain size and crystallographic texture in the Tension–Compression yield asymmetry and strain hardening behavior of a Magnesium–Silver–Rare Earth alloy 被引量:3
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作者 Sourav Mishra F.Khan S.K.Panigrahi 《Journal of Magnesium and Alloys》 SCIE EI CAS CSCD 2022年第9期2546-2562,共17页
Existence of tension–compression yield asymmetry is a serious limitation to the load bearing capablities of Magnesium alloys in a number of light weight structural applications.The present work is aimed at nullifying... Existence of tension–compression yield asymmetry is a serious limitation to the load bearing capablities of Magnesium alloys in a number of light weight structural applications.The present work is aimed at nullifying the tension to compression asymmetry problem and strain hardening anomalies in a Magnesium–Silver–Rare Earth alloy by engineering different levels of microstructural conditions via friction stir processing and post process annealing.The existence and extent of yield asymmetry ratio in the range of microstructural conditions was experimentally obtained through quasistatic tensile and compression tests.The yield asymmetry problem was profoundly present in specimens of coarse grained microstructures when compared to their fine grained and ultra fine grained counterparts.The impact of the microstructure and associated mechanisms of plasticity on the macroscopic strain hardening behavior was established by Kock–Mecking’s analysis.Crystal plasticity simulations using Viscoplastic Self Consistency approach revealed the consequential role of extension twinning mechanism for the existence of yield asymmetry and anomalies in strain hardening behavior.This was especially dominant with coarsening of grain size.Electron Microscopy and characterization were conducted thoroughly in partially deformed specimens to confirm the predictions of the above simulations.The role of crystallographic texture for inducing the polarity to Tension–Compression yield asymmetry was corroborated.A critical grain size in Magnesium–Silver–Rare earth alloy was hereby established which could nullify influences of extension twinning in yield asymmetry ratio. 展开更多
关键词 Magnesium silver rare earth alloy Friction stir processing ultrafine-grained microstructure Tension to compression yield strength asymmetry Crystallographic texture Strain hardening Kock mecking plots Visco plastic self consistency
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Enhanced mechanical properties of a carbon and nitrogen co-doped interstitial high-entropy alloy via tuning ultrafine-grained microstructures
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作者 Wei Jiang Heng Wang +1 位作者 Zhiming Li Yonghao Zhao 《Journal of Materials Science & Technology》 SCIE EI CAS CSCD 2023年第13期128-137,共10页
C-N co-doped interstitial high entropy alloy(iHEA)was reported to have high strength and ductility.However,iHEA with fully recrystallized ultrafine grains(UFGs)and underlying thermally activated pro-cesses associated ... C-N co-doped interstitial high entropy alloy(iHEA)was reported to have high strength and ductility.However,iHEA with fully recrystallized ultrafine grains(UFGs)and underlying thermally activated pro-cesses associated with dislocation slip,twinning,and solute drag have not been reported yet.In this work,a C-N co-doped iHEA with nominal composition Fe_(48.5)Mn_(30)Co_(10)Cr_(10)C_(0.5)N_(1.0)(at.%)was prepared,and the microstructures were tuned by cold-rolling and annealing treatments to improve mechanical properties.Upon cold-rolling with a strain of 1.74,the main microstructures in the iHEA are composed of nano-grains,nano-twins,HCP laminates,and high density of dislocations,leading to ultrahigh hardness of 466.7 HV and tensile strength of 1730 MPa at the expense of ductility(2.44%).Both the nanostructures and the high hardness of the iHEA can be maintained up to an annealing temperature of 600℃(462.5 HV).After annealing at 650℃ for 1 h,the UFG microstructures are obtained in the iHEA,containing re-crystallized grains with an average grain size of 0.91μm and nanoprecipitates with an average diameter of 90.8 nm.The combined strengthening and hardening effects of UFGs,nanoprecipitates,twinning,and solutes contribute to high strain hardening(n=0.81),gigapascal yield strength(984 MPa),and good duc-tility(20%).The C-N co-doping leads to a strong drag effect on dislocation slip,resulting in a nano-scale mean free path of dislocation slip λ(1.44 nm)and much small apparent activation volume V^(∗)(15.8 b^(3))of the UFG iHEA. 展开更多
关键词 ultrafine-grained high-entropy alloys Interstitial atoms Thermomechanical processing MICROSTRUCTURES Mechanical properties
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塑性变形中晶粒变形与细化机制的影响因素 被引量:3
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作者 黄丰 钟飞 +1 位作者 李鹏云 梁永纯 《铸造技术》 CAS 北大核心 2011年第11期1602-1605,共4页
讨论了层错能、应变速率和变形温度等因素在塑性变形制备超细晶/纳米晶材料的变形过程中,对变形机制与晶粒细化机制的影响。研究表明,随着层错能的降低,晶粒的变形机制会由位错滑移向机械孪生转变,有利于晶粒的细化。应变速率的增加与... 讨论了层错能、应变速率和变形温度等因素在塑性变形制备超细晶/纳米晶材料的变形过程中,对变形机制与晶粒细化机制的影响。研究表明,随着层错能的降低,晶粒的变形机制会由位错滑移向机械孪生转变,有利于晶粒的细化。应变速率的增加与变形温度的降低有利于抑制位错动态回复、增加流变应力,促使晶粒进一步细化。 展开更多
关键词 超细晶结构材料 纳米结构材料 塑性变形
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A high-Nb-TiAl alloy with ultrafine-grained structure fabricated by cryomilling and spark plasma sintering
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作者 Hao Deng Yong-Qiang Wei +3 位作者 Jun Tang Ai-Jun Chen Long-Qing Chen Zu-Xi Xia 《Rare Metals》 SCIE EI CAS CSCD 2023年第5期1678-1685,共8页
In this work,an ultrafine-grained high-Nb-TiAl alloy with a nominal composition of Ti-45Al-8Nb-0.2W-0.2B(at%)was prepared by cryomilling and subsequent spark plasma sintering(SPS)technique.The chemical composition,par... In this work,an ultrafine-grained high-Nb-TiAl alloy with a nominal composition of Ti-45Al-8Nb-0.2W-0.2B(at%)was prepared by cryomilling and subsequent spark plasma sintering(SPS)technique.The chemical composition,particle size,morphology and crystallite size of cryomilled powder were studied.It is found that cryomilling can effectively reduce the particle size and enhance grain refinement.The ingots sintered at 900 and 1000℃ show an equiaxed near-γmicrostructure with grain sizes<700 nm,while the sample sintered at 1100℃exhibits duplex microstructure.Especially,the one sintered at 1000℃ has excellent mechanical properties,whose compression yield strength,fracture strength,bending strength and plastic strain achieve 1310,2174,578 MPa and 16.8%,respectively.The reasons for the effect of cryomilling and the mechanical behavior of sintered ingots were discussed.It is suggested that cryomilling in combination with SPS is an effective way to synthesize high-NbTiAl alloy with ultrafine-grained structure. 展开更多
关键词 CRYOMILLING Spark plasma sintering Titanium aluminide ultrafine-grained structure
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Nanoscale deformation of multiaxially forged ultrafine-grained Mg-2Zn-2Gd alloy with high strength-high ductility combination and comparison with the coarse-grained counterpart 被引量:2
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作者 K. Li V.S.Y.Injeti +2 位作者 P. Trivedi L.E. Murr R.D.K. Misra 《Journal of Materials Science & Technology》 SCIE EI CAS CSCD 2018年第2期311-316,共6页
Cold processing of magnesium (Mg) alloys is a challenge because Mg has a hexagonal close-packed (HCP) lattice with limited slip systems, which makes it difficult to plastically deform at low temperature. To addres... Cold processing of magnesium (Mg) alloys is a challenge because Mg has a hexagonal close-packed (HCP) lattice with limited slip systems, which makes it difficult to plastically deform at low temperature. To address this challenge, a combination of annealing of as-cast alloy and multi-axial forging was adopted ro obtain isotropic ultrafine-grained (UFG) structure in a lean Mg-2Zn-2Gd alloy with high strength (yield strength: ~227 MPa)-high ductility (% elongation: ~30%) combination. This combination of strength and ductility is excellent for the lean alloy, enabling an understanding of deformation processes in a formable high strength Mg-rare earth alloy. The nanoscale deformation behavior was studied via nanoindentation and electron microscopy, and the behavior was compared with its low strength (yield strength: ~46 MPa) - low ductility (% elongation: ~7%) coarse-grained (CG) counterpart. In the UFG alloy, extensive dislocation slip was an active deformation mechanism, while in the CG alloy, mechanical twinning occurred. The differences in the deformation mechanisms of UFG and CG alloys were reflected in the discrete burst in the load-displacement plots. The deformation of Mg-2Zn-2Gd alloys was significantly influenced by the grain structure, such that there was change in the deformation mechanism from dislocation slip (non-basal slip) to nanoscale twins in the CG structure. The high plasticity ofUFG Mg alloy involved high dislocation activity and change in activation volume. 展开更多
关键词 Magnesium alloy ultrafine-grained Nanoscale deformation
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