The preparation of ultra fine Y A G( Y3 Al5 O12) po w der through co precipitation techniquew as investigated . The for m ation tem perature of Y A G w as lo wered belo w 800 ℃ by carefullycontrolling process...The preparation of ultra fine Y A G( Y3 Al5 O12) po w der through co precipitation techniquew as investigated . The for m ation tem perature of Y A G w as lo wered belo w 800 ℃ by carefullycontrolling process para m eters . Ultra fine Y A G po w der w ith even size distribution , spheri cal shapes , and 40 n m particle size has been produced . It is found that for m ation of Y A Gisnot through the Y A M an d Y A Pinter mediate phases that are often observed during the synthe sis of Y A G by m ixed oxide m ethod . The sm all particle size of the precursor po w der , them olecular scale mixing of the constituents , and the poly m orphic transfor m ation of Al2 O3during heating accou nt m ainly for the reduction of for m ation tem perature of Y A Gan d the e lim ination of inter m ediate Y A M and Y A Pphases .展开更多
Using yttriu m nitrate as the m other salt , synthesis of ultrafine yttria po w der through w et che mical route w as investigated . Choice of precipitant has dra m atic effects on co m position ,particle size distrib...Using yttriu m nitrate as the m other salt , synthesis of ultrafine yttria po w der through w et che mical route w as investigated . Choice of precipitant has dra m atic effects on co m position ,particle size distribution and particle m orphology of the precipitates . When a m m onia solutionw as used as the precipitant , the precursor precipitate w as m ainly Y2( O H) 5 14( N O3) 0 86· H2 O with co m paratively large particle size , broad size distribution and co m plex particleshapes . When sodiu m hydroxide solution w as used , roughly spherical α Y( O H)3·3 H2 Opre cipitate w ith sm all particle size and narro w size distribution w as obtained . The transfor m a tion sequence of dry α Y( O H)3 ·3 H2 O gel during calcination w as determ ined to be α Y( O H) 3·3 H2 O→ Y O O H→ Y2 O3 . After calcining at 600 ℃ for 1 hour , both Y2( O H) 5 14( N O3) 0 86· H2 O and α Y( O H) 3·3 H2 O transfor m to well crystallized Y2 O3 pow ders ,w ith particle sizes of 50 ~3000 n m and 20 n m , respectively .展开更多
Data management becomes essential component of patient healthcare.Internet of Medical Things(IoMT)performs a wireless communication between E-medical applications and human being.Instead of consulting a doctor in the ...Data management becomes essential component of patient healthcare.Internet of Medical Things(IoMT)performs a wireless communication between E-medical applications and human being.Instead of consulting a doctor in the hospital,patients get health related information remotely from the physician.The main issues in the E-Medical application are lack of safety,security and priv-acy preservation of patient’s health care data.To overcome these issues,this work proposes block chain based IoMT Processed with Hybrid consensus protocol for secured storage.Patients health data is collected from physician,smart devices etc.The main goal is to store this highly valuable health related data in a secure,safety,easy access and less cost-effective manner.In this research we combine two smart contracts such as Practical Byzantine Fault Tolerance with proof of work(PBFT-PoW).The implementation is done using cloud technology setup with smart contracts(PBFT-PoW).The accuracy rate of PBFT is 90.15%,for PoW is 92.75%and our proposed work PBFT-PoW is 99.88%.展开更多
According to Angelica Duran and Yuhan Huang, Mo Yan's "artistic works" are "towering within the literatures of the world." His novel Si shi yi pao (Pow!, 2o12) offers one of the clearest recent examples of what...According to Angelica Duran and Yuhan Huang, Mo Yan's "artistic works" are "towering within the literatures of the world." His novel Si shi yi pao (Pow!, 2o12) offers one of the clearest recent examples of what Shelley W. Chan calls Mo's "postmodern playfulness." In his afterword to Pow! Mo says that the story "gives way to an improvisation that swings between reality and illusion," thus suggesting the notion of "hallucinatory realism" as a "blending" or "merging" of the illusory and the real. This article examines the ideology--that is, the class politics of consciousness--of this swingy postmodern storytelling, taking a critical view of Mo's playfully bold assertion: "I've always taken pride in my lack of ideology, especially when I'm writing." I argue that the swinginess of "imagination" in Pow! embodies what Marx calls a "happy confusion" that (re)articulates the "post"-class doctrine of "combine two into one."展开更多
Hydrocarbons separation in petrochemical industries is a key,energy-consuming stage in the manufacture of high-quality added-value products—hence the need for more efficient materials and environmentally friendly met...Hydrocarbons separation in petrochemical industries is a key,energy-consuming stage in the manufacture of high-quality added-value products—hence the need for more efficient materials and environmentally friendly methodologies to improve this process.In this context,we have studied the effect of metal-organic frameworks(MOFs)pore functionalization in hexane isomers separation,isolating the robust isoreticular zinc(ll)bipyrazolates Zn(BPZ),showing no pore decoration,Zn(Me_(2)BPZ),the pores of which are decorated with apolar methyl groups,and Zn(BPZ(NH_(2))_(2)),the spacers of which possess polar Lewis-basic functions(H_(2)BPZ=1H,1'H-4,4'-bipyrazole;H_(2)Me_(2)BPZ=3,3'-dimethyl-1H,1'H-4,4'-bipyrazole;H_(2)BPZ(NH_(2))_(2)=3,5-diamino-1H,1'H-4,4'-bipyrazole;DMF=dimethylformamide).After characterizing Zn(BPZ(NH_(2))_(2))as per its crystal structure and thermal behaviour,and all the three MOFs as per their textural properties,we investigated,from the experimental and computational points of view,the impact of the square one-dimensional channels decoration on the separation of the hexane isomers,demonstrating the relevance of pore constrictions in the resolution of the title alkanes mixture.展开更多
文摘The preparation of ultra fine Y A G( Y3 Al5 O12) po w der through co precipitation techniquew as investigated . The for m ation tem perature of Y A G w as lo wered belo w 800 ℃ by carefullycontrolling process para m eters . Ultra fine Y A G po w der w ith even size distribution , spheri cal shapes , and 40 n m particle size has been produced . It is found that for m ation of Y A Gisnot through the Y A M an d Y A Pinter mediate phases that are often observed during the synthe sis of Y A G by m ixed oxide m ethod . The sm all particle size of the precursor po w der , them olecular scale mixing of the constituents , and the poly m orphic transfor m ation of Al2 O3during heating accou nt m ainly for the reduction of for m ation tem perature of Y A Gan d the e lim ination of inter m ediate Y A M and Y A Pphases .
文摘Using yttriu m nitrate as the m other salt , synthesis of ultrafine yttria po w der through w et che mical route w as investigated . Choice of precipitant has dra m atic effects on co m position ,particle size distribution and particle m orphology of the precipitates . When a m m onia solutionw as used as the precipitant , the precursor precipitate w as m ainly Y2( O H) 5 14( N O3) 0 86· H2 O with co m paratively large particle size , broad size distribution and co m plex particleshapes . When sodiu m hydroxide solution w as used , roughly spherical α Y( O H)3·3 H2 Opre cipitate w ith sm all particle size and narro w size distribution w as obtained . The transfor m a tion sequence of dry α Y( O H)3 ·3 H2 O gel during calcination w as determ ined to be α Y( O H) 3·3 H2 O→ Y O O H→ Y2 O3 . After calcining at 600 ℃ for 1 hour , both Y2( O H) 5 14( N O3) 0 86· H2 O and α Y( O H) 3·3 H2 O transfor m to well crystallized Y2 O3 pow ders ,w ith particle sizes of 50 ~3000 n m and 20 n m , respectively .
基金Research Supporting Project number(RSP-2021/323)King Saud University,Riyadh,Saudi Arabia.
文摘Data management becomes essential component of patient healthcare.Internet of Medical Things(IoMT)performs a wireless communication between E-medical applications and human being.Instead of consulting a doctor in the hospital,patients get health related information remotely from the physician.The main issues in the E-Medical application are lack of safety,security and priv-acy preservation of patient’s health care data.To overcome these issues,this work proposes block chain based IoMT Processed with Hybrid consensus protocol for secured storage.Patients health data is collected from physician,smart devices etc.The main goal is to store this highly valuable health related data in a secure,safety,easy access and less cost-effective manner.In this research we combine two smart contracts such as Practical Byzantine Fault Tolerance with proof of work(PBFT-PoW).The implementation is done using cloud technology setup with smart contracts(PBFT-PoW).The accuracy rate of PBFT is 90.15%,for PoW is 92.75%and our proposed work PBFT-PoW is 99.88%.
文摘According to Angelica Duran and Yuhan Huang, Mo Yan's "artistic works" are "towering within the literatures of the world." His novel Si shi yi pao (Pow!, 2o12) offers one of the clearest recent examples of what Shelley W. Chan calls Mo's "postmodern playfulness." In his afterword to Pow! Mo says that the story "gives way to an improvisation that swings between reality and illusion," thus suggesting the notion of "hallucinatory realism" as a "blending" or "merging" of the illusory and the real. This article examines the ideology--that is, the class politics of consciousness--of this swingy postmodern storytelling, taking a critical view of Mo's playfully bold assertion: "I've always taken pride in my lack of ideology, especially when I'm writing." I argue that the swinginess of "imagination" in Pow! embodies what Marx calls a "happy confusion" that (re)articulates the "post"-class doctrine of "combine two into one."
基金R.V.and S.G.acknowledge Universita delFInsubria for partial funding.J.A.R.N.is very grateful to Spanish MINECO(No.CTQ2017-84692-R)and EU Feder funding.C.D.N.and C.P.acknowledge University of Cam erinofor partial funding.
文摘Hydrocarbons separation in petrochemical industries is a key,energy-consuming stage in the manufacture of high-quality added-value products—hence the need for more efficient materials and environmentally friendly methodologies to improve this process.In this context,we have studied the effect of metal-organic frameworks(MOFs)pore functionalization in hexane isomers separation,isolating the robust isoreticular zinc(ll)bipyrazolates Zn(BPZ),showing no pore decoration,Zn(Me_(2)BPZ),the pores of which are decorated with apolar methyl groups,and Zn(BPZ(NH_(2))_(2)),the spacers of which possess polar Lewis-basic functions(H_(2)BPZ=1H,1'H-4,4'-bipyrazole;H_(2)Me_(2)BPZ=3,3'-dimethyl-1H,1'H-4,4'-bipyrazole;H_(2)BPZ(NH_(2))_(2)=3,5-diamino-1H,1'H-4,4'-bipyrazole;DMF=dimethylformamide).After characterizing Zn(BPZ(NH_(2))_(2))as per its crystal structure and thermal behaviour,and all the three MOFs as per their textural properties,we investigated,from the experimental and computational points of view,the impact of the square one-dimensional channels decoration on the separation of the hexane isomers,demonstrating the relevance of pore constrictions in the resolution of the title alkanes mixture.