The CoCrFeNiMn high entropy alloy was produced by homogenization, cold rolling and recrystallization. The effects of thermomechanical processing on microstructures and tensile properties at different temperatures were...The CoCrFeNiMn high entropy alloy was produced by homogenization, cold rolling and recrystallization. The effects of thermomechanical processing on microstructures and tensile properties at different temperatures were investigated using X-ray diffractometry（XRD）, optical microscopy（OM）, scanning electron microscopy（SEM） and multi-functional testing machine. The results show that dendritic structures in cast alloy evolve into equiaxed grains after being recrystallized, with single face-centered cubic（FCC） phase detected. The most refined alloys, stemming from the highest rolling ratio（40%）, exhibit the highest strength due to the grain boundary strengthening, while the variation of elongation with temperature shows a concave feature. For the coarse-grained alloys, both the ductility and work hardening ability decrease monotonically with increasing temperature. Serrated flow observed at intermediate temperatures is attributed to the effective pinning of dislocations, which manifests the occurrence of dynamic strain hardening and results in the deterioration in ductility. Besides, dimples on the fracture surfaces indicate the typical ductile rupture mode.展开更多
The effect of different homogenization treatments on the microstructure and properties of the 7N01 aluminum alloy was investigated using hardness measurements, electrical conductivity measurements, tensile and slow st...The effect of different homogenization treatments on the microstructure and properties of the 7N01 aluminum alloy was investigated using hardness measurements, electrical conductivity measurements, tensile and slow strain rate tests, electron probe microanalysis, optical microscopy, scanning electron microscopy, and transmission electron microscopy. The results revealed that three-step homogenization improved the uniformity of Zr distribution by eliminating segregation of the main alloying elements. During the second homogenization step at 350 °C for 10 h, coarse and strip-like equilibrium η phases formed which assisted the nucleation of Al3Zr dispersoids and reduced the width of the precipitate-free zone of A13Zr dispersoids. As a result, coarse recrystallization was greatly reduced after homogenization at 200 °C, 2 h ＋ 350 °C, 10 h ＋ 470 °C, 12 h, which contributed to improving the overall properties of the 7N01 aluminum alloys.展开更多
Numerical simulation and experiments were introduced to develop AA4045/AA3003 cladding billets with different clad-ratios. The temperature fields, microstructures and mechanical properties near interface were investig...Numerical simulation and experiments were introduced to develop AA4045/AA3003 cladding billets with different clad-ratios. The temperature fields, microstructures and mechanical properties near interface were investigated in detail. The results show that cladding billets with different clad-ratios were fabricated successfully. Si and Mn elements diffused across the bonding interface and formed diffusion layer. With the increase of clad-layer thickness, the interfacial region transforms from semisolid-solid state to liquid-solid state and the diffusion layer increased from 10 to 25 μm. The hardness at interface is higher than that of AA3003 side but lower than that of the other side. The bonding strength increased with the clad-layer thickness, attributing to solution strengthening due to elements diffusion. The cladding billets were extruded into clad pipe by indirect extrusion process after homogenization. The clad pipe remained the interfacial characteristics of as-cast cladding billet and the heredity of clad-ratio during deformation was testified.展开更多
基金Project(11572306)supported by the National Natural Science Foundation of China
文摘The CoCrFeNiMn high entropy alloy was produced by homogenization, cold rolling and recrystallization. The effects of thermomechanical processing on microstructures and tensile properties at different temperatures were investigated using X-ray diffractometry（XRD）, optical microscopy（OM）, scanning electron microscopy（SEM） and multi-functional testing machine. The results show that dendritic structures in cast alloy evolve into equiaxed grains after being recrystallized, with single face-centered cubic（FCC） phase detected. The most refined alloys, stemming from the highest rolling ratio（40%）, exhibit the highest strength due to the grain boundary strengthening, while the variation of elongation with temperature shows a concave feature. For the coarse-grained alloys, both the ductility and work hardening ability decrease monotonically with increasing temperature. Serrated flow observed at intermediate temperatures is attributed to the effective pinning of dislocations, which manifests the occurrence of dynamic strain hardening and results in the deterioration in ductility. Besides, dimples on the fracture surfaces indicate the typical ductile rupture mode.
基金Projects(2016YFB0300901,2016YFB0300902)supported by the National Key Research and Development Program of ChinaProject(51375503)supported by the National Natural Science Foundation of ChinaProject(2013A017)supported by Guangxi Zhuangzu Autonomous Region of China
文摘The effect of different homogenization treatments on the microstructure and properties of the 7N01 aluminum alloy was investigated using hardness measurements, electrical conductivity measurements, tensile and slow strain rate tests, electron probe microanalysis, optical microscopy, scanning electron microscopy, and transmission electron microscopy. The results revealed that three-step homogenization improved the uniformity of Zr distribution by eliminating segregation of the main alloying elements. During the second homogenization step at 350 °C for 10 h, coarse and strip-like equilibrium η phases formed which assisted the nucleation of Al3Zr dispersoids and reduced the width of the precipitate-free zone of A13Zr dispersoids. As a result, coarse recrystallization was greatly reduced after homogenization at 200 °C, 2 h ＋ 350 °C, 10 h ＋ 470 °C, 12 h, which contributed to improving the overall properties of the 7N01 aluminum alloys.
基金Project(2015B090926013)supported by the Science and Technology Program of Guangdong Province,ChinaProject(20170540307)supported by the Natural Science Foundation of Liaoning Province,China
文摘Numerical simulation and experiments were introduced to develop AA4045/AA3003 cladding billets with different clad-ratios. The temperature fields, microstructures and mechanical properties near interface were investigated in detail. The results show that cladding billets with different clad-ratios were fabricated successfully. Si and Mn elements diffused across the bonding interface and formed diffusion layer. With the increase of clad-layer thickness, the interfacial region transforms from semisolid-solid state to liquid-solid state and the diffusion layer increased from 10 to 25 μm. The hardness at interface is higher than that of AA3003 side but lower than that of the other side. The bonding strength increased with the clad-layer thickness, attributing to solution strengthening due to elements diffusion. The cladding billets were extruded into clad pipe by indirect extrusion process after homogenization. The clad pipe remained the interfacial characteristics of as-cast cladding billet and the heredity of clad-ratio during deformation was testified.
