Ternary Pb-Sn-Cd alloy nanoparticles were prepared b y the sonochemical dispersion method. The nanoparticles were found to be about 40 —60 nm and coated with an amorphous layer of surfactant dioctadecyldithiophosph a...Ternary Pb-Sn-Cd alloy nanoparticles were prepared b y the sonochemical dispersion method. The nanoparticles were found to be about 40 —60 nm and coated with an amorphous layer of surfactant dioctadecyldithiophosph ate(DDP).The formation and constituent of the as-prepared nanoalloy were charac terized by transmission electron microscopy (TEM), high resolution transmission electron microscopy (HRTEM), X-ray diffraction (XRD), differential thermal anal ysis and thermogravimetry (DTA-TG), and Fourier transform infrared (FT-IR) spe ctrophotometer.It was also found that the powder showed excellent antiwear prope rty by tribological test results.展开更多
Three oxide-dispersion-strengthened(ODS)steels with compositions of Fe-14Cr-2W-0.2V-0.07Ta-0.3Y_2O_3(wt%,so as the follows)(14Y),Fe-14Cr-2W-0.2V-0.07Ta-1Al-0.3Y_2O_3(14YAl),and Fe-14Cr-2W-0.2V-0.07Ta-0.3Ti-0.3 Y_2O_3(...Three oxide-dispersion-strengthened(ODS)steels with compositions of Fe-14Cr-2W-0.2V-0.07Ta-0.3Y_2O_3(wt%,so as the follows)(14Y),Fe-14Cr-2W-0.2V-0.07Ta-1Al-0.3Y_2O_3(14YAl),and Fe-14Cr-2W-0.2V-0.07Ta-0.3Ti-0.3 Y_2O_3(14YTi)were fabricated by hot pressing.Transmission electron microscopy(TEM)was used to characterize the microstructures and nanoparticles of these ODS steels.According to the TEM results,14Y,14YAl,and 14YTi ODS steels present similar bimodal structures containing both large and small grains.The addition of Al or Ti has no obvious effect on the microstructure of the steels.The spatial and size distribution of the nanoparticles was also analyzed.The results indicate that the average size of nanoparticles in the 14YTi ODS steel is smaller than that in the 14YAl ODS steel.Nanoparticles such as Y_2O_3,Y_3Al_5O_(12) and YAlO_3,and Y_2Ti_2O_7 were identified in the 14Y,14YAl,and 14YTiODS steels,respectively.展开更多
文摘Ternary Pb-Sn-Cd alloy nanoparticles were prepared b y the sonochemical dispersion method. The nanoparticles were found to be about 40 —60 nm and coated with an amorphous layer of surfactant dioctadecyldithiophosph ate(DDP).The formation and constituent of the as-prepared nanoalloy were charac terized by transmission electron microscopy (TEM), high resolution transmission electron microscopy (HRTEM), X-ray diffraction (XRD), differential thermal anal ysis and thermogravimetry (DTA-TG), and Fourier transform infrared (FT-IR) spe ctrophotometer.It was also found that the powder showed excellent antiwear prope rty by tribological test results.
基金financially supported by the National Natural Science Foundation of China(Nos.51474156 and U1660201)the National Magnetic Confinement Fusion Energy Research Project(No.2015GB119000)
文摘Three oxide-dispersion-strengthened(ODS)steels with compositions of Fe-14Cr-2W-0.2V-0.07Ta-0.3Y_2O_3(wt%,so as the follows)(14Y),Fe-14Cr-2W-0.2V-0.07Ta-1Al-0.3Y_2O_3(14YAl),and Fe-14Cr-2W-0.2V-0.07Ta-0.3Ti-0.3 Y_2O_3(14YTi)were fabricated by hot pressing.Transmission electron microscopy(TEM)was used to characterize the microstructures and nanoparticles of these ODS steels.According to the TEM results,14Y,14YAl,and 14YTi ODS steels present similar bimodal structures containing both large and small grains.The addition of Al or Ti has no obvious effect on the microstructure of the steels.The spatial and size distribution of the nanoparticles was also analyzed.The results indicate that the average size of nanoparticles in the 14YTi ODS steel is smaller than that in the 14YAl ODS steel.Nanoparticles such as Y_2O_3,Y_3Al_5O_(12) and YAlO_3,and Y_2Ti_2O_7 were identified in the 14Y,14YAl,and 14YTiODS steels,respectively.
