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Al_2O_3-ZrO_2(3Y)-SiC纳米复合材料的制备及性能 被引量:20
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作者 王宏志 高濂 +1 位作者 归林华 郭景坤 《无机材料学报》 SCIE EI CAS CSCD 北大核心 1999年第2期280-286,共7页
本文研究了非均相沉淀法制备Al2O3-ZrO2(3Y)-SiC复合粉体的工艺过程,认为粉体的理烧温度是至关重要的,热压烧结得到了致密的Al2O3-ZrO2(3Y)-SiC纳米复合材料,ZrO2的加入对烧结温度的影响不大.通过TEM观察,SiC颗粒均匀分散... 本文研究了非均相沉淀法制备Al2O3-ZrO2(3Y)-SiC复合粉体的工艺过程,认为粉体的理烧温度是至关重要的,热压烧结得到了致密的Al2O3-ZrO2(3Y)-SiC纳米复合材料,ZrO2的加入对烧结温度的影响不大.通过TEM观察,SiC颗粒均匀分散于材料中,大的ZrO2颗粒位于Al2O3晶粒间,小的圆形ZrO2颗粒位于Al2O3晶粒内,一部分Al2O3晶粒呈非等轴状.80Wt%Al2O3-15wt%ZrO2-5Wt%SiC纳米复合材料的抗弯强度可达555MPa,韧性为3.8MPa.m1/2. 展开更多
关键词 纳米复合材料 性能 复合材料 氧化物 碳化硅
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何首乌炮制后新产生成分含量分析 被引量:12
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作者 刘振丽 宋志前 +3 位作者 巢志茂 吕署一 王淳 李林福 《中国中药杂志》 CAS CSCD 北大核心 2008年第20期2326-2329,共4页
目的:分析何首乌炮制后新产生成分2,3-二氢-3,5-二羟基-6-甲基-4氢-吡喃4-酮(DDMP)和5-羟甲基糠醛(5-HMF)的含量随炮制时间的变化以及不同地区市售何首乌生品与炮制品中5-HMF含量。方法:采用HPLC测定,Zorbax C18色谱柱(3.9mm... 目的:分析何首乌炮制后新产生成分2,3-二氢-3,5-二羟基-6-甲基-4氢-吡喃4-酮(DDMP)和5-羟甲基糠醛(5-HMF)的含量随炮制时间的变化以及不同地区市售何首乌生品与炮制品中5-HMF含量。方法:采用HPLC测定,Zorbax C18色谱柱(3.9mm×150mm,5μm);流动相甲醇-水(10:90);检测波长280nm;柱温40℃。结果:在炮制的60h时间内,随炮制时间的延长DDMP的含量逐渐升高,至炮制24h达到最高,随后开始逐渐降低;5-HMF的含量随炮制时间的延长逐渐升高。11个批次制何首乌中5-HMF含量为0.013%~0.101%,4个批次何首乌中只有1个批次含有微量5-HMF。结论:炮制过程中内部成分处于动态变化,应严格控制和规范何首乌炮制工艺。 展开更多
关键词 何首乌 炮制 DDMP 5-HMF 含量测定
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气质联用研究麻黄及其炮制品中挥发油 被引量:6
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作者 曾诠 刘成基 +2 位作者 楼冠峰 郑丽真 江虹 《中国中药杂志》 CAS CSCD 北大核心 1992年第2期83-87,共5页
研究麻黄炮制前后挥发油含量及其油中化学成分的变化。结果表明:低沸点物质增多,含量也增高;高沸点物质减少,含量也降低。以炒黄麻黄变化尤为明显。
关键词 麻黄 挥发油 炮制
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Visualization of the Precessing Vortex Core in a Cyclone Separator by PIV 被引量:8
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作者 吴小林 时铭显 《Chinese Journal of Chemical Engineering》 SCIE EI CAS CSCD 2003年第6期633-637,共5页
The precessing vortex core (PVC) in a cyclone separator plays an important role in the separation performance and in further understanding of the general law of periodic unsteady flow therein. In this paper, the unste... The precessing vortex core (PVC) in a cyclone separator plays an important role in the separation performance and in further understanding of the general law of periodic unsteady flow therein. In this paper, the unsteady flow field is investigated with particle image velocimetry (PIV), and the instantaneous velocity, vorticity, tangential velocity, and radial velocity are acquired by analyzing the images of instantaneous flow. It is for the first time reported that there is a centrifugal flow region close to the dust discharge zone and its maximum value is higher than the mean radial velocity. This discovery is very important for understanding the principle of separation of particles in the area of dust discharge. Determination of the frequency and amplitude of PVC was conducted in the region where the phenomenon of PVC is remarkable. Results agree well with those obtained by hot wire anemometry. The observations of the center of vortex core and the bimodal distribution of the amplitude of the PVC indicate the vortex core precesses around the geometric axis of the cyclone in its own way. 展开更多
关键词 cyclone separator flow field instantaneous velocity precessing vortex core particle image velocimetry
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武昌鱼真空冷冻升华干燥工艺的研究 被引量:7
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作者 陈学玲 何建军 +5 位作者 程薇 文胜利 张光阳 熊光权 叶丽秀 陈玉霞 《湖北农业科学》 北大核心 2006年第3期367-369,388,共4页
利用真空冷冻升华干燥技术对武昌鱼进行保鲜加工研究,对影响产品质量和设备生产能力的主要参数进行了L12(35)正交试验设计,并评定了冻干产品的含水量、外观、复水性、营养成分等感官理化特性。结果表明,冻干技术既保持了新鲜武昌鱼的风... 利用真空冷冻升华干燥技术对武昌鱼进行保鲜加工研究,对影响产品质量和设备生产能力的主要参数进行了L12(35)正交试验设计,并评定了冻干产品的含水量、外观、复水性、营养成分等感官理化特性。结果表明,冻干技术既保持了新鲜武昌鱼的风味,又提高了其营养价值;武昌鱼冻干的最佳工艺为速冻温度-36℃,速冻时间16h,干燥升华时仓压100±10Pa,干燥解析时仓压80±10Pa,解析时物料温度50℃。 展开更多
关键词 真空冷冻干燥 武昌鱼 加工 干燥工艺 产品质量 营养价值
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Tomographic particle image velocimetry measurement on three-dimensional swirling flow in dual-stage counter-rotating swirler
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作者 Yuyang ZHOU Ling DONG +2 位作者 Mingtao SHANG Jibao LI Akira RINOSHIKA 《Chinese Journal of Aeronautics》 SCIE EI CAS CSCD 2024年第3期7-20,共14页
Three-Dimensional(3D)swirling flow structures,generated by a counter-rotating dualstage swirler in a confined chamber with a confinement ratio of 1.53,were experimentally investigated at Re=2.3×10^(5)using Tomogr... Three-Dimensional(3D)swirling flow structures,generated by a counter-rotating dualstage swirler in a confined chamber with a confinement ratio of 1.53,were experimentally investigated at Re=2.3×10^(5)using Tomographic Particle Image Velocimetry(Tomo-PIV)and planar Particle Image Velocimetry(PIV).Based on the analysis of the 3D time-averaged swirling flow structures and 3D Proper Orthogonal Decomposition(POD)of the Tomo-PIV data,typical coherent flow structures,including the Corner Recirculation Zone(CRZ),Central Recirculation Zone(CTRZ),and Lip Recirculation Zone(LRZ),were extracted.The counter-rotating dual-stage swirler with a Venturi flare generates the independence process of vortex breakdown from the main stage and pilot stage,leading to the formation of an LRZ and a smaller CTRZ near the nozzle outlet.The confinement squeezes the CRZ to the corner and causes a reverse rotation flow to limit the shape of the CTRZ.A large-scale flow structure caused by the main stage features an explosive breakup,flapping,and Precessing Vortex Core(PVC).The explosive breakup mode dominates the swirling flow structures owing to the expansion and construction of the main jet,whereas the flapping mode is related to the wake perturbation.Confinement limits the expansion of PVC and causes it to contract after the impacting area. 展开更多
关键词 Coherent structures Dual-stage counter-rotating swirler cup precessing vortex core Proper orthogonal decomposition Swirling flow Tomographic particle image velocimetry
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千金子炮制工艺研究 被引量:5
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作者 李群 江波 《中国现代中药》 CAS 2007年第9期14-15,共2页
目的:探讨千金子制霜新工艺。方法:以秦皮乙素、七叶树苷为对照品,采用薄层扫描法和高效液相法对传统制霜和新法制霜制得的成品进行含量测定。结果:新法与传统法制霜的成品在脂肪油、秦皮乙素、七叶树苷的含量上均无显著性差异(P>0.... 目的:探讨千金子制霜新工艺。方法:以秦皮乙素、七叶树苷为对照品,采用薄层扫描法和高效液相法对传统制霜和新法制霜制得的成品进行含量测定。结果:新法与传统法制霜的成品在脂肪油、秦皮乙素、七叶树苷的含量上均无显著性差异(P>0.05)。结论:说明新法(提油返油法)制霜完全可以代替传统方法,不仅提高效率、更易控制成品质量,而且具有推广价值。 展开更多
关键词 千金子 炮制工艺 提油返油法制霜新工艺
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Large eddy simulation of unconfined turbulent swirling flow 被引量:5
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作者 ZHANG HongDa HAN Chao +2 位作者 YE TaoHong ZHANG JiMin CHEN YiLiang 《Science China(Technological Sciences)》 SCIE EI CAS CSCD 2015年第10期1731-1744,共14页
Large eddy simulations(LES) were performed to study the non-reacting flow fields of a Cambridge swirl burner. The dynamic Smagorinsky eddy viscosity model is used as the sub-grid scale turbulence model. Comparisons of... Large eddy simulations(LES) were performed to study the non-reacting flow fields of a Cambridge swirl burner. The dynamic Smagorinsky eddy viscosity model is used as the sub-grid scale turbulence model. Comparisons of experimental data show that the LES results are capable of predicting mean and root-mean-square velocity profiles. The LES results show that the annular swirling flow has a minor impact on the formation of the bluff-body recirculation zone. The vortex structures near the shear layers, visualized by the iso-surface of Q-criterion, display ring structures in non-swirling flow and helical structures in swirling flow near the burner exit. Spectral analysis was employed to predict the occurrence of flow oscillations induced by vortex shedding and precessing vortex core(PVC). In order to extract accurately the unsteady large-scale structures in swirling flow, a three-dimensional proper orthogonal decomposition(POD) method was developed to reconstruct turbulent fluctuating velocity fields. POD analysis reveals that flow fields contain co-existing helical and toroidal shaped coherent structures. The helical structure associated with the PVC is the most energetic dynamic flow structure. The latter toroidal structure associated with vortex shedding has lower energy content which indicates that it is a secondary structure. 展开更多
关键词 Cambridge swirl burner large eddy simulation proper orthogonal decomposition vortex shedding and breakdown precessing vortex core
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Precessing Ball Solitons as Self-Organizing Systems during a Phase Transition in a Ferromagnet
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作者 V. V. Nietz 《Applied Mathematics》 2013年第10期78-83,共6页
Precessing ball solitons (PBS) in a ferromagnet during the first order phase transition is induced by a magnetic field directed along the axis of anisotropy, while the action of the periodic field perpendicular to the... Precessing ball solitons (PBS) in a ferromagnet during the first order phase transition is induced by a magnetic field directed along the axis of anisotropy, while the action of the periodic field perpendicular to the main magnetic field has been analyzed. Under these conditions, the characteristics of arising equilibrium PBS are uniquely determined by the frequency of the periodic field, but the solitons with other frequencies are impossible. For such structure, the entropy increase connected with dissipation is compensated by the decrease of the entropy due to the external periodic field. It is shown that the equilibrium PBS are essentially the “self-organizing systems” that can arise spotaneously in a metastable state of ferromagnet. 展开更多
关键词 FERROMAGNET MAGNETIC FIELD Periodic MAGNETIC FIELD FIRST-ORDER Phase Transition precessing BALL Soliton Dissipative MAGNETIC Structures SELF-ORGANIZING Systems
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Spin-dependent tunneling through a spin precession quantum dot
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作者 张爱芳 辛子华 +2 位作者 宋红岩 吴留坡 施耀铭 《Journal of Shanghai University(English Edition)》 CAS 2008年第1期39-42,共4页
Spin-polarized transport through a precessing magnetic spin coupled to ferromagnetic electrodes is studied using a non-equilibrium Green's function approach. The characteristic of conductance is obtained at zero temp... Spin-polarized transport through a precessing magnetic spin coupled to ferromagnetic electrodes is studied using a non-equilibrium Green's function approach. The characteristic of conductance is obtained at zero temperature. We find that competition between spin-exchange interaction on the spin site and spin-orbit interaction in the barriers dominates the resonant behavior of conductance. In a parallel configuration, conductance peaks have identical amplitude. With the angle θ increasing, the width of resonant peaks is broadened or narrowed for different spin coherent states. In an anti-parallel case, spin-flip tunneling in the barriers will essentially enhance amplitude of the conductance peak. 展开更多
关键词 spin-dependent transport precessing spin ferromagnetic electrodes
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RESARCH ON NEEDLE SHAPED WOLLASTONITE POWDER PROCESSING WITH HORIZONTAL DISK TYPE JET MILL
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作者 周立秋 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS 1994年第2期36-41,共6页
The way of producing needle-shaped wolldstonite pow-der has never been released, the key to the matter is to get high enough length to -width ratio of the particle. With φ 50 mm horizontal disk type jet mill,rue carr... The way of producing needle-shaped wolldstonite pow-der has never been released, the key to the matter is to get high enough length to -width ratio of the particle. With φ 50 mm horizontal disk type jet mill,rue carry out a series of experiments, and discover that select-ing reasonable technological operating condition, with the aim of weak-ening colliding pulverizing effect and reinforcing rubbing pulverizing effect, is helpful to improve effectively the L-W radio. 展开更多
关键词 needle luottastonete powder precessing horizontal disk type jet mill.
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Movement of Self-Organizing Solitons in Ferromagnet
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作者 V. V. Nietz 《Applied Mathematics》 2015年第10期1747-1754,共8页
Precessing ball solitons (PBS) in a ferromagnet during the first order phase transition induced by a magnetic field directed along the axis of anisotropy, while the additional action of high-frequency field perpendicu... Precessing ball solitons (PBS) in a ferromagnet during the first order phase transition induced by a magnetic field directed along the axis of anisotropy, while the additional action of high-frequency field perpendicular to the main magnetic field, are analyzed. It is shown that the spatial motion of solitons, associated with thermal fluctuations in the crystal, does not destroy the equilibrium of self-organized PBS. 展开更多
关键词 FERROMAGNET FIRST-ORDER Phase Transition MAGNETIC FIELD High-Frequency MAGNETIC FIELD precessing Ball Soliton SELF-ORGANIZING State Equilibrium Spatial Motion of SOLITONS
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Coulomb Interaction in Quantum Dot with a Precessing Magnetic Field
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作者 WU Liu-Po ZHOU Shi-Ping SONG Hong-Yan SHI Yao-Ming 《Communications in Theoretical Physics》 SCIE CAS CSCD 2007年第5X期943-948,共6页
We study electronic transport through a quantum dot (QD) with a precessing magnetic field. By using the Keldysh nonequilibrium Green function method, formulas of local density of states (LDOS) and conductance of Q... We study electronic transport through a quantum dot (QD) with a precessing magnetic field. By using the Keldysh nonequilibrium Green function method, formulas of local density of states (LDOS) and conductance of QD are derived self-consistently. It shows that the LDOS and conductance have obvious changes with the Coulomb blockade interaction. The intensity and angle of the magnetic field or temperatures, which reflect the mesoscopic structure of the QD are derived. The superiority of this device is that the QD can be controlled easily by the magnetic field, so it is valuable to apply in generating, manipulating and probing spin state. 展开更多
关键词 Coulomb interaction quantum dot precessing magnetic field
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中药炮制对药效的影响
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作者 高斐斐 刘志明 《中医临床研究》 2010年第24期24-25,共2页
目的:探讨中药炮制对药方的影响.方法:通过对中药采用不同的方法和辅料炮制,对药效进行比较.结果:通过炮制,消除方中某些药物的不良反应,利于治疗,提高药方疗效,调整方剂部分适应证,扩大应用范围,满足药方的剂型要求,保证临床安全有效.
关键词 中药 炮制 药效
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新型通用级苯酚-淀粉模塑料(PF2A1)的研制
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作者 陈国民 陈朝辉 简科 《材料工程》 EI CAS CSCD 北大核心 2004年第4期28-30,36,共4页
研制的产品典型配方(质量份)是苯酚-淀粉树脂∶六次甲基四胺∶木粉∶碳酸钙∶氧化镁∶硬脂酸锌∶硬脂酸∶油溶苯胺黑∶群青=37.0∶6.4∶48.0∶6.0∶0.6∶0.6∶0.4∶0.5∶0.5;制备工艺参数是混合时间≥60min,工作辊温度85-95℃,空转辊温... 研制的产品典型配方(质量份)是苯酚-淀粉树脂∶六次甲基四胺∶木粉∶碳酸钙∶氧化镁∶硬脂酸锌∶硬脂酸∶油溶苯胺黑∶群青=37.0∶6.4∶48.0∶6.0∶0.6∶0.6∶0.4∶0.5∶0.5;制备工艺参数是混合时间≥60min,工作辊温度85-95℃,空转辊温度145-155℃,辊距2.3~2.5mm,热炼时间4~5min,拼批时间≥45min;模塑工艺参数是预热温度100~110℃,预热时间10~15min,模塑压力≥25MPa,模塑温度175~180℃,模塑时间0.8~1.0min/mm,排气≥3次。产品性能达到酚醛模塑料(PF2A1)国家标准或优良,原料成本比苯酚-甲醛模塑料(PF2A1)低20.4%。 展开更多
关键词 苯酚-淀粉模塑料 PF2A1 配方设计 工艺 成本 物理性能 力学性能
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旋风分离器旋进涡核的数值模拟 被引量:60
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作者 吴小林 熊至宜 +1 位作者 姬忠礼 时铭显 《化工学报》 EI CAS CSCD 北大核心 2007年第2期383-390,共8页
采用雷诺应力模型对旋风分离器内三维非稳态流场进行了模拟计算。结果表明,旋风分离器全空间内都存在旋进涡核现象。对旋进涡核现象和旋进涡核中心的运动规律进行了详细的描述,分析了不同轴向位置的旋进涡核区域内不同点的速度波动幅值... 采用雷诺应力模型对旋风分离器内三维非稳态流场进行了模拟计算。结果表明,旋风分离器全空间内都存在旋进涡核现象。对旋进涡核现象和旋进涡核中心的运动规律进行了详细的描述,分析了不同轴向位置的旋进涡核区域内不同点的速度波动幅值和频率,得到了旋进涡核影响范围以及速度波动规律;通过分析旋进涡核中心的运动频率,得到了旋进涡核出现的强度。模拟结果与采用热线风速仪以及激光粒子成像技术(PIV)测定的实验结果基本吻合。研究结果可以分析旋进涡核对分离效率和压降的影响。 展开更多
关键词 旋风分离器 旋进涡核 数值模拟
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铬渣处理处置技术研究进展 被引量:40
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作者 景学森 蔡木林 杨亚提 《环境技术》 2006年第3期33-36,42,共5页
介绍了国内外铬渣处理处置技术的研究现状,并对各种处理处置技术的解毒机理、工艺条件及过程、优缺点、以及实践应用状况进行了分析。
关键词 铬渣 解毒 综合利用
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脂肪酶的底物特异性及其应用潜力 被引量:13
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作者 曹淑桂 《生物化学与生物物理进展》 SCIE CAS CSCD 北大核心 1995年第1期9-13,共5页
不同来源的Lipase对底物油脂中脂肪酸的链长、不饱和度及不饱和脂肪酸的双键位置表现出不同的脂肪酸特异性;对甘油酯中Sn-1(3)和Sn-2位酯键具有不同的位置特异性;对甘油酯中立体对映结构的1位和3位酯键呈现不同的... 不同来源的Lipase对底物油脂中脂肪酸的链长、不饱和度及不饱和脂肪酸的双键位置表现出不同的脂肪酸特异性;对甘油酯中Sn-1(3)和Sn-2位酯键具有不同的位置特异性;对甘油酯中立体对映结构的1位和3位酯键呈现不同的立体特异性,脂肪酶能够催化酯水解和酯合成(或酯交换)反应,用于制备甘油单酯、多不饱和脂肪酸及其酯和具有光学活性的有机化合物,因此它在油酯加工和有机合成中具有很大的应用潜力。 展开更多
关键词 脂肪酶 底物特异性 油脂加工 有机合成 应用
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中国地质标准物质制备技术与方法研究进展 被引量:30
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作者 王毅民 王晓红 +2 位作者 高玉淑 张学华 樊兴涛 《地质通报》 CAS CSCD 北大核心 2010年第7期1090-1104,共15页
评介了中国地质标准物质研制中技术方法方面的研究进展,包括样品加工技术,粒度检测与表征方法,均匀性检验与评价,最小取样量的确定,稳定性检验及其结果表述,定值方式,分析方法、数据处理及定值条件,不确定度评价与量值溯源保证等。对照... 评介了中国地质标准物质研制中技术方法方面的研究进展,包括样品加工技术,粒度检测与表征方法,均匀性检验与评价,最小取样量的确定,稳定性检验及其结果表述,定值方式,分析方法、数据处理及定值条件,不确定度评价与量值溯源保证等。对照国家相关的技术规范、国际标准化组织(ISO)的相关指南和国际地质分析者协会(IAG)关于地质标准物质研制的协议,讨论了目前中国地质标准物质制备技术的现状及未来的发展。 展开更多
关键词 地质标准物质 样品加工 粒度检测与表征 均匀性及稳定性检验 不确定度评价 量值溯源
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基于小波变换与形态学的一种边界重叠图像的拼接算法 被引量:5
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作者 赵唯 李端义 《微机发展》 2001年第6期3-6,共4页
针对噪声环境下的图像拼接问题 ,本文给出了一种基于小波变换与数学形态学的方法。该方法首先是通过小波变换的多尺度分析提取出不同边缘方向的边缘图像 ,然后将其混合 ,利用形态学方法寻找可能的拼接物再进行拼接。
关键词 图像处理 小波变换 数学形态学 图像拼接算法
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