页岩基质孔隙主要包含有机孔隙和无机孔隙,页岩油气在有机孔隙和无机孔隙中的渗流机理不同,对页岩中有机孔隙和无机孔隙的微观结构进行定量表征具有重要意义.首先通过扫描电子显微镜(scanning electron microscope,简称SEM)实验分别获...页岩基质孔隙主要包含有机孔隙和无机孔隙,页岩油气在有机孔隙和无机孔隙中的渗流机理不同,对页岩中有机孔隙和无机孔隙的微观结构进行定量表征具有重要意义.首先通过扫描电子显微镜(scanning electron microscope,简称SEM)实验分别获取具有代表性的页岩无机孔隙和有机孔隙扫描电镜图像,其中,无机孔隙相对较大,其图像的分辨率较低,有机孔隙相对较小,其图像的分辨率较高;然后,通过图像处理和马尔可夫链蒙特卡洛(Markov chain Monte Carlo,简称MCMC)法重构出相应的无机孔隙数字岩心和有机孔隙数字岩心,并提出局部叠加法构建同时包含无机孔隙和有机孔隙的页岩基质孔隙数字岩心;最后对无机孔隙数字岩心、有机孔隙数字岩心和基质孔隙数字岩心的结构特征进行了对比分析.结果表明,局部叠加法构建的页岩基质孔隙数字岩心能够同时描述页岩中的无机孔隙和有机孔隙结构特征,无机孔隙本身连通性较差,有机孔隙本身连通性较好,有机孔隙的局部孔隙度和局部渗透率较高,对页岩中的流体渗流有着重要作用.该方法为页岩中不同的孔隙结构特征描述和油气在纳米尺度孔隙中的传输模拟提供了一个可靠的研究平台.展开更多
For understanding the rock microscopic damage and dynamic mechanical properties subjected to recurrent freeze-thaw cycles, experiments for five groups of homogeneous sandstone under different freeze-thaw cycles were c...For understanding the rock microscopic damage and dynamic mechanical properties subjected to recurrent freeze-thaw cycles, experiments for five groups of homogeneous sandstone under different freeze-thaw cycles were conducted. After freezethaw, nuclear magnetic resonance(NMR) tests and impact loading tests were carried out, from which microscopic damage characteristics of sandstone and dynamic mechanical parameters were obtained. The results indicate that the porosity increases with the increase of cycle number, the rate of porosity growth descends at the beginning of freeze-thaw, yet accelerates after a certain number of cycles. The proportion of pores with different sizes changes dynamically and the multi-scale distribution of pores tends to develop on pore structure with the continuing impact of freeze-thaw and thawing. Dynamic compressive stress-strain curve of sandstone undergoing freeze-thaw can be divided into four phases, and the phase of compaction is inconspicuous compared with the static curve. Elastic modulus and dynamic peak intensity of sandstone gradually decrease with freeze-thaw cycles, while peak strain increases. The higher the porosity is, the more serious the degradation of dynamic intensity is. The porosity is of a polynomial relationship with the dynamic peak intensity.展开更多
文摘页岩基质孔隙主要包含有机孔隙和无机孔隙,页岩油气在有机孔隙和无机孔隙中的渗流机理不同,对页岩中有机孔隙和无机孔隙的微观结构进行定量表征具有重要意义.首先通过扫描电子显微镜(scanning electron microscope,简称SEM)实验分别获取具有代表性的页岩无机孔隙和有机孔隙扫描电镜图像,其中,无机孔隙相对较大,其图像的分辨率较低,有机孔隙相对较小,其图像的分辨率较高;然后,通过图像处理和马尔可夫链蒙特卡洛(Markov chain Monte Carlo,简称MCMC)法重构出相应的无机孔隙数字岩心和有机孔隙数字岩心,并提出局部叠加法构建同时包含无机孔隙和有机孔隙的页岩基质孔隙数字岩心;最后对无机孔隙数字岩心、有机孔隙数字岩心和基质孔隙数字岩心的结构特征进行了对比分析.结果表明,局部叠加法构建的页岩基质孔隙数字岩心能够同时描述页岩中的无机孔隙和有机孔隙结构特征,无机孔隙本身连通性较差,有机孔隙本身连通性较好,有机孔隙的局部孔隙度和局部渗透率较高,对页岩中的流体渗流有着重要作用.该方法为页岩中不同的孔隙结构特征描述和油气在纳米尺度孔隙中的传输模拟提供了一个可靠的研究平台.
基金Project(2013YQ17046310)supported by the National Key Scientific Instrument and Equipment Development Project of ChinaProject(2013M542138)supported by China Postdoctoral Science FoundationProjects(20130162110010,20130162120012)supported by Specialized Research Fund for the Doctoral Program of Higher Education of China
文摘For understanding the rock microscopic damage and dynamic mechanical properties subjected to recurrent freeze-thaw cycles, experiments for five groups of homogeneous sandstone under different freeze-thaw cycles were conducted. After freezethaw, nuclear magnetic resonance(NMR) tests and impact loading tests were carried out, from which microscopic damage characteristics of sandstone and dynamic mechanical parameters were obtained. The results indicate that the porosity increases with the increase of cycle number, the rate of porosity growth descends at the beginning of freeze-thaw, yet accelerates after a certain number of cycles. The proportion of pores with different sizes changes dynamically and the multi-scale distribution of pores tends to develop on pore structure with the continuing impact of freeze-thaw and thawing. Dynamic compressive stress-strain curve of sandstone undergoing freeze-thaw can be divided into four phases, and the phase of compaction is inconspicuous compared with the static curve. Elastic modulus and dynamic peak intensity of sandstone gradually decrease with freeze-thaw cycles, while peak strain increases. The higher the porosity is, the more serious the degradation of dynamic intensity is. The porosity is of a polynomial relationship with the dynamic peak intensity.
