Stress relaxation behavior of two turbine bolt steels was evaluated by the manual-controlled tensile stress relaxation test (TSRT) at high temperature. First, feasibility and the procedure of the manual-controlled ten...Stress relaxation behavior of two turbine bolt steels was evaluated by the manual-controlled tensile stress relaxation test (TSRT) at high temperature. First, feasibility and the procedure of the manual-controlled tensile stress relaxation test (TSRT) is discussed and carried out on a general creep testing machine. And then, the experimental results from such type of test were compared to the existing data provided by certain Laboratory U.K. Overall good agreement between the results of manual-controlled TSRT method and the existing data provides confidence in the use of the proposed method in practice. Finally, the experimental results of turbine bolt steels from TSRT were compared with that of bending test. It is observed that great difference exists between the results from two different type stress relaxation tests. It is therefore suggested that the results from TSRT method be adopted in turbine bolt design in engineering.展开更多
In order to extend the application of epoxy vitrimer, 1,4-cyclohexanedicarboxylic acid（CHDA） was used as a co-curing agent and structure modifier for sebacic acid（SA） cured diglycidyl ether of bisphenol A（DGEBA）...In order to extend the application of epoxy vitrimer, 1,4-cyclohexanedicarboxylic acid（CHDA） was used as a co-curing agent and structure modifier for sebacic acid（SA） cured diglycidyl ether of bisphenol A（DGEBA） epoxy vitrimer to tailor the mechanical properties of epoxy vitrimers with 1,5,7-triazabicylo[4.4.0]dec-5-ene（TBD） as a transesterification catalyst. The glass transition temperature（Tg） of vitrimer increased gradually with the increase in CHDA content. Vitrimers behaved from elastomer to tough and hard plastics were successfully achieved by varying the feed ratio of CHDA to SA. Both the Young＇s modulus and storage modulus increased apparently with the increase in CHDA content. Stress relaxation measurement indicated that more prominent stress relaxation occurred at elevated temperatures and the stress relaxation decreased with the increase of CHDA content due to the reduced mobility of the vitrimer backbone. The vitrimers showed excellent recyclability as evidenced by the unchanged gel fraction and mechanical properties after compression molded for several times. With tunable mechanical properties, the epoxy vitrimers may find extensive potential applications.展开更多
Surimi gel was made from silver carp(hypophthalmichthys molitrix).Texture analyzer was adopted to measure stress-relaxation curve to study the effects of water,Na+ and Ca2+ on relaxation properties of surimi gel,so as...Surimi gel was made from silver carp(hypophthalmichthys molitrix).Texture analyzer was adopted to measure stress-relaxation curve to study the effects of water,Na+ and Ca2+ on relaxation properties of surimi gel,so as to provide the basic data for development of surimi gel products.Micromodel of gel based on continuous phase of protein network with water embed and dispersed phase of myofibril was established.Stress-relaxation properties of the gel were imitated by use of five-element relaxation mathematical model,with high fitted precision.The results show that addition of water can reduce hardness of gel;Na+ and Ca2+ can improve the viscoelasticity of gel.展开更多
文摘Stress relaxation behavior of two turbine bolt steels was evaluated by the manual-controlled tensile stress relaxation test (TSRT) at high temperature. First, feasibility and the procedure of the manual-controlled tensile stress relaxation test (TSRT) is discussed and carried out on a general creep testing machine. And then, the experimental results from such type of test were compared to the existing data provided by certain Laboratory U.K. Overall good agreement between the results of manual-controlled TSRT method and the existing data provides confidence in the use of the proposed method in practice. Finally, the experimental results of turbine bolt steels from TSRT were compared with that of bending test. It is observed that great difference exists between the results from two different type stress relaxation tests. It is therefore suggested that the results from TSRT method be adopted in turbine bolt design in engineering.
基金financially supported by the National Natural Science Foundation of China (No.51703188)Fundamental Research Funds for the Central Universities (Nos.XDJK2017A016 and XDJK2017C022)
文摘In order to extend the application of epoxy vitrimer, 1,4-cyclohexanedicarboxylic acid（CHDA） was used as a co-curing agent and structure modifier for sebacic acid（SA） cured diglycidyl ether of bisphenol A（DGEBA） epoxy vitrimer to tailor the mechanical properties of epoxy vitrimers with 1,5,7-triazabicylo[4.4.0]dec-5-ene（TBD） as a transesterification catalyst. The glass transition temperature（Tg） of vitrimer increased gradually with the increase in CHDA content. Vitrimers behaved from elastomer to tough and hard plastics were successfully achieved by varying the feed ratio of CHDA to SA. Both the Young＇s modulus and storage modulus increased apparently with the increase in CHDA content. Stress relaxation measurement indicated that more prominent stress relaxation occurred at elevated temperatures and the stress relaxation decreased with the increase of CHDA content due to the reduced mobility of the vitrimer backbone. The vitrimers showed excellent recyclability as evidenced by the unchanged gel fraction and mechanical properties after compression molded for several times. With tunable mechanical properties, the epoxy vitrimers may find extensive potential applications.
基金Projects(2006BAD05A18) supported by National Key Technology R & D Program during the 11th Five-Year Plan PeriodProject(2007ABA350) supported by the Natural Science Foundation of Hubei Province
文摘Surimi gel was made from silver carp(hypophthalmichthys molitrix).Texture analyzer was adopted to measure stress-relaxation curve to study the effects of water,Na+ and Ca2+ on relaxation properties of surimi gel,so as to provide the basic data for development of surimi gel products.Micromodel of gel based on continuous phase of protein network with water embed and dispersed phase of myofibril was established.Stress-relaxation properties of the gel were imitated by use of five-element relaxation mathematical model,with high fitted precision.The results show that addition of water can reduce hardness of gel;Na+ and Ca2+ can improve the viscoelasticity of gel.
