Chemical fertilizers,such as potash,have a strong tendency to cake when exposed to humidity.In this work,a novel synchrotron-based X-ray tomography 3D-imaging technique was for the first time employed to investigate t...Chemical fertilizers,such as potash,have a strong tendency to cake when exposed to humidity.In this work,a novel synchrotron-based X-ray tomography 3D-imaging technique was for the first time employed to investigate the solid bridge formation from 2D and 3D perspectives.Image processing and a theoretical model were presented to demonstrate recrystallization near contact points between potash particles during a conventional drying process.The effect of initial moisture content on the water activity of surface surrounding the contact points was investigated.The results showed that by increasing the moisture content of particles(3%–5%),the dissolution of sylvite increased and the solid bridge length between potash particles was enlarged from 28μm to 44μm due to supersaturation conditions.In addition,the external porosity of potash particles at the end of drying process decreased from 25.3%to 19.5%for 3%and 5%moisture content,respectively.展开更多
In this paper, a unified internal state variable(ISV) model for predicting microstructure evolution during hot working process of AZ80 magnesium alloy was developed. A novel aspect of the proposed model is that the in...In this paper, a unified internal state variable(ISV) model for predicting microstructure evolution during hot working process of AZ80 magnesium alloy was developed. A novel aspect of the proposed model is that the interactive effects of material hardening, recovery and dynamic recrystallization(DRX) on the characteristic deformation behavior were considered by incorporating the evolution laws of viscoplastic flow, dislocation activities, DRX nucleation and boundary migration in a coupled manner. The model parameters were calibrated based on the experimental data analysis and genetic algorithm(GA) based objective optimization. The predicted flow stress, DRX fraction and average grain size match well with experimental results. The proposed model was embedded in the finite element(FE) software DEFORM-3 D via user defined subroutine to simulate the hot compression and equal channel angular extrusion(ECAE) processes. The heterogeneous microstructure distributions at different deformation zones and the dislocation density evolution with competitive deformation mechanisms were captured.This study can provide a theoretical solution for the hot working problems of magnesium alloy.展开更多
A recrystallization and partial melting(RAP) process was introduced to prepare the semi-solid 7075 aluminum alloy used for thixoforming. In order to obtain an ideal semi-solid microstructure, a series of extrusion exp...A recrystallization and partial melting(RAP) process was introduced to prepare the semi-solid 7075 aluminum alloy used for thixoforming. In order to obtain an ideal semi-solid microstructure, a series of extrusion experiments were conducted to comparatively investigate the optimum extrusion process parameters. Commercial 7075 Al alloy samples were firstly extruded with varying extrusion ratios below the recrystallization temperature followed by homogenization, then these samples were reheated to the semi-solid state and held in the range of 5 to 50 minutes. The experimental results show that varying process cause the difference in the deformation degree and microstructure for as-extruded samples, resulting in various semi-solid microstructure. It is verified that the formation of equiaxed grains in semi-solid microstructure depends on recrystallization behavior of extruded samples during partial melting. Both relative high extrusion temperature and low extrusion ratio lead to high volume fraction of recrystallized area, thus entirely equiaxed solid grains in semi-solid 7075 Al alloy samples can be obtained finally. In addition, Ostwald ripening was determined as the dominate coarsening mechanism of solid grains in semi-solid state for this 7075 Al alloy during the RAP route. The influence of predeformation on recrystallization behavior of this 7075 Al alloy was discussed in detail.展开更多
The control of microstructure during hot rolling process of steel is of great importance and will affect the properties of the steel products.According to the production line,a three-dimensional multi-field coupled fi...The control of microstructure during hot rolling process of steel is of great importance and will affect the properties of the steel products.According to the production line,a three-dimensional multi-field coupled finite element model of 24-pass continuous hot rolling process of 38CrMoAl steel rod is established using the finite element software MSC.Marc.Based on the recrystallization kinetics model and the grain growth model,a subroutine written in Fortran is introduced to calculate the recrystallization behavior and microstructure evolution of 38CrMoAl steel during the entire rolling process.The distribution and evolution of variables such as strain,temperature and recrystallization fractions during the rolling process are analyzed.The temperature variations and grain sizes at both the center and surface of the tested steel are compared with the experimental results.And it is found that the simulation results are in good agreement with the experimental ones,confirming the reliability of the established model.展开更多
The dynamic recrystallization（DRX） behavior of Ti-6Al-2Zr-1Mo-1V alloy was investigated at deformation temperature of 1000-1100 °C and strain rate of 10-3-1.0 s-1 by using compression test.The results show that...The dynamic recrystallization（DRX） behavior of Ti-6Al-2Zr-1Mo-1V alloy was investigated at deformation temperature of 1000-1100 °C and strain rate of 10-3-1.0 s-1 by using compression test.The results show that discontinuous dynamic recrystallization（DDRX） is the predominant recrystallization mechanism at temperature higher than 1050 °C and strain rate lower than 0.01 s-1.Meanwhile,continuous dynamic recrystallization is the main mechanism observed at temperature below 1050 °C and strain rate above 0.01 s-1,mixed with a few DDRX grains.In addition,decreasing strain rate and increasing deformation temperature are found to facilitate the progress of DRX and refinement of grains in the Ti alloy in β forging process.展开更多
文摘Chemical fertilizers,such as potash,have a strong tendency to cake when exposed to humidity.In this work,a novel synchrotron-based X-ray tomography 3D-imaging technique was for the first time employed to investigate the solid bridge formation from 2D and 3D perspectives.Image processing and a theoretical model were presented to demonstrate recrystallization near contact points between potash particles during a conventional drying process.The effect of initial moisture content on the water activity of surface surrounding the contact points was investigated.The results showed that by increasing the moisture content of particles(3%–5%),the dissolution of sylvite increased and the solid bridge length between potash particles was enlarged from 28μm to 44μm due to supersaturation conditions.In addition,the external porosity of potash particles at the end of drying process decreased from 25.3%to 19.5%for 3%and 5%moisture content,respectively.
基金funding supported by National Natural Science Foundation of China(No.52175285)Beijing Municipal Natural Science Foundation(No.3182025)+1 种基金National Defense Science and Technology Rapid support Project(No.61409230113)Scientific and Technological Innovation Foundation of Shunde Graduate School,USTB and Fundamental Research Funds for the Central Universities(No.FRFBD-20-08A,FRF-TP-20-009A2)。
文摘In this paper, a unified internal state variable(ISV) model for predicting microstructure evolution during hot working process of AZ80 magnesium alloy was developed. A novel aspect of the proposed model is that the interactive effects of material hardening, recovery and dynamic recrystallization(DRX) on the characteristic deformation behavior were considered by incorporating the evolution laws of viscoplastic flow, dislocation activities, DRX nucleation and boundary migration in a coupled manner. The model parameters were calibrated based on the experimental data analysis and genetic algorithm(GA) based objective optimization. The predicted flow stress, DRX fraction and average grain size match well with experimental results. The proposed model was embedded in the finite element(FE) software DEFORM-3 D via user defined subroutine to simulate the hot compression and equal channel angular extrusion(ECAE) processes. The heterogeneous microstructure distributions at different deformation zones and the dislocation density evolution with competitive deformation mechanisms were captured.This study can provide a theoretical solution for the hot working problems of magnesium alloy.
基金Funded by the National Natural Science Foundation of China(Nos.51774054 and 51974050)
文摘A recrystallization and partial melting(RAP) process was introduced to prepare the semi-solid 7075 aluminum alloy used for thixoforming. In order to obtain an ideal semi-solid microstructure, a series of extrusion experiments were conducted to comparatively investigate the optimum extrusion process parameters. Commercial 7075 Al alloy samples were firstly extruded with varying extrusion ratios below the recrystallization temperature followed by homogenization, then these samples were reheated to the semi-solid state and held in the range of 5 to 50 minutes. The experimental results show that varying process cause the difference in the deformation degree and microstructure for as-extruded samples, resulting in various semi-solid microstructure. It is verified that the formation of equiaxed grains in semi-solid microstructure depends on recrystallization behavior of extruded samples during partial melting. Both relative high extrusion temperature and low extrusion ratio lead to high volume fraction of recrystallized area, thus entirely equiaxed solid grains in semi-solid 7075 Al alloy samples can be obtained finally. In addition, Ostwald ripening was determined as the dominate coarsening mechanism of solid grains in semi-solid state for this 7075 Al alloy during the RAP route. The influence of predeformation on recrystallization behavior of this 7075 Al alloy was discussed in detail.
基金This research was funded by the National Key Research and Development Program of China(No.2019YFA0705300)the Joint Research Fund of Natural Science Foundation of Liaoning-the State Key Laboratory of Rolling and Automation,Northeastern University(2019KF0506)the Fundamental Research Funds for the Central Universities of China(DUT19JC26).
文摘The control of microstructure during hot rolling process of steel is of great importance and will affect the properties of the steel products.According to the production line,a three-dimensional multi-field coupled finite element model of 24-pass continuous hot rolling process of 38CrMoAl steel rod is established using the finite element software MSC.Marc.Based on the recrystallization kinetics model and the grain growth model,a subroutine written in Fortran is introduced to calculate the recrystallization behavior and microstructure evolution of 38CrMoAl steel during the entire rolling process.The distribution and evolution of variables such as strain,temperature and recrystallization fractions during the rolling process are analyzed.The temperature variations and grain sizes at both the center and surface of the tested steel are compared with the experimental results.And it is found that the simulation results are in good agreement with the experimental ones,confirming the reliability of the established model.
基金Project (2007CB613803) supported by the National Basic Research Program of ChinaProject (2010GQC0170) supported by the Natural Science Foundation of Jiangxi Province,ChinaProject (GJJ11159) supported by the Educational Committee of Jiangxi Province,China
文摘The dynamic recrystallization（DRX） behavior of Ti-6Al-2Zr-1Mo-1V alloy was investigated at deformation temperature of 1000-1100 °C and strain rate of 10-3-1.0 s-1 by using compression test.The results show that discontinuous dynamic recrystallization（DDRX） is the predominant recrystallization mechanism at temperature higher than 1050 °C and strain rate lower than 0.01 s-1.Meanwhile,continuous dynamic recrystallization is the main mechanism observed at temperature below 1050 °C and strain rate above 0.01 s-1,mixed with a few DDRX grains.In addition,decreasing strain rate and increasing deformation temperature are found to facilitate the progress of DRX and refinement of grains in the Ti alloy in β forging process.
