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An efficient regioselective sonochemical synthesis of novel 4-aryl-3-methyl-4,5-dihydro-1H-pyrazolo[3,4-b]pyridin-6(7H)-ones 被引量:1
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作者 Abbas Azimi Roshan Manouchehr Mamaghani +1 位作者 Nosrat Ollah Mahmoodi Farhad Shirini 《Chinese Chemical Letters》 SCIE CAS CSCD 2012年第4期399-402,共4页
An efficient ultrasound-assisted preparation of a series of novel 4-aryl-3-methyl-4,5-dihydro-l//-pyrazolo[34-b]pyridin-6(7H)ones via the reaction of 5-amino-3-methyl-1H-pyrazole,Meldrum's acid and various arylalde... An efficient ultrasound-assisted preparation of a series of novel 4-aryl-3-methyl-4,5-dihydro-l//-pyrazolo[34-b]pyridin-6(7H)ones via the reaction of 5-amino-3-methyl-1H-pyrazole,Meldrum's acid and various arylaldehydes using one-pot three-component approach is described.This rapid method produced the products in short reaction times(3-4 min) and excellent yields(87-95%). 展开更多
关键词 Pyrazolo[3 4-b]pyridin-67h)-one Meldrum's acid 5-Amino-3-methylpyrazole one-pot Ultrasonic irradiation Three-component REGIOSELECTIVE
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The mechanism of unexpected reduction of dimethyl pyridine-2,3-dicarboxylate to l,2,3,4-tetrahydrofuro[3,4-b]-pyridin-5(7H)-one with sodium borohydride
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作者 Yan Bo Tang Qing Jian Zhang De Quan Yu 《Chinese Chemical Letters》 SCIE CAS CSCD 2012年第10期1122-1124,共3页
An unexpected reduction of dimethyl pyridine-2,3-dicarboxylate to 1,2,3,4-tetrahydrofuro[3,4-b]pyridin-5(7H)-one with sodium borohydride in ethanol and tetrahydrofuran, respectively, is described, a hypothetic mecha... An unexpected reduction of dimethyl pyridine-2,3-dicarboxylate to 1,2,3,4-tetrahydrofuro[3,4-b]pyridin-5(7H)-one with sodium borohydride in ethanol and tetrahydrofuran, respectively, is described, a hypothetic mechanism for the unusual reductive product is proposed. 展开更多
关键词 REDUCTION Sodium borohydride Dimethyl pyridine-2 3-dicarboxylate 1 2 3 4-Tetrahydrofuro[3 4-b]pyridin-5(7h)-one Reactionmechanism
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