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化学镀Ni-P合金/TiO_2复合膜的耐蚀性研究 被引量:10
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作者 宋来洲 李健 王福君 《材料科学与工艺》 EI CAS CSCD 2002年第2期148-151,共4页
在改进常规制备方法的基础上,提出化学镀/溶胶-凝胶复合法在碳钢表面制备TiO2复合膜的新技术.用X衍射研究了复合膜的组织形态,采用环境扫描电镜(ESEM)表征了复合膜的表观和断面形貌,用极化电阻、阳极极化曲线测量等方法研究TiO2复合膜在... 在改进常规制备方法的基础上,提出化学镀/溶胶-凝胶复合法在碳钢表面制备TiO2复合膜的新技术.用X衍射研究了复合膜的组织形态,采用环境扫描电镜(ESEM)表征了复合膜的表观和断面形貌,用极化电阻、阳极极化曲线测量等方法研究TiO2复合膜在0.5mol/L硫酸和0.5mol/L氯化钠溶液中的耐蚀性能.结果表明A3钢表面的TiO2复合膜耐蚀性能优良. 展开更多
关键词 NI-P合金 化学镀 溶胶-凝胶复合法 TiO2复合膜 耐蚀性 镍磷合金 二氧化钛 碳钢
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TiO_2复合膜的耐蚀性能研究 被引量:5
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作者 林万舟 宋来洲 《腐蚀与防护》 CAS 2003年第1期9-12,共4页
采用化学镀 /溶胶 凝胶复合法在碳钢表面制备TiO2 复合膜 ,用X射线衍射法研究复合膜的组织形态 ,采用环境扫描电镜 (ESEM)表征了复合膜的表观形貌 ,用极化阻力、电化学阻抗谱测量等方法研究TiO2 复合膜在0 5mol/L硫酸和 0 .5mol/L氯... 采用化学镀 /溶胶 凝胶复合法在碳钢表面制备TiO2 复合膜 ,用X射线衍射法研究复合膜的组织形态 ,采用环境扫描电镜 (ESEM)表征了复合膜的表观形貌 ,用极化阻力、电化学阻抗谱测量等方法研究TiO2 复合膜在0 5mol/L硫酸和 0 .5mol/L氯化钠溶液中的耐蚀性能。结果表明A3钢表面的TiO2 展开更多
关键词 化学镀/溶胶-凝胶复合法 TiO2复合膜 耐蚀性
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PREPARATION AND CORROSION RESISTANCE OF NiP/TiO_2 COMPOSITE FILM ON CARBON STEEL IN SULFURIC ACID SOLUTION 被引量:3
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作者 L.Z. Song S.Z. Song J. Zhao 《Acta Metallurgica Sinica(English Letters)》 SCIE EI CAS CSCD 2006年第2期117-123,共7页
A NiP/TiO2 composite film on carbon steel was prepared by electroless plating and sol-gel composite process. An artificial neural network was applied to optimize the prepared condition of the composite film. Corrosion... A NiP/TiO2 composite film on carbon steel was prepared by electroless plating and sol-gel composite process. An artificial neural network was applied to optimize the prepared condition of the composite film. Corrosion behavior of the NiP/TiO2 composite film was investigated by polarization resistance measurement, anode polarization, ESEM (environmental scanning electron microscopy) and EIS (electrochemical impedance spectroscopy) measurements. Results showed that the NiP/ TiO2 composite film has a good corrosion resistance in 0.5mol/L H2SO4 solution. The element valence of the composite film was characterized by XPS (X-ray photoelectron spectroscopy) spectrum, and an anticorrosion mechanism of the composite film was discussed. 展开更多
关键词 electroless plating and sol-gel composite process artificial neural network NiP/TiO2 composite film corrosion resistance
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Formation of TiO2 Modified Film on Carbon Steel 被引量:2
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作者 LaizhouSONG ShizheSONG ZhimingGAO 《Journal of Materials Science & Technology》 SCIE EI CAS CSCD 2004年第5期599-601,共3页
A new technique for preparing TiO2 modified film on carbon steel was accomplished by electroless plating and sol-gel composite process. The artificial neural network was applied to optimize the preparing condition of ... A new technique for preparing TiO2 modified film on carbon steel was accomplished by electroless plating and sol-gel composite process. The artificial neural network was applied to optimize the preparing condition of TiO2 modified film. The optimized condition for forming TiO2 modified film on carbon steel was that NiP plating for 50 min, dip-coating times as 4, heat treatment time for 2 h, and the molar ratio of complexing agent and Ti(OC4HZ9)4 kept 1.5:1. The results showed that TiO2 modified film have good corrosion resistance. The result conformed that it is feasible to design the preparing conditions of TiO2 modified film by artificial neural network. 展开更多
关键词 electroless plating sol-gel composite process Artificial neural network TiO2 modified film Corrosion resistance
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Modification and Anticorrosion Property of Carbon Steel with TiO_2 Film 被引量:2
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作者 SONG Lai-zhou ZHAO Jing WANG Xiu-li 《Journal of Iron and Steel Research International》 SCIE CAS CSCD 2005年第6期37-41,共5页
A new TiO2 modified film on carbon steel was prepared by electroless plating and sol gel composite process. An artificial neural net was used to optimize the preparing condition of the film. The optimized condition of... A new TiO2 modified film on carbon steel was prepared by electroless plating and sol gel composite process. An artificial neural net was used to optimize the preparing condition of the film. The optimized condition of the TiO2-modified film on carbon steel is as follows: plating time of NiP is 50 min, number of dip coating is 4, heat treatment time is 2 h, and the molar ratio of complexing reagent to Ti(OC4 H9)4 is 1.5 : 1. Corrosion behavior of carbon steel with coating was investigated by polarization resistance measurement, anode polarization, EIS and ESEM measurement. XPS was used to characterize the element valence of the modified film. Results show that carbon steel with TiO2 modified film has good corrosion resistance in 0.5 mol/L of H2SO4 solution and 0.5 mol/L of NaCl solution. It is also found that the preparing condition of forming TiO2-modified film can be obtained easily by the artificial neural net. 展开更多
关键词 electroless plating sol-gel composite process artificial neural net TiO2-modified film corrosion resistance
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