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2-取代-3-氨基-4(3H)-喹唑啉酮类化合物的合成与表征 被引量:2
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作者 高兴文 严敏 +1 位作者 刘玉琦 田烨 《化学试剂》 CAS CSCD 北大核心 2010年第5期461-464,共4页
以(未)取代邻氨基苯甲酸与乙酐或芳甲酰氯反应并环化,生成2-甲基-4(H)-3,1-苯并噁嗪酮衍生物,该中间体与80%水合肼反应即得目标化合物,收率76.1%~90.1%。
关键词 3-氨基-4(3H)-喹唑啉酮 4(H)-3 1-苯并噁嗪酮 邻氨基苯甲酸 合成
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3-Phenyl/Pyridinyl Derivatives of <i>Trans</i>-2-(aryl/heteryl)vinyl-3<i>H</i>-quinazolin-4-ones: Synthesis and Fluorescent Properties
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作者 Emiliya V. Nosova Tatyana V. Stupina +3 位作者 Galina N. Lipunova Marina S. Valova Pavel A. Slepukhin Valery N. Charushin 《International Journal of Organic Chemistry》 2012年第1期56-63,共8页
Novel 3-phenyl/pyridinyl-trans-2-(aryl/heteryl)vinyl-3H-quinazolin-4-ones 3a,b, 4a, 5a, 7a and their 6,7-difluoro de- rivatives 3c,d, 4b, 5b, 7b have been obtained by condensation of the correspondent 2-methylquinazol... Novel 3-phenyl/pyridinyl-trans-2-(aryl/heteryl)vinyl-3H-quinazolin-4-ones 3a,b, 4a, 5a, 7a and their 6,7-difluoro de- rivatives 3c,d, 4b, 5b, 7b have been obtained by condensation of the correspondent 2-methylquinazolin-4-ones 1, 6 with aromatic (heterocyclic) aldehydes in the presence of ZnCl2 (AcONa) or by the reaction of 2-methyl-3,1-benzoxazin-4- ones 2 with the Shiff bases. Effects of aryl(heteryl) substituents on photophysical properties of (aryl/heteryl) quinazolinylethenes have been studied. 展开更多
关键词 Styryl Benzazines Fluorinated Quinazolin-4-Ones UV and FL Spectra X-Ray Trans-cis-Isomerisation 2-Methylquinazolinones 2-Methyl-3 1-benzoxazinones
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