应用电子背散射衍射(EBSD)和取向成像显微技术(OIM)研究了材料初始状态、冷轧压下量和1100℃退火对690合金晶界特征分布(GBCD)的影响。低层错能面心立方金属镍基690合金,冷轧5%后在1100℃退火5min可使低ΣCSL(coincidence site lattice...应用电子背散射衍射(EBSD)和取向成像显微技术(OIM)研究了材料初始状态、冷轧压下量和1100℃退火对690合金晶界特征分布(GBCD)的影响。低层错能面心立方金属镍基690合金,冷轧5%后在1100℃退火5min可使低ΣCSL(coincidence site lattice,Σ≤29)晶界比例提高到70%以上(Palumbo-Aust标准),同时形成大尺寸的晶粒团簇。低ΣCSL晶界比例和这种晶粒团簇的尺寸随冷轧压下量的增加而下降。初始状态的固溶或时效对690合金在1100℃再结晶退火后的晶界特征分布无明显影响。展开更多
The quantitative analysis of substructure in the martensite/bainite mixed structure, which is obtained from low-carbon NiCrMoV steels under different cooling conditions, was made by means of optical microscope (OM),...The quantitative analysis of substructure in the martensite/bainite mixed structure, which is obtained from low-carbon NiCrMoV steels under different cooling conditions, was made by means of optical microscope (OM), scanning electron microscope (SEM), electron backscatter diffraction (EBSD), and transmission electron microscope (TEM), in order to research the effect on toughness. The test results indicate that the toughness of the steel is en- hanced with the decrease in the packet and block size under the condition of the same prior austenite grain size mixed with different ratios of martensite and bainite while the lath width is about 0.38μm. The calculation shows that both the packet and block boundaries have the same hindering effect on crack extension. Furthermore, the effect of the block width on impact energy is much larger than that of the packet. Therefore, the block can be used as microstruc- tural substructure to affect the toughness in low-carbon martensite steels, suggesting that the block size is "the effective grain size" for controlling toughness.展开更多
文摘应用电子背散射衍射(EBSD)和取向成像显微技术(OIM)研究了材料初始状态、冷轧压下量和1100℃退火对690合金晶界特征分布(GBCD)的影响。低层错能面心立方金属镍基690合金,冷轧5%后在1100℃退火5min可使低ΣCSL(coincidence site lattice,Σ≤29)晶界比例提高到70%以上(Palumbo-Aust标准),同时形成大尺寸的晶粒团簇。低ΣCSL晶界比例和这种晶粒团簇的尺寸随冷轧压下量的增加而下降。初始状态的固溶或时效对690合金在1100℃再结晶退火后的晶界特征分布无明显影响。
文摘The quantitative analysis of substructure in the martensite/bainite mixed structure, which is obtained from low-carbon NiCrMoV steels under different cooling conditions, was made by means of optical microscope (OM), scanning electron microscope (SEM), electron backscatter diffraction (EBSD), and transmission electron microscope (TEM), in order to research the effect on toughness. The test results indicate that the toughness of the steel is en- hanced with the decrease in the packet and block size under the condition of the same prior austenite grain size mixed with different ratios of martensite and bainite while the lath width is about 0.38μm. The calculation shows that both the packet and block boundaries have the same hindering effect on crack extension. Furthermore, the effect of the block width on impact energy is much larger than that of the packet. Therefore, the block can be used as microstruc- tural substructure to affect the toughness in low-carbon martensite steels, suggesting that the block size is "the effective grain size" for controlling toughness.