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雪松松针黄酮类化学成分的研究 被引量:43
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作者 刘东彦 石晓峰 +2 位作者 李冲 王东东 张军民 《中草药》 CAS CSCD 北大核心 2011年第4期631-633,共3页
目的研究雪松Cedrus deodara松针中黄酮类化学成分。方法采用硅胶、Sephadex LH-20等柱色谱方法对其醋酸乙酯萃取部位中黄酮类化学成分进行分离和纯化,并根据其理化性质及波谱数据鉴定结构。结果从雪松松针中分离得到5个黄酮类化合物,... 目的研究雪松Cedrus deodara松针中黄酮类化学成分。方法采用硅胶、Sephadex LH-20等柱色谱方法对其醋酸乙酯萃取部位中黄酮类化学成分进行分离和纯化,并根据其理化性质及波谱数据鉴定结构。结果从雪松松针中分离得到5个黄酮类化合物,分别鉴定为3′,5′-二甲氧基杨梅素-3-O-(6″-O-乙酰基)-α-D-吡喃葡萄糖苷[3′,5′-dimethoxymyricetin-3-O-(6′′-O-acetyl)-α-D-glucopyranoside,1]、杨梅素(myricetin,2)、2R,3R-二氢杨梅素(2R,3R-dihydromyricetin,3)、槲皮素(quercetin,4)、2R,3R-二氢槲皮素(2R,3R-dihydroquercetin,5)。结论化合物1为新化合物,命名为雪松酮A(cedrusone A),化合物2~5均为首次从该属植物针叶中分离得到。 展开更多
关键词 雪松松针 黄酮类 雪松酮A 杨梅素 槲皮素
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A New Flavonoid in Pine Needles of Cedrus deodara 被引量:15
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作者 LIU Dong-yan1,2,SHI Xiao-feng1,WANG Dong-dong1,2,MA Qu-huan1,ZHANG Jun-min1,2,LI Chong2 1.Gansu Academy of Medical Science,Lanzhou 730050,China 2.School of Pharmacy,Lanzhou University,Lanzhou 730030,China 《Chinese Herbal Medicines》 CAS 2011年第1期5-6,共2页
Objective To study the chemical constituents of flavonoids in pine needles of Cedrus deodara.Methods Flavonoids were isolated and purified from ethyl acetate extract of pine needles by chromatography on silica gel and... Objective To study the chemical constituents of flavonoids in pine needles of Cedrus deodara.Methods Flavonoids were isolated and purified from ethyl acetate extract of pine needles by chromatography on silica gel and Sephadex LH-20.Their structures were identified on the basis of spectroscopic analysis and chemical evidence.Results Five flavonoids were isolated and purified.Their structures were identified as cedrusone A(1),myricetin (2),2R,3R-dihydromyricetin(3),quercetin(4),and 2R,3R-dihydroquercetin(5).Conclusion Compound 1 is a new compound.Compounds 2-5 are isolated from pine needles of this genus for the first time. 展开更多
关键词 cedrusone A FLAVONOIDS MYRICETIN pine needles of Cedrus deodara QUERCETIN
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