In order to investigate the effect of microstructural characterization on the mechanical properties and retained austenite stability, a different type of quenching and partitioning steel(I-Q&P) through intercritica...In order to investigate the effect of microstructural characterization on the mechanical properties and retained austenite stability, a different type of quenching and partitioning steel(I-Q&P) through intercritical annealing before the quenching and partitioning process was designed, which can realize lamellar intercritical microstructure compared to the conventional quenching and partitioning(Q&P) process. The morphology of ferrite and martensite/retained austenite is lamellar in the I-Q&P steel while it is equiaxed after being heat-treated by conventional Q&P process. The I-Q&P steel is proved to have better formability and mechanical properties than conventional Q&P steel, which is due to the highervolume fraction of retained austenite in the I-Q&P steel and confirmed by electron backscattering diffraction patterns and X-ray diffraction. Furthermore, the stability of retained austenite in I-Q&P steel is also higher than that in conventional Q&P steel, which is investigated by tensile tests and differential scanning calorimetry.展开更多
Thermal decomposition of retained austenite in TRIP steel was investigated by means of differential scanning calorimetry(DSC).The decomposition curve was abnormal,and the decomposition temperature and the activation...Thermal decomposition of retained austenite in TRIP steel was investigated by means of differential scanning calorimetry(DSC).The decomposition curve was abnormal,and the decomposition temperature and the activation energy were measured by the Kissinger method,which were all higher than those in quenched steel.The thermal decomposition data of samples soaked in liquid nitrogen after TRIP treatment were all similar to those without additional low temperature treatment.It indicated that there is a high thermal stability in retained austenite of the TRIP steel at low temperature,which was also proved by XRD analysis.展开更多
In this work, the effect of prior cold deformation on the stability of retained austenite in GCr15 bearing steel was investigated after quenching and tempering treatment. The thermal stability was evaluated by calcula...In this work, the effect of prior cold deformation on the stability of retained austenite in GCr15 bearing steel was investigated after quenching and tempering treatment. The thermal stability was evaluated by calculating thermal activation energy for decomposition of retained austenite using differential scanning calorimeter. The mechanical stability was investigated according to the strain-induced martensitic transformation behavior of retained austenite under the standard compression testing. It is found that the prior cold deformation not only accelerates the carbide dissolution during the austenitization process but also contributes to the carbon partitioning in the tempering stage due to the higher density of phase boundaries, which results in the improvement of the thermal stability of retained austenite. Due to the enhanced carbide dissolution, the higher carbon content in the prior austenite will intensify the isotropic strain of martensitic transformation. As a consequence, the film-like retained austenite is likely to form under a higher hydrostatic pressure and thus shows a higher mechanical stability. Additionally, it is noteworthy that the benefits of the prior cold deformation to the stability of retained austenite would be saturated when the cold deformation degree is larger than 40%.展开更多
文摘In order to investigate the effect of microstructural characterization on the mechanical properties and retained austenite stability, a different type of quenching and partitioning steel(I-Q&P) through intercritical annealing before the quenching and partitioning process was designed, which can realize lamellar intercritical microstructure compared to the conventional quenching and partitioning(Q&P) process. The morphology of ferrite and martensite/retained austenite is lamellar in the I-Q&P steel while it is equiaxed after being heat-treated by conventional Q&P process. The I-Q&P steel is proved to have better formability and mechanical properties than conventional Q&P steel, which is due to the highervolume fraction of retained austenite in the I-Q&P steel and confirmed by electron backscattering diffraction patterns and X-ray diffraction. Furthermore, the stability of retained austenite in I-Q&P steel is also higher than that in conventional Q&P steel, which is investigated by tensile tests and differential scanning calorimetry.
基金Item Sponsored by National Natural Science Foundation of China(50171038)Belgium-China Bilateral Project BIL04/13
文摘Thermal decomposition of retained austenite in TRIP steel was investigated by means of differential scanning calorimetry(DSC).The decomposition curve was abnormal,and the decomposition temperature and the activation energy were measured by the Kissinger method,which were all higher than those in quenched steel.The thermal decomposition data of samples soaked in liquid nitrogen after TRIP treatment were all similar to those without additional low temperature treatment.It indicated that there is a high thermal stability in retained austenite of the TRIP steel at low temperature,which was also proved by XRD analysis.
基金supported by the National Natural Science Foundation of China (Nos. 51575414 and 51605354)the 111 Project (B17034), the China Postdoctoral Science Foundation (No. 2017M612524)the State Key Laboratory of Materials Processing and Die & Mould Technology, Huazhong University of Science and Technology (P2019-017)
文摘In this work, the effect of prior cold deformation on the stability of retained austenite in GCr15 bearing steel was investigated after quenching and tempering treatment. The thermal stability was evaluated by calculating thermal activation energy for decomposition of retained austenite using differential scanning calorimeter. The mechanical stability was investigated according to the strain-induced martensitic transformation behavior of retained austenite under the standard compression testing. It is found that the prior cold deformation not only accelerates the carbide dissolution during the austenitization process but also contributes to the carbon partitioning in the tempering stage due to the higher density of phase boundaries, which results in the improvement of the thermal stability of retained austenite. Due to the enhanced carbide dissolution, the higher carbon content in the prior austenite will intensify the isotropic strain of martensitic transformation. As a consequence, the film-like retained austenite is likely to form under a higher hydrostatic pressure and thus shows a higher mechanical stability. Additionally, it is noteworthy that the benefits of the prior cold deformation to the stability of retained austenite would be saturated when the cold deformation degree is larger than 40%.