Magnetite concentrate was recovered from ferrous sulphate by co-precipitation and magnetic separation. In co-precipitation process, the effects of reaction conditions on iron recovery were studied, and the optimal rea...Magnetite concentrate was recovered from ferrous sulphate by co-precipitation and magnetic separation. In co-precipitation process, the effects of reaction conditions on iron recovery were studied, and the optimal reaction parameters are proposed as follows: n(CaO)/n(Fe2+) 1.4:1, reaction temperature 80 ℃, ferrous ion concentration 0.4 mol/L, and the final mole ratio of Fe3+ to FJ+ in the reaction solution 1.9-2.1. In magnetic separation process, the effects of milling time and magnetic induction intensity on iron recovery were investigated. Wet milling played an important part in breaking the encapsulated magnetic phases. The results showed that the mixed product was wet-milled for 20 min before magnetic separation, the grade and recovery rate of iron in magnetite concentrate were increased from 51.41% and 84.15% to 62.05% and 85.35%, respectively.展开更多
基金financially supported by the National Basic Research Program of China(Nos.2013CB632601 and 2013CB632604)the National Science Foundation for Distinguished Young Scholars of China(Nos.51125018 and 51504230)+2 种基金the Key Research Program of Chinese Academy of Sciences(No.KGZD-EW-201-2)the National Natural Science Foundation of China(Nos.51374191 and 2110616751104139)China Postdoctoral Science Foundation(Nos.2012M510552 and 2013T60175)
基金Project(2013A090100013)supported by the Special Project on the Integration of Industry,Education and Research of Guangdong Province,ChinaProject(201407300993)supported by the High Technology Research and Development Program of Xinjiang Uygur Autonomous Region,China
文摘Magnetite concentrate was recovered from ferrous sulphate by co-precipitation and magnetic separation. In co-precipitation process, the effects of reaction conditions on iron recovery were studied, and the optimal reaction parameters are proposed as follows: n(CaO)/n(Fe2+) 1.4:1, reaction temperature 80 ℃, ferrous ion concentration 0.4 mol/L, and the final mole ratio of Fe3+ to FJ+ in the reaction solution 1.9-2.1. In magnetic separation process, the effects of milling time and magnetic induction intensity on iron recovery were investigated. Wet milling played an important part in breaking the encapsulated magnetic phases. The results showed that the mixed product was wet-milled for 20 min before magnetic separation, the grade and recovery rate of iron in magnetite concentrate were increased from 51.41% and 84.15% to 62.05% and 85.35%, respectively.