Deformation can change the transition pathway of materials under high pressure,thus significantly affects physical and chemical properties of matters.However,accurate pressure calibration under deformation is challeng...Deformation can change the transition pathway of materials under high pressure,thus significantly affects physical and chemical properties of matters.However,accurate pressure calibration under deformation is challenging and thereby causes relatively large pressure uncertainties in deformation experiments,resulting in the synthesis of complex multiphase materials.Here,pressure generations of three types of deformation assemblies were well calibrated in a Walker-type largevolume press(LVP)by electrical resistance measurements combined with finite element simulations(FESs).Hard Al_(2)O_(3) or diamond pistons in shear and uniaxial deformation assemblies significantly increase the efficiency of pressure generation compared with the conventional quasi-hydrostatic assembly.The uniaxial deformation assembly using flat diamond pistons possesses the highest efficiency in these deformation assemblies.This finding is further confirmed by stress distribution analysis based on FESs.With this deformation assembly,we found shear can effectively promote the transformation of C60 into diamond under high pressure and realized the synthesis of phase-pure diamond at relatively moderate pressure and temperature conditions.The present developed techniques will help improve pressure efficiencies in LVP and explore the new physical and chemical properties of materials under deformation in both science and technology.展开更多
For an ultra-high-pressure hydraulic transmission system of a large-size hydraulic forging press(LHFP),a 70 MPa two-way proportional cartridge valve has been developed to improve the power weight ratio of the hydrauli...For an ultra-high-pressure hydraulic transmission system of a large-size hydraulic forging press(LHFP),a 70 MPa two-way proportional cartridge valve has been developed to improve the power weight ratio of the hydraulic forging press.In this study,a nominal diameter 25 mm(DN25)cartridge valve is taken as the research object.A longer concentric cylindrical annular gap is set to effectively prevent the ultra-high-pressure oil from flowing to the pilot stage and a seated valve structure is set to form the linear sealing zone in the closing state of the main valve port.Electric-displacement feedback is adopted to realize precise control of the main valve port flow and the features of this valve are investigated.In order to verify the strength and static and dynamic characteristics,the finite element model and a simulation model of the valve proposed above are built.There is a little deformation which does not affect the main valve spool movement,and the main valve port flow meets the design demands.Then,the prototype of DN2570 TPCV is manufactured and a ultra-high-pressure experimental platform is developed.The experimental results show that the DN2570 TPCV designed in this study has the advantage of fast response,high control precision,and low leakage,which can meet the requirements of LHFPs.展开更多
基金the National Natural Science Foundation of China(Grant Nos.42272041,41902034,52302043,12304015,52302043,and 12011530063)the National Major Science Facility Synergetic Extreme Condition User Facility Achievement Transformation Platform Construction(Grant No.2021FGWCXNLJSKJ01)+2 种基金the China Postdoctoral Science Foundation(Grant Nos.2022M720054 and 2023T160257)the National Key Research and Development Program of China(Grant No.2022YFB3706602)the Jilin Univer-sity High-level Innovation Team Foundation,China(Grant No.2021TD-05).
文摘Deformation can change the transition pathway of materials under high pressure,thus significantly affects physical and chemical properties of matters.However,accurate pressure calibration under deformation is challenging and thereby causes relatively large pressure uncertainties in deformation experiments,resulting in the synthesis of complex multiphase materials.Here,pressure generations of three types of deformation assemblies were well calibrated in a Walker-type largevolume press(LVP)by electrical resistance measurements combined with finite element simulations(FESs).Hard Al_(2)O_(3) or diamond pistons in shear and uniaxial deformation assemblies significantly increase the efficiency of pressure generation compared with the conventional quasi-hydrostatic assembly.The uniaxial deformation assembly using flat diamond pistons possesses the highest efficiency in these deformation assemblies.This finding is further confirmed by stress distribution analysis based on FESs.With this deformation assembly,we found shear can effectively promote the transformation of C60 into diamond under high pressure and realized the synthesis of phase-pure diamond at relatively moderate pressure and temperature conditions.The present developed techniques will help improve pressure efficiencies in LVP and explore the new physical and chemical properties of materials under deformation in both science and technology.
基金Supported by the Natural Science Foundation of Hebei Province(E2018203028)。
文摘For an ultra-high-pressure hydraulic transmission system of a large-size hydraulic forging press(LHFP),a 70 MPa two-way proportional cartridge valve has been developed to improve the power weight ratio of the hydraulic forging press.In this study,a nominal diameter 25 mm(DN25)cartridge valve is taken as the research object.A longer concentric cylindrical annular gap is set to effectively prevent the ultra-high-pressure oil from flowing to the pilot stage and a seated valve structure is set to form the linear sealing zone in the closing state of the main valve port.Electric-displacement feedback is adopted to realize precise control of the main valve port flow and the features of this valve are investigated.In order to verify the strength and static and dynamic characteristics,the finite element model and a simulation model of the valve proposed above are built.There is a little deformation which does not affect the main valve spool movement,and the main valve port flow meets the design demands.Then,the prototype of DN2570 TPCV is manufactured and a ultra-high-pressure experimental platform is developed.The experimental results show that the DN2570 TPCV designed in this study has the advantage of fast response,high control precision,and low leakage,which can meet the requirements of LHFPs.
