Two compounds of dehydroabietylamine acetate 1 and dehydroabietylamine 2 have been studied. The X-ray study demonstrated that compound 1 is in orthorhombic space group P212121 with a = 6.1310（12）, b = 10.605（2）, c...Two compounds of dehydroabietylamine acetate 1 and dehydroabietylamine 2 have been studied. The X-ray study demonstrated that compound 1 is in orthorhombic space group P212121 with a = 6.1310（12）, b = 10.605（2）, c = 35.717（7）A, C23H39NO3, Mr = 377.55, V = 2322.3（8）A^3, Z = 4, Dc = 1.080 g/cm^3, F（000） = 832,μ = 0.070 mm^-1, R = 0.0795 and wR = 0.1528. Hydrogen bonds are cross-linked by the N and O atoms to form one-dimensional chains running along the a axis. Antibacterial analysis shows strong activity against studied bacteria and fungi in compound 2.展开更多
Three derivatives of dehydroabietylamine were synthesized from dehydroabietylamine through trifluoro-acetyltion,nitration and hydrolysis.Two of them were first reported as new compounds.The compounds were characterize...Three derivatives of dehydroabietylamine were synthesized from dehydroabietylamine through trifluoro-acetyltion,nitration and hydrolysis.Two of them were first reported as new compounds.The compounds were characterized by FT-IR,1H NMR,EI-MS,elemental analyses and HRMS.Their bactericidal activities were investigated,and the results indicated that 12-nitro-dehydroabietylamine and 12,14-dinitro-dehydroabietylamine had strong bactericidal activity against E.coli,Staphylococcus aureus,Pseudomonas fluorescens.展开更多
文摘Two compounds of dehydroabietylamine acetate 1 and dehydroabietylamine 2 have been studied. The X-ray study demonstrated that compound 1 is in orthorhombic space group P212121 with a = 6.1310（12）, b = 10.605（2）, c = 35.717（7）A, C23H39NO3, Mr = 377.55, V = 2322.3（8）A^3, Z = 4, Dc = 1.080 g/cm^3, F（000） = 832,μ = 0.070 mm^-1, R = 0.0795 and wR = 0.1528. Hydrogen bonds are cross-linked by the N and O atoms to form one-dimensional chains running along the a axis. Antibacterial analysis shows strong activity against studied bacteria and fungi in compound 2.
文摘Three derivatives of dehydroabietylamine were synthesized from dehydroabietylamine through trifluoro-acetyltion,nitration and hydrolysis.Two of them were first reported as new compounds.The compounds were characterized by FT-IR,1H NMR,EI-MS,elemental analyses and HRMS.Their bactericidal activities were investigated,and the results indicated that 12-nitro-dehydroabietylamine and 12,14-dinitro-dehydroabietylamine had strong bactericidal activity against E.coli,Staphylococcus aureus,Pseudomonas fluorescens.
