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Differences of element distribution between free and wheel side surface of NdFeB/α-Fe ribbons 被引量:1
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作者 査五生 刘锦云 +1 位作者 宋天秀 王正云 《Journal of Rare Earths》 SCIE EI CAS CSCD 2011年第1期94-96,共3页
The ribbons of NdFeB/College of Material Science & Engineering, Xihua University, Chengdu 610039, China-Fe composite alloy were prepared by melt spinning and post crystallizing technique. The element distri- butions ... The ribbons of NdFeB/College of Material Science & Engineering, Xihua University, Chengdu 610039, China-Fe composite alloy were prepared by melt spinning and post crystallizing technique. The element distri- butions and phase component of both surfaces of as-spun ribbons were measured by energy dispersive spectrometry (EDS) and X-ray diffraction (XRD). Because of the centrifugation, a segregation of B, Fe, and Nd concentrations was observed at the cross section. After crystallizing annealing, the element concentration segregation still existed in the as-crystallized ribbons. Due to the segregation of B, Fe, and Nd, the B-rich phase was observed near the wheel side surface. The B-rich phase may deteriorate the magnetic property of NdFeB/a-Fe composite alloy. 展开更多
关键词 ndfeb/a-fe alloy melt spin concentration segregation B-rich phase rare earths
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NdFeB/α-Fe合金快淬薄带表面微观形貌 被引量:4
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作者 查五生 刘锦云 +2 位作者 王正云 周胜海 贾永灿 《稀有金属材料与工程》 SCIE EI CAS CSCD 北大核心 2010年第A01期174-176,共3页
采用快淬加后续晶化退火方法,制备了NdFeB/α-Fe双相纳米晶复合永磁合金的快淬态和晶化态薄带,用原子力显微镜(AFM)观察了薄带贴辊面和自由面的微观形貌,分析研究了薄带不同表面晶粒尺寸与均匀性的差异。贴辊面快淬时冷却速度快、结晶度... 采用快淬加后续晶化退火方法,制备了NdFeB/α-Fe双相纳米晶复合永磁合金的快淬态和晶化态薄带,用原子力显微镜(AFM)观察了薄带贴辊面和自由面的微观形貌,分析研究了薄带不同表面晶粒尺寸与均匀性的差异。贴辊面快淬时冷却速度快、结晶度高,快淬态主要由非晶体组成,退火时新相的析出以均匀形核的方式成核,晶化态晶粒数量少、平均尺寸(~70nm)大,但晶粒大小均匀。自由面快淬时析出了数量较多、尺寸较大的微晶,退火时以非均匀形核为主,成核率高,晶粒数量多、尺寸小,平均晶粒尺寸(~50nm)小于贴辊面,但由于微晶本身的长大,形成了超过100nm的粗大晶粒,使微观结构的均匀性变差。薄带不同表面微观形貌的差异将会对纳米晶复合永磁材料的磁性能产生直接的影响。 展开更多
关键词 ndfeb/α—fe合金 快淬薄带 表面形貌:晶粒尺寸 均匀性
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