An innovative application of laser ablation inductively coupled plasma mass spectrometry （LA-ICP-MS） technique in illustrating elemental distributions on stainless steel sheets was presented. The technique proved to...An innovative application of laser ablation inductively coupled plasma mass spectrometry （LA-ICP-MS） technique in illustrating elemental distributions on stainless steel sheets was presented. The technique proved to be a systematic and accurate ap- proach in producing visual images or maps of elemental distributions at cross-sectional surface of a stainless steel sheet. Two stain- less steel sheets served as research objects： 3 mm×l 300 mm hot-rolled stainless steel plate and 1 mm×l 260 mm cold-rolled plate. The cross-sectional surfaces of the two samples at 1/4 position along the width direction were scanned （raster area -44 mm2 and 11 mm2） with a focused laser beam （wavelength 213 nm, diameter of laser crater 100 μm, and laser power 1.6 mJ） in a laser abla- tion chamber. The laser ablation system was coupled to a quadrupole ICP-MS, which made the detection of ion intensities of 27A1＋, 44Ca＋, 47Ti-, 55Mn＋ and 56Fe＋ within an area of interest possible. One-dimensional （ID） content line distribution maps and two- dimensional （2D） contour maps for specific positions or areas were plotted to indicate the element distribution of a target area with high accuracy. Statistic method was used to analyze the acquired data by calculating median contents, maximum segregation, sta- tistic segregation and content-frequency distribution.展开更多
研究车体用2 mm不锈钢材料X2Cr Ni N18-7及其焊接薄板通过火焰调修后的力学性能。采用低温、中温和高温三种温度分别对不锈钢母材、焊接钢板的焊缝进行火焰调修,获得了调修温度对母材、焊缝以及调修后焊缝的屈服强度、抗拉强度、延伸率...研究车体用2 mm不锈钢材料X2Cr Ni N18-7及其焊接薄板通过火焰调修后的力学性能。采用低温、中温和高温三种温度分别对不锈钢母材、焊接钢板的焊缝进行火焰调修,获得了调修温度对母材、焊缝以及调修后焊缝的屈服强度、抗拉强度、延伸率和硬度的影响规律。结果表明:采用较高温度火焰调修能够获得焊缝区域屈服强度524 MPa、抗拉强度760 MPa和延伸率22.0%,性能良好。火焰调修能够提高焊缝及熔合区的硬度,但调修温度在450℃~850℃之间时,调修温度对硬度的影响并不显著。展开更多
基金Sponsored by National Major Instrument and Equipment Development Special Project of China(2011YQ14014710)
文摘An innovative application of laser ablation inductively coupled plasma mass spectrometry （LA-ICP-MS） technique in illustrating elemental distributions on stainless steel sheets was presented. The technique proved to be a systematic and accurate ap- proach in producing visual images or maps of elemental distributions at cross-sectional surface of a stainless steel sheet. Two stain- less steel sheets served as research objects： 3 mm×l 300 mm hot-rolled stainless steel plate and 1 mm×l 260 mm cold-rolled plate. The cross-sectional surfaces of the two samples at 1/4 position along the width direction were scanned （raster area -44 mm2 and 11 mm2） with a focused laser beam （wavelength 213 nm, diameter of laser crater 100 μm, and laser power 1.6 mJ） in a laser abla- tion chamber. The laser ablation system was coupled to a quadrupole ICP-MS, which made the detection of ion intensities of 27A1＋, 44Ca＋, 47Ti-, 55Mn＋ and 56Fe＋ within an area of interest possible. One-dimensional （ID） content line distribution maps and two- dimensional （2D） contour maps for specific positions or areas were plotted to indicate the element distribution of a target area with high accuracy. Statistic method was used to analyze the acquired data by calculating median contents, maximum segregation, sta- tistic segregation and content-frequency distribution.
