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A Pioneering Approach to the Synthesis of Silver Nanoparticles
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作者 Wasan A. Al-Dulaimi Zeena M. Al-Azzawi Emad K. Al-Shakarchi 《Journal of Materials Science and Chemical Engineering》 2024年第7期14-22,共9页
Our research introduces a groundbreaking chemical reduction method for synthesizing silver nanoparticles, marking a significant advancement in the field. The nanoparticles were meticulously characterized using various... Our research introduces a groundbreaking chemical reduction method for synthesizing silver nanoparticles, marking a significant advancement in the field. The nanoparticles were meticulously characterized using various techniques, including optical analysis, structural analysis, transmission electron microscopy (TEM), and field-emission scanning electron microscope (FESEM). This thorough process instills confidence in the accuracy of our findings. The results unveiled that the silver nanoparticles had a diameter of less than 20 nm, a finding of great importance. The absorption spectrum decreased in the peak wavelength range (405 - 394 mm) with increasing concentrations of Ag nanoparticles in the range (1 - 5%). The XRD results indicated a cubic crystal structure for silver nanoparticles with the lattice constant (a = 4.0855 Å), and Miller indices were (111), (002), (002), and (113). The simulation on the XRD pattern showed a face center cubic phase with space group Fm-3m, providing valuable insights into the structure of the nanoparticles. 展开更多
关键词 Chemical Reduction Method uv-vis absorption spectrometer Field-Emission Scanning Electron Microscope (FESEM) Transmission Electron Microscopy (TEM)
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The Preparation of Nano Silver by Chemical Reduction Method 被引量:1
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作者 Tevfik Raci Sertbakan Emad K. Al-Shakarchi Saif Sultan Mala 《Journal of Modern Physics》 2022年第1期81-88,共8页
A silver nanostructures prepared by using chemical reduction method. The silver nanoparticles were prepared with diameters of about (20 nm). Numerous techniques had been used to study the optical, structural like the ... A silver nanostructures prepared by using chemical reduction method. The silver nanoparticles were prepared with diameters of about (20 nm). Numerous techniques had been used to study the optical, structural like the UV-Vis absorption spectrometer, Ttransmission Electron Microscopy (TEM), Field-Emission Scanning Electron microscope (FESEM), and X-ray diffraction (XRD). The practical results exhibited the absorption spectrum of the prepared nanoparticles at (357 nm), it was found that there is a relationship between the positions of the optical absorption peak and the size of the silver nanoparticles. The analysis of TEM results showed the presence of nanoparticles in the range (20 nm). The analyzing of XRD results explained the crystal structure for silver nanoparticles. It is found a cubic unit cell have a lattice constants (a = 4.0855 <span style="white-space:nowrap;">&Aring;</span>), with the Miller indices were (111), (002), (002), and (113). 展开更多
关键词 Chemical Reduction Method uv-vis absorption spectrometer Field-Emission Scanning Electron Microscope Ttransmission Electron Microscopy
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天然与处理翡翠的光谱学研究 被引量:19
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作者 范建良 郭守国 +1 位作者 刘学良 王以群 《激光与红外》 CAS CSCD 北大核心 2007年第8期769-772,共4页
文章通过对天然翡翠和漂白充填处理翡翠的共焦显微拉曼光谱(514nm)测定,得到表征翡翠硬玉结构的拉曼位移为1036cm-1,696cm-1和374cm-1,显微放大能观察到翡翠经酸洗产生的裂纹及其充填的有机物,经红外光谱的测定证实该充填物为环氧树脂,... 文章通过对天然翡翠和漂白充填处理翡翠的共焦显微拉曼光谱(514nm)测定,得到表征翡翠硬玉结构的拉曼位移为1036cm-1,696cm-1和374cm-1,显微放大能观察到翡翠经酸洗产生的裂纹及其充填的有机物,经红外光谱的测定证实该充填物为环氧树脂,且表征环氧树脂的拉曼峰为777cm-1,1123cm-1,1611cm-1,2930cm-1和3065cm-1;通过相同测试条件下,并在极短的积分时间内对天然翡翠的绿色、白色部位和染绿色翡翠进行拉曼光谱(785nm)测定,并结合绿色翡翠紫外-可见光-近红外吸收光谱的测定,得到吸收光谱中的吸收峰637nm,658nm和691nm归属于翡翠晶体中的Cr3+,Cr3+的大量存在将使翡翠的拉曼光谱产生极强的荧光,而染色翡翠中染料产生的荧光相对较弱。 展开更多
关键词 翡翠 拉曼光谱 红外光谱 紫外-可见光-近红外吸收光谱
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