Pretreatment of high content of Si- and Al-containing cyanide tailings by water leaching to remove some impurities, such as the major impurities minerals of Si and A1, as well as its effect on Fe extraction in the wat...Pretreatment of high content of Si- and Al-containing cyanide tailings by water leaching to remove some impurities, such as the major impurities minerals of Si and A1, as well as its effect on Fe extraction in the water leaching process was investigated. The effects of different parameters on iron recovery were studied, and the reaction parameters were proposed as follows： sodium carbonate content of 30%, water leaching at 60 ~C for 5 min, liquid/solid ratio of 15：1, and exciting current of 2 A. Under these optimal conditions, magnetic concentrate containing 59.11% total iron and a total iron recovery rate of 76.12% was obtained. In addition, the microstructure and phase transformation of the process of water leaching were studied by X-ray powder diffraction technique （XRD）, Electronic image of backscattering （BEI）, X-ray fluorescence （XRF）, and energy dispersive spectrometry （EDS）. The results indicate that the soluble compound impurities generated in the roasting process are washed out, and the dissoluble substances enter into nonmagnetic materials by water leaching, realizing the effective separation of impurities and Fe.展开更多
本文通过对某硫化铜镍矿的矿石性质调查发现,随着矿石深度开采,矿石中铜镍品位的变化明显,铜镍比由原来的0.64提升到现在的0.9左右。随着铜镍比的增加,一段粗精矿的铜镍品位呈现下降趋势,对一段粗选精矿进行单体解离度分析发现铜镍矿物...本文通过对某硫化铜镍矿的矿石性质调查发现,随着矿石深度开采,矿石中铜镍品位的变化明显,铜镍比由原来的0.64提升到现在的0.9左右。随着铜镍比的增加,一段粗精矿的铜镍品位呈现下降趋势,对一段粗选精矿进行单体解离度分析发现铜镍矿物的单体解离度不够是造成精矿品位降低的主要原因。因此,对一段粗精矿进行磨矿细度、药剂添加等工艺条件的小型试验研究,试验结果表明:(1)相对于其他细度条件,在粗精矿再磨后,细度为-0.043 mm/ 80%和添加丁黄药20 g/t条件下,产生的铜镍精矿的产率、铜镍品位和回收率较高;(2)在粗精矿再磨后不添加捕收剂条件下,随着细度的增加,得到的铜镍精矿产率降低,镍品位和回收率也降低,原因可能是由于磨矿过程中有用矿物表面发生脱药所致;(3)闭路试验结果表明:相对于粗精矿不再磨(细度-0.043 mm /69%),在粗精矿再磨后(细度-0.043 mm /80%)和再磨后添加丁黄药20 g/t条件下,产生的精矿产率提高0.64个百分点,镍品位和回收率分别提高0.63个百分点和4.61个百分点,铜品位和回收率分别提高0.57个百分点和5.54个百分点。通过粗精矿再磨工艺工业应用实践可知:相对于应用前,产生的精矿镍品位和回收率分别提高了0.81个百分点和2.94个百分点,铜品位和回收率分别提高了0.30个百分点和5.85个百分点,同时,精矿中氧化镁含量满足冶炼厂对产品的要求。展开更多
The objective of the experiment was to determine the effect of feeding three levels (T3.5, T7.0 and T10.5) of energy concentrate (3.5, 7.0 and 10.5 kg cow-1 day-1) on total dry matter (DM) and energy intakes, milk yie...The objective of the experiment was to determine the effect of feeding three levels (T3.5, T7.0 and T10.5) of energy concentrate (3.5, 7.0 and 10.5 kg cow-1 day-1) on total dry matter (DM) and energy intakes, milk yield and composition, nutritional value of milk and rumen pasture neutral detergent fiber (NDF) digestion in grazing dairy cows. Twenty-one multiparous Holstein cows in early lactation (70.2 ± 13 days postpartum) producing 37.1 (±4.7) kg of milk were assigned to a 3 treatments (7 cows/treatment) × 3 periods Latin square design. Parameters of ruminal environment and pasture NDF degradation were obtained using 3 additional cows of the same breed fitted with rumen cannulae. On a wet basis, concentrate was composed by corn grain (68%), soybean meal (22%), wheat bran (8%) and a vitamin-mineral nucleus with monensin. Pasture (Medicago sativa, sp) was used in a rotational grazing system with an herbage allowance of 30 kg DM cow-1 d-1. Yield (kg cow-1 d-1) of fat corrected milk (4% FCM) resulted higher (p < 0.05) in T7.0 (29.0) compared to T3.5 (26.8) but similar to T10.5 (30.2). Milk and protein yields were linearly increased (p < 0.01) by concentrate intake. Milk fat (3.13 g/100g) and total solid contents (11.79 g/100g) did not differ whereas milk protein (p < 0.03) and casein (p < 0.01) levels (g/100g) increased linearly from 3.05 to 3.10 (protein) and from 2.42 to 2.47 (casein). Pasture intake decreased but total DM and energy consumption were enhanced showing addition effects after concentrate feeding. Body weight (BW) loss and plasmatic levels of non esterified fatty acids (NEFA) decreased with concentrate intake. Circulating levels of insulin-like growth factor-I (IGF-I) were higher (p < 0.05) in T10.5 while those of glucose, plasma urea nitrogen, insulin and somatotrophin were not affected. Ruminal pH and acetate concentration resulted lower (p < 0.05) in T10.5 when compared to T3.5. The acetate:propionate ratio decreased (p < 0.01) from 4.25 in T3.5 to 3.08 in T10.5 and ruminal ammonia nitrogen lev展开更多
基金Projects(ZR2010EL006,Y2007F60) supported by the National Science Foundation of Shandong Province of ChinaProject(J12LA04) supported by High Education Science Technology Program of Shandong Province,China
文摘Pretreatment of high content of Si- and Al-containing cyanide tailings by water leaching to remove some impurities, such as the major impurities minerals of Si and A1, as well as its effect on Fe extraction in the water leaching process was investigated. The effects of different parameters on iron recovery were studied, and the reaction parameters were proposed as follows： sodium carbonate content of 30%, water leaching at 60 ~C for 5 min, liquid/solid ratio of 15：1, and exciting current of 2 A. Under these optimal conditions, magnetic concentrate containing 59.11% total iron and a total iron recovery rate of 76.12% was obtained. In addition, the microstructure and phase transformation of the process of water leaching were studied by X-ray powder diffraction technique （XRD）, Electronic image of backscattering （BEI）, X-ray fluorescence （XRF）, and energy dispersive spectrometry （EDS）. The results indicate that the soluble compound impurities generated in the roasting process are washed out, and the dissoluble substances enter into nonmagnetic materials by water leaching, realizing the effective separation of impurities and Fe.
文摘本文通过对某硫化铜镍矿的矿石性质调查发现,随着矿石深度开采,矿石中铜镍品位的变化明显,铜镍比由原来的0.64提升到现在的0.9左右。随着铜镍比的增加,一段粗精矿的铜镍品位呈现下降趋势,对一段粗选精矿进行单体解离度分析发现铜镍矿物的单体解离度不够是造成精矿品位降低的主要原因。因此,对一段粗精矿进行磨矿细度、药剂添加等工艺条件的小型试验研究,试验结果表明:(1)相对于其他细度条件,在粗精矿再磨后,细度为-0.043 mm/ 80%和添加丁黄药20 g/t条件下,产生的铜镍精矿的产率、铜镍品位和回收率较高;(2)在粗精矿再磨后不添加捕收剂条件下,随着细度的增加,得到的铜镍精矿产率降低,镍品位和回收率也降低,原因可能是由于磨矿过程中有用矿物表面发生脱药所致;(3)闭路试验结果表明:相对于粗精矿不再磨(细度-0.043 mm /69%),在粗精矿再磨后(细度-0.043 mm /80%)和再磨后添加丁黄药20 g/t条件下,产生的精矿产率提高0.64个百分点,镍品位和回收率分别提高0.63个百分点和4.61个百分点,铜品位和回收率分别提高0.57个百分点和5.54个百分点。通过粗精矿再磨工艺工业应用实践可知:相对于应用前,产生的精矿镍品位和回收率分别提高了0.81个百分点和2.94个百分点,铜品位和回收率分别提高了0.30个百分点和5.85个百分点,同时,精矿中氧化镁含量满足冶炼厂对产品的要求。
文摘The objective of the experiment was to determine the effect of feeding three levels (T3.5, T7.0 and T10.5) of energy concentrate (3.5, 7.0 and 10.5 kg cow-1 day-1) on total dry matter (DM) and energy intakes, milk yield and composition, nutritional value of milk and rumen pasture neutral detergent fiber (NDF) digestion in grazing dairy cows. Twenty-one multiparous Holstein cows in early lactation (70.2 ± 13 days postpartum) producing 37.1 (±4.7) kg of milk were assigned to a 3 treatments (7 cows/treatment) × 3 periods Latin square design. Parameters of ruminal environment and pasture NDF degradation were obtained using 3 additional cows of the same breed fitted with rumen cannulae. On a wet basis, concentrate was composed by corn grain (68%), soybean meal (22%), wheat bran (8%) and a vitamin-mineral nucleus with monensin. Pasture (Medicago sativa, sp) was used in a rotational grazing system with an herbage allowance of 30 kg DM cow-1 d-1. Yield (kg cow-1 d-1) of fat corrected milk (4% FCM) resulted higher (p < 0.05) in T7.0 (29.0) compared to T3.5 (26.8) but similar to T10.5 (30.2). Milk and protein yields were linearly increased (p < 0.01) by concentrate intake. Milk fat (3.13 g/100g) and total solid contents (11.79 g/100g) did not differ whereas milk protein (p < 0.03) and casein (p < 0.01) levels (g/100g) increased linearly from 3.05 to 3.10 (protein) and from 2.42 to 2.47 (casein). Pasture intake decreased but total DM and energy consumption were enhanced showing addition effects after concentrate feeding. Body weight (BW) loss and plasmatic levels of non esterified fatty acids (NEFA) decreased with concentrate intake. Circulating levels of insulin-like growth factor-I (IGF-I) were higher (p < 0.05) in T10.5 while those of glucose, plasma urea nitrogen, insulin and somatotrophin were not affected. Ruminal pH and acetate concentration resulted lower (p < 0.05) in T10.5 when compared to T3.5. The acetate:propionate ratio decreased (p < 0.01) from 4.25 in T3.5 to 3.08 in T10.5 and ruminal ammonia nitrogen lev
