In the traditional research of volatile compounds, some trace-level compounds could not be identified by gas chromatography-mass spectrometry. Target and post-targeted methods were applied in the investigation of trac...In the traditional research of volatile compounds, some trace-level compounds could not be identified by gas chromatography-mass spectrometry. Target and post-targeted methods were applied in the investigation of trace-level volatile compounds in fresh turf crop (Lolium perenne L.) based on gas chromatography in combination with hybrid quadrupole time-of-flight mass spectrometry. According to literatures published, a target analysis was performed by using retention index, accurate masses of characteristic ions and second-stage mass spectra (MS2 spectra). And a series of experiments showed that low electron impact energy was beneficial to the improvement of the abundances of low abundance molecular ion peak. peak was beneficial to qualitative analysis. Totally, 60 Enhancing the abundances of low abundance molecular ion volatile compounds were identified, the great majority cornpounds of which were benzeneacetaldehyde (14.8%), 2,5-dimethyl-pyrazine (9.6%), and hexanal (9.3%). Identification was complied by mass spectral search, retention index and accurate masses of characteristic ions.展开更多
EHP(English for Hotel Purpose)即饭店专门用途英语使用者的真实需求分析一直以来缺乏相关的实证调查和研究,导致饭店英语的教学与实际需求不一致。本文采用实地调查方法对武汉市涉外星级饭店员工的饭店英语需求分析进行了深度和广度了...EHP(English for Hotel Purpose)即饭店专门用途英语使用者的真实需求分析一直以来缺乏相关的实证调查和研究,导致饭店英语的教学与实际需求不一致。本文采用实地调查方法对武汉市涉外星级饭店员工的饭店英语需求分析进行了深度和广度了解,并对得出的结论进行探讨,最后提出必须依据饭店英语使用者的真实需求运用相关原则以改进饭店英语的教学水平。展开更多
文摘In the traditional research of volatile compounds, some trace-level compounds could not be identified by gas chromatography-mass spectrometry. Target and post-targeted methods were applied in the investigation of trace-level volatile compounds in fresh turf crop (Lolium perenne L.) based on gas chromatography in combination with hybrid quadrupole time-of-flight mass spectrometry. According to literatures published, a target analysis was performed by using retention index, accurate masses of characteristic ions and second-stage mass spectra (MS2 spectra). And a series of experiments showed that low electron impact energy was beneficial to the improvement of the abundances of low abundance molecular ion peak. peak was beneficial to qualitative analysis. Totally, 60 Enhancing the abundances of low abundance molecular ion volatile compounds were identified, the great majority cornpounds of which were benzeneacetaldehyde (14.8%), 2,5-dimethyl-pyrazine (9.6%), and hexanal (9.3%). Identification was complied by mass spectral search, retention index and accurate masses of characteristic ions.
文摘EHP(English for Hotel Purpose)即饭店专门用途英语使用者的真实需求分析一直以来缺乏相关的实证调查和研究,导致饭店英语的教学与实际需求不一致。本文采用实地调查方法对武汉市涉外星级饭店员工的饭店英语需求分析进行了深度和广度了解,并对得出的结论进行探讨,最后提出必须依据饭店英语使用者的真实需求运用相关原则以改进饭店英语的教学水平。