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Preparation of V-Ti-Fe master alloys by metallothermic reduction method 被引量:5
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作者 王斌 刘奎仁 +2 位作者 陈建设 高腾跃 何季麟 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2012年第6期1507-1512,共6页
V-Ti-Fe master alloys were prepared by metaUothermic reduction method, and the influences of the mass ratio of V205 to TiO2, Al and Al-Mg alloy addition amounts on the metal recovery rates and alloy compositions were ... V-Ti-Fe master alloys were prepared by metaUothermic reduction method, and the influences of the mass ratio of V205 to TiO2, Al and Al-Mg alloy addition amounts on the metal recovery rates and alloy compositions were investigated. The results show that appropriate technological parameters are: the mass ratio of V205 to TiO2 is 0.5:1, Al addition represents 95% of the theoretical value, and the Al-Mg alloy addition amount is one third that of the Al addition. The results from energy spectrum analysis show that V and Fe distribute uniformly in the prepared alloy, while the segregation for Ti, i.e. Ti-rich phase is detected. A spray refming process was carried out to reduce the impurity contents of Al and O in the prepared alloys. The Al content drops from 4.27% to 1.86%, and the O content drops from 2.10% to 0.91% after the refining process. 展开更多
关键词 v-ti-fe master alloys metallothermic reduction method recovery rates refining process
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V-Ti-Fe中间合金的精炼工艺 被引量:1
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作者 王斌 刘奎仁 +1 位作者 高腾跃 何季麟 《东北大学学报(自然科学版)》 EI CAS CSCD 北大核心 2012年第5期689-693,共5页
以金属热还原法制备的V-Ti-Fe中间合金为原料,采用喷吹造渣的方式对其进行精炼研究,实验考察了渣系组成和精炼温度对精炼效果的影响.结果表明:渣体中m(CaF2)/m(CaO)值为3.0,TiO2用量为总渣量的10%,用渣量为合金用量的35%,精炼温度为1 60... 以金属热还原法制备的V-Ti-Fe中间合金为原料,采用喷吹造渣的方式对其进行精炼研究,实验考察了渣系组成和精炼温度对精炼效果的影响.结果表明:渣体中m(CaF2)/m(CaO)值为3.0,TiO2用量为总渣量的10%,用渣量为合金用量的35%,精炼温度为1 600℃时,精炼效果较好;精炼后合金中的Al质量分数由7.11%降到了2.61%,合金中的Si质量分数变化较小,仅由1.25%降到了0.97%.XRD和SEM分析表明,精炼后合金中没有出现氧化物相,精炼有效地去除了合金中的氧化物夹杂,降低了合金的成分偏析. 展开更多
关键词 v-ti-fe中间合金 精炼 CaO-CaF2渣系 吹氩 氧化物夹杂
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