The molecular weight of acrylonitrile/itaconic acid copolymer can be calculated from the intrinsic viscosities of the dilute reaction solutions directly, when the conversion was higher than 90% during the solution pol...The molecular weight of acrylonitrile/itaconic acid copolymer can be calculated from the intrinsic viscosities of the dilute reaction solutions directly, when the conversion was higher than 90% during the solution polymerization. Because of the sample treatment processes such as film preparing, washing, drying and redissolving were simplified, the analysis time was reduced substantially. The proposed method is more suitable for rapid analysis. The measurement error compared with common method of determination for the copolymer in DMSO by single point method was about 1%.展开更多
文摘The molecular weight of acrylonitrile/itaconic acid copolymer can be calculated from the intrinsic viscosities of the dilute reaction solutions directly, when the conversion was higher than 90% during the solution polymerization. Because of the sample treatment processes such as film preparing, washing, drying and redissolving were simplified, the analysis time was reduced substantially. The proposed method is more suitable for rapid analysis. The measurement error compared with common method of determination for the copolymer in DMSO by single point method was about 1%.