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用多层次模糊综合评判法确定单层剩余油分布 被引量:25
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作者 杜庆龙 计秉玉 +2 位作者 王元庆 杨会东 朱丽红 《石油学报》 EI CAS CSCD 北大核心 2003年第2期57-60,共4页
针对非均质多层砂岩油田高含水后期的剩余油分布高度零散、影响因素多、识别难度大等问题 ,在对影响剩余油分布的地质及开发因素综合分析的基础上 ,结合不同研究区块的动静态资料情况 ,提出了利用多层次模糊综合评判法识别单层剩余油分... 针对非均质多层砂岩油田高含水后期的剩余油分布高度零散、影响因素多、识别难度大等问题 ,在对影响剩余油分布的地质及开发因素综合分析的基础上 ,结合不同研究区块的动静态资料情况 ,提出了利用多层次模糊综合评判法识别单层剩余油分布的有效方法 ,并在大庆油田高含水后期三次加密试验区剩余油研究中得到成功的应用。经新钻检查井资料检验 ,单层剩余油识别符合率为 81 4% ,为非均质多层砂岩油田单层剩余油分布研究提供了新的方法。 展开更多
关键词 多层砂岩油田 模糊综合评判法 单层 剩余油分布 识别
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钎焊法制造金刚石单层工具的研究 被引量:17
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作者 林增栋 《金刚石与磨料磨具工程》 CAS 2004年第3期1-5,共5页
含强碳化物形成元素合金对金刚石表面浸润的机理与金刚石表面金属化技术是钎焊制造单层金刚石工具的技术基础。由于金刚石颗粒被强力焊接及其出刃突出 ,并可有序排布决定了钎焊单层金刚石工具具有磨削效率高、工具寿命长的基本特点。本... 含强碳化物形成元素合金对金刚石表面浸润的机理与金刚石表面金属化技术是钎焊制造单层金刚石工具的技术基础。由于金刚石颗粒被强力焊接及其出刃突出 ,并可有序排布决定了钎焊单层金刚石工具具有磨削效率高、工具寿命长的基本特点。本文以三种金刚石工具为例 ,详细介绍了钎焊法制造金刚石工具的工艺。并与电镀金刚石工具进行了对比。 展开更多
关键词 金刚石工具 钎焊 单层 出刃
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单层雷达吸波材料研究 被引量:15
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作者 周永江 程海峰 +2 位作者 曹义 陈朝辉 才鸿年 《材料工程》 EI CAS CSCD 北大核心 2006年第4期8-11,共4页
通过数值分析确定了单层电损耗吸波材料理想电磁参数,探讨了单层吸波材料的吸波机理。分析表明:单层吸波材料要实现宽频吸收,其电磁参数必须具有频散效应,即随电磁波频率的升高电磁参数有规律的降低,其中ε′.μ′与f2成反比。以羰基铁... 通过数值分析确定了单层电损耗吸波材料理想电磁参数,探讨了单层吸波材料的吸波机理。分析表明:单层吸波材料要实现宽频吸收,其电磁参数必须具有频散效应,即随电磁波频率的升高电磁参数有规律的降低,其中ε′.μ′与f2成反比。以羰基铁粉/聚氯乙烯吸波贴片为实例验证了理论分析结果,讨论了常规单层吸波材料性能的影响因素。 展开更多
关键词 单层 宽频带 雷达吸波材料 吸波机理
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Research on failure scenarios of domes based on form vulnerability 被引量:15
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作者 YE JiHong LIU WenZheng PAN Rui 《Science China(Technological Sciences)》 SCIE EI CAS 2011年第11期2834-2853,共20页
In this paper, form vulnerability theory was applied to the analysis of the failure mechanisms of single-layer latticed spherical shells subjected to seismic excitations. Three 1/10 scale testing models were designed ... In this paper, form vulnerability theory was applied to the analysis of the failure mechanisms of single-layer latticed spherical shells subjected to seismic excitations. Three 1/10 scale testing models were designed with characteristics as follows: Model 1 possesses overall uniform stiffness and is expected to collapse in the strength failure mode as some members become plastic; Model 2 possesses six man-made weak parts located on six radial main rib zones and is expected to collapse in the dynamic in- stability mode with all members still in the elastic stage; Model 3 strengthens the six weak zones of Model 2, and therefore, its stiffness is uniform. Model 3 is proposed to collapse in the strength failure mode when the members are still in the elastic stage By increasing the peak ground accelerations of seismic waves gradually, the shaking table tests were carried out until all three models collapsed (or locally collapsed). On the basis of form vulnerability theory, topological hierarchy models of the test models were established through a clustering process, and various failure scenarios, including overall collapse scenarios and partial collapse scenarios, were identified by unzipping corresponding hierarchical models. By comparison of the failure scenarios based on theoretical analysis and experiments, it was found that vulnerability theory could effectively reflect the weak- ness zones in topological relations of the structures from the perspective of internal causes. The intemal mechanisms of the distinct failure characteristics of reticulated shells subjected to seismic excitations were also revealed in this process. The well-formedness of structural clusters, Q, is closely related to the collapse modes, i.e., uniform changes of Q indicate a uniform distribution of overall structural stiffness, which indicates that strength failure is likely to happen; conversely, non-uniform changes of Q indicate that weak zones exist in the structure, and dynamic instability is likely to occur. 展开更多
关键词 single-layer latticed spherical shell form vulnerabifity collapse mode failure mechanism shaking table test
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Comparative investigation on high-speed grinding of TiCp/Ti–6Al–4V particulate reinforced titanium matrix composites with single-layer electroplated and brazed CBN wheels 被引量:11
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作者 Li Zheng Ding Wenfeng +2 位作者 Shen Long Xi Xinxin Fu Yucan 《Chinese Journal of Aeronautics》 SCIE EI CAS CSCD 2016年第5期1414-1424,共11页
In order to develop the high-efficiency and precision machining technique of TiCp/Ti - 6Al-4V particulate reinforced titanium matrix composites (PTMCs), high-speed grinding experiments were conducted using the singl... In order to develop the high-efficiency and precision machining technique of TiCp/Ti - 6Al-4V particulate reinforced titanium matrix composites (PTMCs), high-speed grinding experiments were conducted using the single-layer electroplated cubic boron nitride (CBN) wheel and brazed CBN wheel, respectively. The comparative grinding performance was studied in terms of grinding force, grinding temperature, grinding-induced surface features and defects. The results display that the grinding forces and grinding temperature obtained with the brazed CBN wheel are always lower than those with the electroplated CBN wheel. Though the voids and microcracks are the dominant grinding-induced surface defects, the brazed CBN wheel produces less surface defects compared to the electroplated wheel according to the statistical analysis results. The max mum materials removal rate with the brazed CBN wheel is much higher than that with the electroplated one. All above indicate that the single-layer brazed CBN super-abrasive wheel is more suitable for high-speed grinding of PTMCs than the electroplated counterpart. 展开更多
关键词 High-speed grinding PTMCs single-layer brazed CBNwheel single-layer electroplated CBN wheel Surface defects
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Single-cell transcriptome atlas of the leaf and root of rice seedlings 被引量:13
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作者 Yu Wang Qing Huan +1 位作者 Ke Li Wenfeng Qian 《Journal of Genetics and Genomics》 SCIE CAS CSCD 2021年第10期881-898,共18页
As a multicellular organism,rice flourishes relying on gene expression diversity among cells of various functions.However,cellular-resolution transcriptome features are yet to be fully recognized,let alone cell-specif... As a multicellular organism,rice flourishes relying on gene expression diversity among cells of various functions.However,cellular-resolution transcriptome features are yet to be fully recognized,let alone cell-specific transcriptional responses to environmental stimuli.In this study,we apply single-cell RNA sequencing to both shoot and root of rice seedlings growing in Kimura B nutrient solution or exposed to various abiotic stresses and characterize transcriptomes for a total of 237,431 individual cells.We identify 15 and 9 cell types in the leaf and root,respectively,and observe that common transcriptome features are often shared between leaves and roots in the same tissue layer,except for endodermis or epidermis.Abiotic stress stimuli alter gene expression largely in a cell type-specific manner,but for a given cell type,different stresses often trigger transcriptional regulation of roughly the same set of genes.Besides,we detect proportional changes in cell populations in response to abiotic stress and investigate the underlying molecular mechanisms through single-cell reconstruction of the developmental trajectory.Collectively,our study represents a benchmark-setting data resource of single-cell transcriptome atlas for rice seedlings and an illustration of exploiting such resources to drive discoveries in plant biology. 展开更多
关键词 single-cell RNA-seq Rice seedling Cell-to-cell heterogeneity Plant tissue layer Developmental trajectory Abiotic stress
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Single atom catalyst by atomic layer deposition technique 被引量:13
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作者 Niancai Cheng Xueliang(Andy) Sun 《Chinese Journal of Catalysis》 CSCD 北大核心 2017年第9期1508-1514,共7页
Noble single‐atom catalysts have rapidly been attracting attention due to their unique catalytic properties and maximized utilization.Atomic layer deposition(ALD)is an emerging powerful technique for large‐scale syn... Noble single‐atom catalysts have rapidly been attracting attention due to their unique catalytic properties and maximized utilization.Atomic layer deposition(ALD)is an emerging powerful technique for large‐scale synthesis of stable single atom.In this review,we summarize recent developments of single atom synthesized by ALD as well as explore future research direction and trends. 展开更多
关键词 single‐atom Atomic layer deposition CATALYSIS Noble catalyst MECHANISM
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掺杂TBPe的单一发光层白色OLEDs研究 被引量:12
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作者 牛霞 华玉林 +5 位作者 吴空物 朱飞剑 吴晓明 印寿根 邓家春 刘嵩 《光电子.激光》 EI CAS CSCD 北大核心 2006年第5期522-525,共4页
以聚合物poly(N-vinylcarbazole)(PVK)为主体材料,分别掺入蓝光染料2,5,8,11-tetra-tertbu-tylperylene(TBPe)和橙黄光染料5,6,11,12-tetraphenyl-naphthacene(Rubrebe),制成单层白色有机电致发光器件(WOLED)。通过多组实验结果的对比,... 以聚合物poly(N-vinylcarbazole)(PVK)为主体材料,分别掺入蓝光染料2,5,8,11-tetra-tertbu-tylperylene(TBPe)和橙黄光染料5,6,11,12-tetraphenyl-naphthacene(Rubrebe),制成单层白色有机电致发光器件(WOLED)。通过多组实验结果的对比,最终确定了最佳染料掺杂浓度和器件结构,得到最佳色坐标为(0.33,0.38),已位于该坐标的白色等能区之内,且随着外加电压由8 V增加到16 V,色坐标保持不变。器件的亮度为553 cd/m2,外量子效率为0.16%。 展开更多
关键词 白光 单层 有机电致发光器件(OLED) TBPe
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电渣型单层带极堆焊技术开发 被引量:8
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作者 胡希海 李瑛琦 +1 位作者 曹明 邓刚 《压力容器》 2004年第8期5-7,48,共4页
针对设计院对高压分离器采用不锈钢单层堆焊要求 ,研究开发了单层堆焊技术 ,较好地解决了生产需求 ,创造了效益。
关键词 电渣型 单层 带极堆焊 高压分离器 不锈钢 加氢设备
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二维层状六方氮化硼在芯片散热中的应用 被引量:10
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作者 鲍婕 张勇 +4 位作者 黄时荣 孙双希 路秀真 符益凤 刘建影 《应用基础与工程科学学报》 EI CSCD 北大核心 2016年第1期210-217,共8页
层状六方氮化硼(h-BN)作为典型的二维材料之一,近年来由于其优良的物理化学特性受到广泛关注,本文利用其横向热导率高、绝缘性能好的特点,将其用于功率芯片表面,作为帮助芯片上局部高热流热点横向散热的绝缘保护层.分别将化学气相沉积... 层状六方氮化硼(h-BN)作为典型的二维材料之一,近年来由于其优良的物理化学特性受到广泛关注,本文利用其横向热导率高、绝缘性能好的特点,将其用于功率芯片表面,作为帮助芯片上局部高热流热点横向散热的绝缘保护层.分别将化学气相沉积法制备的单层h-BN薄膜和微米级h-BN颗粒转移到热测试芯片表面,通过加载不同功率,观察h-BN对芯片散热性能的影响.采用电阻-温度曲线法和红外热像仪两种方法对热测试芯片的热点温度进行检测.研究结果表明,h-BN应用到热测试芯片表面,在加载功率约为1W时,可以将芯片热点温度降低3~5℃,从而提高芯片散热效率,并且通过对比发现单层h-BN薄膜表现出更为理想的散热效果. 展开更多
关键词 氮化硼 热测试芯片 单层 散热
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一种新型单层单贴片宽带圆形微带天线 被引量:9
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作者 丁毅 王光明 苏文然 《弹箭与制导学报》 CSCD 北大核心 2007年第5期274-276,共3页
设计了一种新型单贴片单层的开缝微带天线。天线开缝后产生了两个相近的谐振点,通过对缝隙的调整,使得两个谐振点之间的S11<-10dB。带宽因此也得到了比较大的提高。仿真与实测结果表明,该新型天线工作于2.64GHz时,带宽达到了10%(S11&... 设计了一种新型单贴片单层的开缝微带天线。天线开缝后产生了两个相近的谐振点,通过对缝隙的调整,使得两个谐振点之间的S11<-10dB。带宽因此也得到了比较大的提高。仿真与实测结果表明,该新型天线工作于2.64GHz时,带宽达到了10%(S11<-10dB)。由于此种方法对天线的整体结构没有改变,并且只采用了传统的同轴馈电。因此制作成本低,结构简单,同时还保证了天线的低剖面性。 展开更多
关键词 单层 单贴片 缝隙 宽带
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WC/Co单层与多层过渡熔覆层激光熔覆的热应力有限元分析 被引量:5
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作者 陈泽民 廖丕博 曾凯 《昆明理工大学学报(理工版)》 2007年第2期17-20,共4页
在建立WC/Co多层过渡涂层与单层涂层模型的基础上,对两种涂层结构分别选定了两条具有代表性的路径.借助有限元分析软件对高温下涂层和基体的应力分布进行了模拟,并提取两种结构对应路径上的应力进行对比分析.结果表明,在界面和涂层厚度... 在建立WC/Co多层过渡涂层与单层涂层模型的基础上,对两种涂层结构分别选定了两条具有代表性的路径.借助有限元分析软件对高温下涂层和基体的应力分布进行了模拟,并提取两种结构对应路径上的应力进行对比分析.结果表明,在界面和涂层厚度方向,多层过渡涂层的热应力总体上小于单层涂层的热应力,其分布更加平缓. 展开更多
关键词 热应力 多层过渡涂层 单层涂层 WC/Co涂层 激光熔覆
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Enhanced NO_2 gas sensing of a single-layer MoS_2 by photogating and piezo-phototronic effects 被引量:7
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作者 Junmeng Guo Rongmei Wen +1 位作者 Junyi Zhai Zhong Lin Wang 《Science Bulletin》 SCIE EI CSCD 2019年第2期128-135,共8页
NO_2 sensors with ultrahigh sensitivity are demanded for future electronic sensing systems. However,traditional sensors are considerably limited by the relative low sensitivity, high cost and complicated process. Here... NO_2 sensors with ultrahigh sensitivity are demanded for future electronic sensing systems. However,traditional sensors are considerably limited by the relative low sensitivity, high cost and complicated process. Here, we report a simply and reliable flexible NO_2 sensor based on single-layer MoS_2. The flexible sensor exhibits high sensitivity to NO_2 gas due to ultra-large specific surface area and the nature of two-dimensional(2 D) semiconductor. When the NO_2 is 400 ppb(parts per billion), compared with the dark and strain-free conditions, the sensitivity of the single-layer sensor is enhanced to 671% with a625 nm red light-emitting diode(LED) illumination of 4 mW/cm^2 power under 0.67% tensile strain.More important, the response time is dramatically reduced to $16 s and it only needs $65 s to complete90% recovery. A theoretical model is proposed to discuss the microscopic mechanisms. We find that the remarkable sensing characteristics are the result of coupling among piezoelectricity, photoelectricity and adsorption-desorption induced charges transfer in the single-layer MoS_2 Schottky junction based device.Our work opens up the way to further enhancements in the sensitivity of gas sensor based on single-layer MoS_2 by introducing photogating and piezo-phototronic effects in mesoscopic systems. 展开更多
关键词 Ultrahigh sensitivity FLEXIBLE NO2 SENSOR single-layer MOS2 Photogating EFFECT Piezo-phototronic EFFECT
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SnO_2 hollow nanospheres assembled by single layer nanocrystals as anode material for high performance Li ion batteries 被引量:7
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作者 Wei Wei Ling-Xiao Song Lin Guo 《Chinese Chemical Letters》 SCIE CAS CSCD 2015年第1期124-128,共5页
SnO2 hollow nanospheres were successfully synthesized via a facile one-step solvothermal method.Characterizations show that the as-prepared SnO2 spheres are of hollow structure with a diameter at around 50 nm,and espe... SnO2 hollow nanospheres were successfully synthesized via a facile one-step solvothermal method.Characterizations show that the as-prepared SnO2 spheres are of hollow structure with a diameter at around 50 nm,and especially,the shell of the spheres is assembled by single layer SnO2 nanocrystals.The surface area of the material reaches up to 202.5 m^2/g.As an anode material for Li ion batteries,the sample exhibited improved electrochemical performance compared with commercial SnO2 particles.After cycled at high current rate of 0.5 C,1 C and 0.5 C for 20 cycles,respectively,the electrode can maintain a capacity of 509 mAh/g.The suitable shell thickness/diameter ratio endows the good structural stability of the material during cycling,which promises the excellent cycling performance of the electrode.The large surface area and the ultra thin shell ensure the high rate performance of the material. 展开更多
关键词 SNO2 Hollow nanospheres single layer Li ion batteries
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单层圆筒容器爆破压力的概率分布 被引量:8
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作者 刘岑 杨帆 +3 位作者 刘兵 袁小会 张红卫 刘小宁 《机械强度》 CAS CSCD 北大核心 2020年第2期365-373,共9页
研究单层圆筒容器爆破压力的概率分布,是建立压力容器的可靠性设计方法和构建压力容器强度计算公式精度评价体系的一项基础工作。基于84组单层圆筒容器的实测爆破压力,应用数理统计理论的假设检验方法,对单层圆筒容器爆破压力的概率分... 研究单层圆筒容器爆破压力的概率分布,是建立压力容器的可靠性设计方法和构建压力容器强度计算公式精度评价体系的一项基础工作。基于84组单层圆筒容器的实测爆破压力,应用数理统计理论的假设检验方法,对单层圆筒容器爆破压力的概率分布进行了分析。研究表明:(1)根据中国标准的工程实践,按设计压力可将容器爆破压力计算公式的应用范围划分为3个总体:设计压力不超过35 MPa,位于35 MPa^100 MPa之间,以及不超过100 MPa。(2)根据设计压力与爆破压力的关系,公式应用范围样本的实测爆破压力为:不超过105.5 MPa,位于91.0 MPa^329.6 MPa之间,以及不超过329.6 MPa。(3)显著度为0.05时,样本实测爆破压力与中径公式和Tresca公式计算值之比,是6个符合正态分布的随机变量。(4)在双侧置信度为98%时,分别得到6个随机变量分布参数的取值范围。 展开更多
关键词 单层 圆筒容器 爆破压力 概率分布 总体 样本
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Shaking table test and numerical simulation of an isolated cylindrical latticed shell under multiple-support excitations 被引量:6
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作者 Xue Suduo Shan Mingyue +3 位作者 Li Xiongyan Liang Shuanzhu Huang Fuyun Liu Yi 《Earthquake Engineering and Engineering Vibration》 SCIE EI CSCD 2019年第3期611-630,共20页
In order to study the infl uence of the ground motion spatial eff ect on the seismic response of large span spatial structures with isolation bearings, a single-layer cylindrical latticed shell scale model with a simi... In order to study the infl uence of the ground motion spatial eff ect on the seismic response of large span spatial structures with isolation bearings, a single-layer cylindrical latticed shell scale model with a similarity ratio of 1/10 was constructed. An earthquake simulation shaking table test on the response under multiple-support excitations was performed with the high-position seismic isolation method using high damping rubber (HDR) bearings. Small-amplitude sinusoidal waves and seismic wave records with various spectral characteristics were applied to the model. The dynamic characteristics of the model and the seismic isolation eff ect on it were analyzed at varying apparent wave velocities, namely infi nitely great, 1000 m/s, 500 m/s and 250 m/s. Besides, numerical simulations were carried out by Matlab software. According to the comparison results, the numerical results agreed well with the experimental data. Moreover, the results showed that the latticed shell roof exhibited a translational motion as a rigid body after the installation of the HDR bearings with a much lower natural frequency, higher damping ratio and only 1/2~1/8 of the acceleration response peak values. Meanwhile, the structural responses and the bearing deformations at the output end of the seismic waves were greatly increased under multiple-support excitations. 展开更多
关键词 single-layer CYLINDRICAL latticed shell HDR bearings seismic isolation multiple-support EXCITATIONS SHAKING table test
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Effect of Single- versus Double-Layer Uterine Closure during Caesarean Section on Niche Formation and Menstrual Irregularity
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作者 Mohamed Samy Esraa Hussein Fouad Ghoneimy Walid Hitler 《Open Journal of Obstetrics and Gynecology》 2024年第1期57-68,共12页
Background: The myometrium at the location of the CS (caesarean section) scars, also known as residual myometrium thickness (RMT), is larger after a double-layer uterine closure procedure than following a single-layer... Background: The myometrium at the location of the CS (caesarean section) scars, also known as residual myometrium thickness (RMT), is larger after a double-layer uterine closure procedure than following a single-layer one. It may lessen the formation of a niche that is the myometrium’s disruption at the location of the scar of the uterus. Gynecological manifestations, obstetric problems in a future pregnancy and birth, and maybe subfertility are linked to thin RMT and a niche. Objective: To ascertain if double-layer unlocked closure of the uterus is better than single-layer one in terms of post-menstrual spotting and niche development following a first CS. Patients and Methods: In this randomized clinical study, 287 patients were evaluated for qualifying. Of all eligible individuals, 57 patients were excluded from the study based on the inclusion criteria. Results: The variation in ages, gestational age, body mass index (BMI), and cesarean section indications between the two assigned groups is statistically insignificant. However, postmenstrual spotting was statistically significantly more common in single-layer group compared to in double-group. The current study revealed ultrasound findings suggestive of niche formation was statistically significantly more common in single-layer group compared to in double-layer group. Conclusion: As evident from the current study, it demonstrates the advantages of double-layer unlocked closure of the uterus over single-layer one in terms of post-menstrual spotting and niche development following first-time cs. Thus, we deduced that fewer niches are formed, and fewer menstrual spotting occurs in the presence of double unlocked layers closure. To ascertain the impact of uterus closure method on post-operative niche development and the risk of obstetrics and gynaecological problems, further prospective trials with extended follow-up periods are required. 展开更多
关键词 single-layer Double Caesarean Section Residual Myometrium Thickness
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南通体育场开合式钢屋盖结构整体稳定分析研究 被引量:6
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作者 江晓峰 陈以一 +1 位作者 刘魁 陈扬骥 《建筑结构》 CSCD 北大核心 2008年第9期20-23,46,共5页
2006年建成并运营的江苏省南通市体育会展中心主体育场是我国第一个应用于大跨公共建筑的开合式结构。对该结构的设计研究表明,开合式结构稳定性分析应考虑活动屋盖处于不同位置时几何状态与荷载分布的变化,且应准确模拟活动部分和固定... 2006年建成并运营的江苏省南通市体育会展中心主体育场是我国第一个应用于大跨公共建筑的开合式结构。对该结构的设计研究表明,开合式结构稳定性分析应考虑活动屋盖处于不同位置时几何状态与荷载分布的变化,且应准确模拟活动部分和固定部分之间的约束条件。数值分析表明,在设计荷载作用下,南通体育场开合式结构具有足够的整体稳定性。 展开更多
关键词 开合式结构 稳定分析 单层网壳 拱支网壳 南通体育场
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对储层单元分级方案的探讨 被引量:6
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作者 束青林 《油气地质与采收率》 CAS CSCD 北大核心 2006年第1期11-13,共3页
高精度的地层格架是油田开发小尺度流动单元的必要条件。鉴于目前在储层单元划分上术语使用多而乱的现状,应当建立储层单元术语系统,建议使用含油层系、油层组、砂层组、小层、单砂层等术语,以便于成果的交流与比较。储层单元分级是一... 高精度的地层格架是油田开发小尺度流动单元的必要条件。鉴于目前在储层单元划分上术语使用多而乱的现状,应当建立储层单元术语系统,建议使用含油层系、油层组、砂层组、小层、单砂层等术语,以便于成果的交流与比较。储层单元分级是一个涉及多学科多领域的问题。高分辨率地层学和储层建筑结构研究处于储层地质学研究的前沿,以这2个学科的划分意见为基础提出了新的储层单元分级方案,即巨旋回级、超长旋回级、长期旋回级、中期旋回级、短期旋回级、超短期旋回级、复合成因砂体级、单一成因砂体级、纹层组系级、纹层组级和纹层级。 展开更多
关键词 储层单元 旋回 油层组 砂层组 单砂层
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过渡金属碳化物Ti_(3)C_(2)T_(x)的制备及其电磁屏蔽性能研究 被引量:3
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作者 李俊 徐丽慧 +5 位作者 卢光明 潘虹 沈勇 王黎明 徐天阳 蔡央芳 《功能材料》 CAS CSCD 北大核心 2023年第1期1097-1103,共7页
二维过渡金属碳化物(MXene)具有优异的导电性、良好的柔韧性和亲水性等特点,其中Ti_(3)C_(2)T_(x)在电磁波屏蔽领域研究广泛。Ti_(3)C_(2)T_(x)是通过选择性刻蚀MAX相Ti 3AlC 2中Al元素后进一步剥离得到,因此刻蚀和剥离工艺直接决定了Ti... 二维过渡金属碳化物(MXene)具有优异的导电性、良好的柔韧性和亲水性等特点,其中Ti_(3)C_(2)T_(x)在电磁波屏蔽领域研究广泛。Ti_(3)C_(2)T_(x)是通过选择性刻蚀MAX相Ti 3AlC 2中Al元素后进一步剥离得到,因此刻蚀和剥离工艺直接决定了Ti_(3)C_(2)T_(x)的物化性质。采用LiF/HCl选择性刻蚀前驱体Ti 3AlC 2,优化刻蚀时间和剥离时间,制备了单/少层Ti_(3)C_(2)T_(x)。通过X射线衍射(XRD)、拉曼光谱(Raman)、X射线光电子能谱(XPS)和扫描电镜(SEM)等对Ti_(3)C_(2)T_(x)表面形貌、化学组成进行表征,并通过矢量网络分析仪(VNA)和四探针测试仪等研究了Ti_(3)C_(2)T_(x)的电磁屏蔽效能及导电性能。结果表明,采用LiF/HCl选择性刻蚀法能够有效制备单/少层Ti_(3)C_(2)T_(x),在刻蚀时间为48 h,超声剥离时间为50 min时,获得的Ti_(3)C_(2)T_(x)薄膜电磁屏蔽性能最高达到52.5 dB,电导率可达7342.1 S/m。同时,Ti_(3)C_(2)T_(x)自支撑薄膜在低厚度下绝对屏蔽效能达18347.65 dB cm^(2)g^(-1),表现出优异的电磁屏蔽性能。 展开更多
关键词 二维过渡金属碳化物 电磁屏蔽 导电 单层
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