A new method of constant-wavelength synchronous fluorescence spectrometry for simultaneous determination of Sudan Ⅱand Sudan Ⅲ was developed with using their fluorescence phenomenon.Only one single scan is needed fo...A new method of constant-wavelength synchronous fluorescence spectrometry for simultaneous determination of Sudan Ⅱand Sudan Ⅲ was developed with using their fluorescence phenomenon.Only one single scan is needed for effective identification and quantitative determination of the two compounds simultaneously when Δλ=60 nm is chosen.The linear ranges for Sudan Ⅱ and Sudan Ⅲ were 0—3.3 and 0—2.8 μg/mL,respectively.The detection limits for Sudan Ⅱ and Sudan Ⅲ were 14 and 11 ng/mL,respectively.By using this method,Sudan Ⅱand Ⅲ in sausage samples were determined directly with the recoveries of 83.8%—109.5%.展开更多
An optimal synchronous trajectory tracking controller was developed for multi-axis systems. The position synchronization error on each axis was defined as the position difference between this axis and the following ax...An optimal synchronous trajectory tracking controller was developed for multi-axis systems. The position synchronization error on each axis was defined as the position difference between this axis and the following axes. The following error of each axis, the synchronization error, and its derivative were considered in the cost function. A Riccati equation was deduced from the Hamilton-Pontryagin equation. The optimal control law was set up from the Riccati equation solution. Simulations of a two-axis system show that the synchronization error can be significantly reduced and the synchronization performance can be adjusted based on the parameters in the cost function.展开更多
文摘A new method of constant-wavelength synchronous fluorescence spectrometry for simultaneous determination of Sudan Ⅱand Sudan Ⅲ was developed with using their fluorescence phenomenon.Only one single scan is needed for effective identification and quantitative determination of the two compounds simultaneously when Δλ=60 nm is chosen.The linear ranges for Sudan Ⅱ and Sudan Ⅲ were 0—3.3 and 0—2.8 μg/mL,respectively.The detection limits for Sudan Ⅱ and Sudan Ⅲ were 14 and 11 ng/mL,respectively.By using this method,Sudan Ⅱand Ⅲ in sausage samples were determined directly with the recoveries of 83.8%—109.5%.
基金Supported by the National Natural Science Foundation of China(No. 50577037)
文摘An optimal synchronous trajectory tracking controller was developed for multi-axis systems. The position synchronization error on each axis was defined as the position difference between this axis and the following axes. The following error of each axis, the synchronization error, and its derivative were considered in the cost function. A Riccati equation was deduced from the Hamilton-Pontryagin equation. The optimal control law was set up from the Riccati equation solution. Simulations of a two-axis system show that the synchronization error can be significantly reduced and the synchronization performance can be adjusted based on the parameters in the cost function.