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a-Si∶H薄膜固相晶化法制备多晶硅薄膜 被引量:17
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作者 陈城钊 方健文 林璇英 《浙江师范大学学报(自然科学版)》 CAS 2002年第3期246-249,共4页
利用固相晶化法获得多晶硅薄膜 (退火温度 70 0~ 80 0℃ ) ,采用XRD、Raman等分析手段进行了表征与分析 .研究结果表明 :晶粒平均尺寸随着退火温度的降低、掺杂浓度的减少、薄膜厚度的增加而增加 ;并且退火后薄膜暗电导率提高了 2~
关键词 多晶硅薄膜 固相晶化法 α—Si:H薄膜 平均晶粒尺寸 退火温度 掺杂浓度 薄膜厚度
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Effect of ultrasonic power and casting speed on solidification structure of 7050 aluminum alloy ingot in ultrasonic field 被引量:20
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作者 张立华 余军 张晓明 《Journal of Central South University》 SCIE EI CAS 2010年第3期431-436,共6页
With the experiment and finite element simulation, the influences of power ultrasonic on the solidification structure of 7050 aluminum alloy ingot in semi-continuous casting were researched, and the effects of casting... With the experiment and finite element simulation, the influences of power ultrasonic on the solidification structure of 7050 aluminum alloy ingot in semi-continuous casting were researched, and the effects of casting speed on solidification structure in ultrasonic field were also analyzed. The experiment and simulation results show that the solidification structure of the ingot is homogeneously distributed, and its grain size is obviously refined at ultrasonic power of 240 W. The average grain sizes, which can be seen from the Leica microscope, are less than 100 μm. When the casting speed is 45-50 mm/min, the best grain refinement is obtained. 展开更多
关键词 7050 aluminum alloy ultrasonic power casting speed semi-continuous casting solidification structure
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基于激光超声的低碳钢平均晶粒尺寸无损检测方法 被引量:16
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作者 殷安民 杨荃 +4 位作者 何飞 王晓晨 董锋 王燕龙 束学道 《机械工程学报》 EI CAS CSCD 北大核心 2017年第2期11-19,共9页
采用激光超声非接触检测技术,选用各向异性较小的热轧钢板作为研究对象,通过对标准试样的检测分析对平均晶粒尺寸计算公式进行标定。通过分析完整的激光超声一次回波和二次回波的衰减来计算试样的平均晶粒尺寸,并采用电子背散射衍射技... 采用激光超声非接触检测技术,选用各向异性较小的热轧钢板作为研究对象,通过对标准试样的检测分析对平均晶粒尺寸计算公式进行标定。通过分析完整的激光超声一次回波和二次回波的衰减来计算试样的平均晶粒尺寸,并采用电子背散射衍射技术对平均晶粒尺寸检测的结果来验证计算的准确性。针对在实际测量中超声波信号会受到设备稳定性、试样表面状态、检测环境的变化和试样内部组织的不均匀性等的影响,提出利用超声回波时域信号能量衰减来计算衰减系数的方法,即能量衰减特性分析方法,可以有效地提高平均晶粒尺寸的计算精度。 展开更多
关键词 激光超声 平均晶粒尺寸 低碳钢板 能量衰减法
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Microstructure refinement of AZ31 alloy solidified with pulsed magnetic field 被引量:14
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作者 汪彬 杨院生 孙明礼 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2010年第9期1685-1690,共6页
The effects of a pulsed magnetic field on the solidified microstructure of an AZ31 magnesium alloy were investigated.The experimental results show that the remarkable microstructural refinement is achieved when the pu... The effects of a pulsed magnetic field on the solidified microstructure of an AZ31 magnesium alloy were investigated.The experimental results show that the remarkable microstructural refinement is achieved when the pulsed magnetic field is applied to the solidification of the AZ31 alloy.The average grain size of the as-cast microstructure of the AZ31 alloy is refined to 107 μm.By quenching the AZ31 alloy, the different primary α-Mg microstructures are preserved during the course of solidification.The microstructure evolution reveals that the primary α-Mg generates and grows in globular shape with pulsed magnetic field, contrast with the dendritic shape without pulsed magnetic field.The pulsed magnetic field causes melt convection during solidification, which makes the temperature of the whole melt homogenized, and produces an undercooling zone in front of the liquid/solid interface, which makes the nucleation rate increased and big dendrites prohibited.In addition, the Joule heat effect induced in the melt also strengthens the grain refinement effect and spheroidization of dendrite arms. 展开更多
关键词 AZ31 magnesium alloy grain refinement pulsed magnetic field solidified microstructure
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Simulation of electromagnetic-flow fields in Mg melt under pulsed magnetic field 被引量:14
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作者 汪彬 杨院生 +1 位作者 马晓平 童文辉 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2010年第2期283-288,共6页
The effects of a pulsed magnetic field on the solidified microstructure of pure Mg were investigated.The results show that microstructure of pure Mg is considerably refined via columnar-to-equiaxed growth under the pu... The effects of a pulsed magnetic field on the solidified microstructure of pure Mg were investigated.The results show that microstructure of pure Mg is considerably refined via columnar-to-equiaxed growth under the pulsed magnetic field and the average grain size is refined to 260?? under the optimal processing conditions.A mathematical model was built to describe the interaction of the electromagnetic-flow fields during solidification with ANSYS software.The pulsed electric circuit was first solved and then it is substituted into the magnetic field model.The fluid flow model was solved with the acquired electromagnetic force.The effects of pulse voltage frequency on the current wave and on the distribution of magnetic and flow fields were numerically studied.The pulsed magnetic field increases melt convection,which stirs and fractures the dendritic arms into pieces.These broken pieces are transported into the bulk liquid by the liquid flow and act as nuclei to enhance grain refinement.The Joule heat effect produced by the electric current also participates in the microstructural refinement. 展开更多
关键词 pulsed magnetic field numerical simulation pure Mg microstructure refinement
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变形过程中纳米金属镍的微结构演变 被引量:9
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作者 张喜燕 武小雷 +2 位作者 左汝林 夏宝玉 周明哲 《中国有色金属学报》 EI CAS CSCD 北大核心 2005年第10期1607-1611,共5页
利用透射电镜对冷轧变形所致纳米结构金属镍的微结构组织演变特征进行了研究.结果表明,经过轧制变形后,纳米晶的平均晶粒尺寸为50~70 mm,有少量位错结构,但没有发现位错堆积缠结;在晶界处及附近有台阶界面结构,以及与台阶形状相对应的... 利用透射电镜对冷轧变形所致纳米结构金属镍的微结构组织演变特征进行了研究.结果表明,经过轧制变形后,纳米晶的平均晶粒尺寸为50~70 mm,有少量位错结构,但没有发现位错堆积缠结;在晶界处及附近有台阶界面结构,以及与台阶形状相对应的应力场衬度.在变形后期,可以靠晶界发射不全位错从而促使层错生成,并依赖层错尺寸长大(即层错界面位错)的运动进行.而当层错尺寸长大时,其前沿局部变形应力逐渐变大,直至该应力大到一定值时,位错停止运动,层错尺寸也不再长大,并留下了台阶结构. 展开更多
关键词 纳米晶体 微观结构 塑性变形 层错 位错 变形过程 纳米结构 金属镍 结构演变 平均晶粒尺寸
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Characterization of grain growth behaviors by BP-ANN and Sellars models for nickle-base superalloy and their comparisons 被引量:13
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作者 Guo-zheng QUAN Pu ZHANG +3 位作者 Yao-yao MA Yu-qing ZHANG Chao-long LU Wei-yong WANG 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2020年第9期2435-2448,共14页
In order to deeply understand the grain growth behaviors of Ni80A superalloy,a series of grain growth experiments were conducted at holding temperatures ranging from 1223 to 1423 K and holding time ranging from 0 to 3... In order to deeply understand the grain growth behaviors of Ni80A superalloy,a series of grain growth experiments were conducted at holding temperatures ranging from 1223 to 1423 K and holding time ranging from 0 to 3600 s.A back-propagation artificial neural network(BP-ANN)model and a Sellars model were solved based on the experimental data.The prediction and generalization capabilities of these two models were evaluated and compared on the basis of four statistical indicators.The results show that the solved BP-ANN model has better performance as it has higher correlation coefficient(r),lower average absolute relative error(AARE),lower absolute values of mean value(μ)and standard deviation(ω).Eventually,a response surface of average grain size to holding temperature and holding time is constructed based on the data expanded by the solved BP-ANN model,and the grain growth behaviors are described. 展开更多
关键词 grain growth model BP artificial neural network Sellars model average grain size
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微合金元素对Q345钢奥氏体晶粒粗化行为的影响 被引量:9
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作者 刘胜新 陈永 +3 位作者 赵志毅 薛润东 李杏娥 范金辉 《铸造技术》 EI CAS 北大核心 2006年第10期1071-1074,共4页
研究了单独与复合添加V/Nb/Al元素对Q345钢奥氏体晶粒长大行为的影响规律。以ASTM晶粒度级别等于6.0定义实验用钢的实用奥氏体晶粒粗化温度。结果表明:和Fe-V处理相比,以VN12进行微合金化可使Q345钢的奥体氏晶粒粗化温度提高约40℃;和Fe... 研究了单独与复合添加V/Nb/Al元素对Q345钢奥氏体晶粒长大行为的影响规律。以ASTM晶粒度级别等于6.0定义实验用钢的实用奥氏体晶粒粗化温度。结果表明:和Fe-V处理相比,以VN12进行微合金化可使Q345钢的奥体氏晶粒粗化温度提高约40℃;和Fe-Nb处理相比,Nb和V复合加入对Q345钢晶粒粗化温度无显著影响;Al微合金化Q345钢中复合添加微量Nb对其晶粒粗化温度无明显影响。Nb、V、Al的抗奥氏体晶粒粗化能力依次为:Nb>Al>V。 展开更多
关键词 奥氏体粗化温度 平均晶粒尺寸 微合金钢 Q345
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纳米粒子的平均晶粒尺寸和晶格畸变的同时测定 被引量:3
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作者 刘建路 张其春 林金辉 《现代技术陶瓷》 CAS 2002年第1期34-38,共5页
本文使用积分宽度法同时确定了纳米CeO_2粒子的平均晶粒尺寸和晶格畸变率,讨论了使用X射线衍射数据同时计算纳米粒子的平均晶粒尺寸和晶格畸变的方法,以及应用Gaussian/Cauchy型方程进行数据处理的具体细节。研究结果说明,当计算纳米微... 本文使用积分宽度法同时确定了纳米CeO_2粒子的平均晶粒尺寸和晶格畸变率,讨论了使用X射线衍射数据同时计算纳米粒子的平均晶粒尺寸和晶格畸变的方法,以及应用Gaussian/Cauchy型方程进行数据处理的具体细节。研究结果说明,当计算纳米微晶的晶格畸变时,现有的一些简单计算方法可能使计算出来的晶格畸变值严重失实。 展开更多
关键词 纳米粒子 平均晶粒尺寸 晶格畸变 同时测定 X-射线衍射 积分宽度法
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3003铝合金动态再结晶实验研究 被引量:11
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作者 陈贵清 傅高升 +2 位作者 颜文煅 程超增 邹泽昌 《材料工程》 EI CAS CSCD 北大核心 2011年第8期77-81,共5页
采用Gleeble-1500热模拟试验机对3003铝合金进行变形温度为300~500℃、应变速率为0.01~10.0s-1的高温等温压缩实验,由真应力-真应变曲线计算应变硬化速率,并采用截线法测量热压缩后平均晶粒尺寸,结果表明:3003铝合金动态再结晶临界应... 采用Gleeble-1500热模拟试验机对3003铝合金进行变形温度为300~500℃、应变速率为0.01~10.0s-1的高温等温压缩实验,由真应力-真应变曲线计算应变硬化速率,并采用截线法测量热压缩后平均晶粒尺寸,结果表明:3003铝合金动态再结晶临界应变εc随着Z参数的增大而提高,合金发生动态再结晶的临界条件为:ε>εc=7.28×10-5 Z0.1661;动态再结晶的平均晶粒尺寸随温度的升高、应变速率的减小而增大,其关系为:lndave=-0.0824lnZ+4.9532;在实验条件下,该合金具有正的应变速率敏感性,随变形温度的降低和应变速率的增大,合金进入稳态流变阶段时所对应的真应力值逐渐增大,并且峰值应力随动态再结晶平均晶粒尺寸的减小而增大,符合Hall-Petch关系:lnσm=-0.9378lndave+6.5232。 展开更多
关键词 3003铝合金 应变硬化速率 动态再结晶 临界应变 平均晶粒尺寸
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X射线衍射法测定纳米氧化铝的平均晶粒尺寸 被引量:10
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作者 王雷雷 王勤隆 +1 位作者 李晶 黄长荣 《无机盐工业》 CAS CSCD 北大核心 2021年第4期86-89,共4页
以六硼化镧粉末作为标准样品,根据衍射拟合结果分离出任意角度下的仪器宽化值。对焙烧后的氧化铝样品进行X射线衍射分析,结果表明该氧化铝样品为α晶型结构。对样品因素(晶粒细化、微观应变)引起的宽化值分别使用高斯分布法和Hall法进... 以六硼化镧粉末作为标准样品,根据衍射拟合结果分离出任意角度下的仪器宽化值。对焙烧后的氧化铝样品进行X射线衍射分析,结果表明该氧化铝样品为α晶型结构。对样品因素(晶粒细化、微观应变)引起的宽化值分别使用高斯分布法和Hall法进行拟合,计算出氧化铝样品的平均晶粒尺寸。将计算结果与谢乐公式计算出的各晶面晶粒尺寸值进行对比,表明Hall法测试平均晶粒尺寸更加准确,衍射峰晶粒细化和微观应变引起的宽化函数遵循柯西函数关系,确认该氧化铝样品的平均晶粒尺寸为155 nm。 展开更多
关键词 X射线衍射 纳米氧化铝 平均晶粒尺寸 高斯分布法 Hall法
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纳米TiO_2的制备与表征 被引量:7
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作者 胡永茂 项金钟 +3 位作者 李茂琼 方静华 张学清 吴兴惠 《中国陶瓷》 CAS CSCD 2002年第5期19-21,共3页
通过金属醇盐水解制备了纳米TiO2 颗粒 ,用XRD、TEM、ICP等方法进行了分析与表征 ,给出了相关的工艺参数。实验结果表明 ,通过控制溶液的pH值和水解用水量 。
关键词 溶胶—凝胶法 纳米二氧化钛 平均晶粒尺寸 金属醇盐水解法 工艺参数
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Tensile properties and microstructure of AZ31B magnesium alloy sheet processed by repeated unidirectional bending 被引量:10
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作者 黄光胜 李红成 +1 位作者 宋波 张雷 《中国有色金属学会会刊:英文版》 CSCD 2010年第1期28-33,共6页
The mechanical properties of the AZ31B magnesium alloy sheet processed by repeated unidirectional bending (RUB) with a basal pole tilted in the rolling direction were systematically investigated at different temperatu... The mechanical properties of the AZ31B magnesium alloy sheet processed by repeated unidirectional bending (RUB) with a basal pole tilted in the rolling direction were systematically investigated at different temperatures. Compared with the as-received sheet exhibiting approximately the same average grain size, the fracture elongation increased while the proof stress decreased at room temperature. The initial texture had a significant influence on the mechanical properties at room temperature, while it showed a much weaker effect on the mechanical properties because of the activation of non-basal slips and initiation of dynamic recrystallization during deformation at elevated temperature. 展开更多
关键词 AZ31B镁合金 弯曲加工 单向弯曲 微观结构 拉伸性能 板材 室温力学性能 平均晶粒尺寸
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Reconstruction of flood events over the last 150 years in the lower reaches of the Changjiang River 被引量:9
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作者 ZHAN Wang YANG ShouYe +2 位作者 LIU XiaoLi LI JianWei CHOI ManSik 《Chinese Science Bulletin》 SCIE EI CAS 2010年第21期2268-2274,共7页
The reconstruction of paleofloods in the Holocene has become one research highlight for the present global change study.The core sediments from one newly-emerged bar in the lower Changjiang River(Yangtze River)mainstr... The reconstruction of paleofloods in the Holocene has become one research highlight for the present global change study.The core sediments from one newly-emerged bar in the lower Changjiang River(Yangtze River)mainstream were collected for grain size and organic elemental measurements,with aim to reconstruct the flood events over the past 150 years.Major grain size parameters such as mean grain size,probability cumulative curve and C-M diagram of the core sediments clearly indicate the flood event deposition.Furthermore,the TOC/TN ratios in the sediments can indicate flood events considering that during the flash floods,strong surface erosion in the upper and lower reaches of the Changjiang River can transport a large amount of undecomposed plant debris and organic components with relatively low C/N ratios into the lower mainstream.Based on 210Pb dating and sedimentary geochemical results,the research profile recorded several large floods happened from 1850 to 1954,which agrees well with the historical documents and hydrological observations.Interesting to note that the flood events since the 1960s cannot be distinctly recognized on the basis of sediment grain size and organic elemental compositions of the profile,which mainly reflects the intensive human activities over the last fifty years,especially condense dam construction,have significantly changed the characters of suspended sediment into the lower mainstream. 展开更多
关键词 洪水事件 长江下游 柱状沉积物 地球化学测量 平均晶粒尺寸 概率累积曲线 地表侵蚀 长江中下游
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超声辐射沉淀法制备纳米γ-MnO_2的研究 被引量:8
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作者 李东升 王尧宇 +2 位作者 刘萍 王文亮 史启祯 《无机化学学报》 SCIE CAS CSCD 北大核心 2005年第2期202-206,共5页
以KMnO4和MnSO4·H2O为原料,采用超声辐射沉淀法制备出纳米γ-MnO2粉体,研究了反应物浓度、滴速、超声时间及超声功率等合成条件对粉体的影响,得出了最佳工艺条件。ICP、XRD和TEM分析表明,施加超声辐射对反应体系有显著影响,超声辐... 以KMnO4和MnSO4·H2O为原料,采用超声辐射沉淀法制备出纳米γ-MnO2粉体,研究了反应物浓度、滴速、超声时间及超声功率等合成条件对粉体的影响,得出了最佳工艺条件。ICP、XRD和TEM分析表明,施加超声辐射对反应体系有显著影响,超声辐射沉淀法获得了含K量极低,分布均匀,平均晶粒尺寸约10nm的近球形γ-MnO2粉体,而未施加超声辐射的普通沉淀法却得到了棒状KMn8O16粉体。XPS与IR分析表明,两种方法所得粉体中Mn主要以+4价形式存在,而前者具有较多的氧缺位,由于K+进入了确定的晶格位置使后者的Mn-O键红外吸收峰明显不同于前者。 展开更多
关键词 粉体 沉淀法 MNO2 超声辐射 氧缺位 制备 纳米 晶格 IR分析 平均晶粒尺寸
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Sedimentation processes and sedimentary characteristics of tidal bores along the north bank of the Qiantang Estuary 被引量:9
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作者 FAN DaiDux CAI GuoFu +3 位作者 SHANG Shuai WU YiJing ZHANG YanWei GAO Lei 《Chinese Science Bulletin》 SCIE CAS 2012年第13期1578-1589,共12页
A tidal bore is a unique Earth surface process, characterized by its highly destructive energy, predictable periodicities and magni-tudes, and the production of characteristic sedimentary features. Tidal bores and ass... A tidal bore is a unique Earth surface process, characterized by its highly destructive energy, predictable periodicities and magni-tudes, and the production of characteristic sedimentary features. Tidal bores and associated rapid flood flows are highly turbulent flows of the upper-flow regime with a velocity over several meters per second. Reynolds (Re) and Froude (Fr) numbers, respectively, are larger than 104 and 1.0, making them significantly different from regular tidal flows but analogous to turbidity currents. Until now, understanding of tidal-bore depositional processes and products has been limited because of the difficulty and hazards involved with gauging tidal bores directly. The Qiantang bore is known as the largest breaking bore in the world. Field surveys were carried out in May 2010, along the north bank of the Qiantang Estuary to observe the occurrence of peak bores, including regular observations of current, water level and turbidity at the main channel. Several short cores were sampled on the intertidal flats to study the characteristic sedimentary features of tidal bores. Hydrodynamic and sedimentological studies show that the processes of sediment resuspension, transport and deposition are controlled primarily by the tidal bores, and the subsequent abruptly accelerated and decelerated flood flows, which only account for one tenth of each semidiurnal tidal cycle in the estuary. Tidal-bore deposits are generally poorly sorted because of rapid sedimentation after highly mixed suspension by intense turbulence. This behavior is characteristic of the absence of tractive-current depositional components in a C-M diagram. It also goes along with well-developed massive bedding, graded bedding, basal erosion structures, convolute bedding and dewatering structures. Together, these sedimentary features can constitute fingerprinting of turbidites, widely distributed in the deep-water environment. However, a tidal bore is triggered by intensely deformed tidal waves propagating into a shallow-water environme 展开更多
关键词 钱塘江河口 沉积特征 沉积过程 战区导弹防御系统 沉积物再悬浮 平均晶粒尺寸 洪水流量 床上用品
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a-Si:H薄膜固相晶化法制备大晶粒多晶硅薄膜 被引量:7
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作者 吴萍 姚若河 +1 位作者 林璇英 余楚迎 《汕头大学学报(自然科学版)》 1999年第1期19-23,共5页
用等离子体化学气相沉积(PCVD)法制备:a-Si:N薄膜材料(衬底温度20O℃~350℃),用固相晶化法(SPC)获得多晶硅薄膜(退火温度500℃~650℃),用X射线衍射法测得平均晶粒尺寸依赖于退火温度和沉积条件,随着沉积温度的降低需要... 用等离子体化学气相沉积(PCVD)法制备:a-Si:N薄膜材料(衬底温度20O℃~350℃),用固相晶化法(SPC)获得多晶硅薄膜(退火温度500℃~650℃),用X射线衍射法测得平均晶粒尺寸依赖于退火温度和沉积条件,随着沉积温度的降低需要较高的退火温度,用SEM观测形貌测得平均晶粒大小为1,0~1。 展开更多
关键词 固相晶化法 平均晶粒尺寸 多晶硅 薄膜 PVCD
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用脉冲喷射电沉积法制备纳米晶镍镀层 被引量:8
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作者 江山 潘勇 +1 位作者 唐甜 周益春 《材料保护》 CAS CSCD 北大核心 2007年第3期49-51,64,共4页
采用脉冲喷射电沉积方法制备了纳米晶镍镀层,用扫描电子显微镜(SEM)、透射电子显微镜(TEM)和X射线衍射(XRD)等方法研究了镀层的生长形貌和微观结构,并考察了脉冲电流密度对镀层微观结构如晶粒尺寸、织构等的影响。结果表明:镀层内表面(... 采用脉冲喷射电沉积方法制备了纳米晶镍镀层,用扫描电子显微镜(SEM)、透射电子显微镜(TEM)和X射线衍射(XRD)等方法研究了镀层的生长形貌和微观结构,并考察了脉冲电流密度对镀层微观结构如晶粒尺寸、织构等的影响。结果表明:镀层内表面(基体一侧)具有比外表面(镀液一侧)更为精细的晶粒结构,说明随着厚度的增加,镀层中的晶粒逐渐粗化。随着电流密度从45A/dm2增加到180A/dm2,镀层中晶粒生长的择优取向由(111)织构逐渐转变为强(220)织构。当电流密度从45A/dm2增加到120A/dm2时,镀层平均晶粒尺寸逐渐减小;而进一步增加电流密度到180A/dm2,镀层晶粒尺寸又会有轻微的增大。 展开更多
关键词 脉冲喷射电沉积 纳米晶镍镀层 微观结构 织构 平均晶粒尺寸
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TiO2 nanoparticles prepared by sol-gel 被引量:8
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作者 Adnan Saleh Fadhil Abd Rasin Majida Ali Ameen 《材料科学与工程(中英文版)》 2009年第12期81-84,共4页
关键词 纳米二氧化钛 溶胶凝胶法 制备 平均晶粒尺寸 二氧化钛凝胶 二氧化钛颗粒 激光放大器 激光反射镜
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Complex Permittivity and Microwave Absorbing Property of Si_3N_4-SiC Composite Ceramic 被引量:8
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作者 Cuopeng Zheng Xiaowei Yin +2 位作者 Jie Wang Mengluo Cuo Xi Wang 《Journal of Materials Science & Technology》 SCIE EI CAS CSCD 2012年第8期745-750,共6页
Si3N4-SiC composite ceramics were fabricated by chemical vapor infiltration using porous Si3Na ceramic as preform. The average grain size of SiC was 30 nm. Relationship between SiC content and relative complex permitt... Si3N4-SiC composite ceramics were fabricated by chemical vapor infiltration using porous Si3Na ceramic as preform. The average grain size of SiC was 30 nm. Relationship between SiC content and relative complex permittivity of Si3Na-SiC within the frequency range of 8.2-12.4 GHz (X-band) was investigated. The average real part of relative complex permittivity ε′ of Si3N4-SiC increased from 3.7 to 14.9 and the relative imaginary part ε″ increased from 0.017 to 13.4 when the content of SiC increased from 0 to 10 vol.%. The Si3N4-SiC ceramic with 3 vol.% SiC achieved a reflection loss below -10 dB (90% absorption) at 8.0-11.4 GHz, and the minimum value was -27.1 dB at 9.8 GHz when the sample thickness was 2.5 mm. The excellent microwave absorbing abilities of Si3N4-SiC ceramic were attributed to the interfacial polarization at interface between Si3N4 and SiC and at grain boundary between SiC nanocrystals. 展开更多
关键词 SIC SI3N4 Dielectric properties Reflection loss
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