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管约束WC粉末电爆喷涂涂层的形成 被引量:7
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作者 朱亮 石茂虎 王永 《稀有金属材料与工程》 SCIE EI CAS CSCD 北大核心 2014年第4期968-972,共5页
采用压敏胶载送粉末连续电爆喷涂方法,进行WC粉末电爆喷涂,分析初始电压与喷射腔横截面积对涂层形成的影响。结果表明:在3~7mm喷涂范围内,可形成表层为液相喷涂层和底层为气相沉积层的复合涂层。在较小的喷射腔横截面积下升高初始... 采用压敏胶载送粉末连续电爆喷涂方法,进行WC粉末电爆喷涂,分析初始电压与喷射腔横截面积对涂层形成的影响。结果表明:在3~7mm喷涂范围内,可形成表层为液相喷涂层和底层为气相沉积层的复合涂层。在较小的喷射腔横截面积下升高初始电压,能提高爆炸的区域温度和产物速度,增加气相份额。分析认为:气相优先形成气相沉积层,且气相沉积层与基体结合致密;残留的液相滞后喷射,并覆盖在气相沉积层上形成液相喷涂层。 展开更多
关键词 管约束 电爆 液相喷涂层 气相沉积层
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Application of nanotechnology in a silver/graphite contact material and optimization of its physical and mechanical properties 被引量:5
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作者 YUHaifeng LEIJingxuan +4 位作者 MAXueming ZHULihui LUYao XIANGJing WENGWei 《Rare Metals》 SCIE EI CAS CSCD 2004年第1期79-83,共5页
By applying nanotechnology, a new type of silver/graphite (AgC) electricalcontact was fabricated and characterized. The AgC coating powders were obtained through high-energyball milling and reducer liquid spraying-coa... By applying nanotechnology, a new type of silver/graphite (AgC) electricalcontact was fabricated and characterized. The AgC coating powders were obtained through high-energyball milling and reducer liquid spraying-coating method. The as-prepared powders were examined bytransmission electron microscope (TEM), scanning electron microscope (SEM), and X-ray diffraction(XRD). The results show that the thickness of graphite flakes milled for 10 h is about 50-60 nm andthe AgC coating powders exhibit flocculent structure with quite fine and homogeneous internalmicropores. XRD implies that the average crystalline size of silver in coating powders is about 50nm. The mechanical and physical properties of this newly developed AgC contact made from theabove-mentioned nanocrystalline powders by traditional powder metallurgy technique were measured.Compared with its counterparts made from other techniques, the properties of this new AgC contacthave been optimized. High surface energy and high-energy interfaces of the nanocrystalline AgCcoating powders provide powerful driving force for sintering densification. Moreover, the flocculentstructure of the powders is also an important factor to acquire fine density ratio. 展开更多
关键词 contact material AgC-N (newly developed) NANOTECHNOLOGY high-energy ballmilling reducer liquid spraying-coating method optimization
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挤出滚圆-流化床工艺制备小儿化斑消疹包衣微丸 被引量:3
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作者 何艳萍 陈丽婷 王莹涛 《天津药学》 2018年第6期11-13,39,共4页
目的:采用挤出滚圆-流化床技术制备小儿化斑消疹包衣微丸。方法:以空白微晶纤维素(MCC)微丸为丸芯,液体层积载药,形成载药素丸;再以载药微丸为丸芯,包一层薄膜衣,形成小儿化斑消疹包衣微丸,并对其外观性状、粉体学性质及吸湿性等进行系... 目的:采用挤出滚圆-流化床技术制备小儿化斑消疹包衣微丸。方法:以空白微晶纤维素(MCC)微丸为丸芯,液体层积载药,形成载药素丸;再以载药微丸为丸芯,包一层薄膜衣,形成小儿化斑消疹包衣微丸,并对其外观性状、粉体学性质及吸湿性等进行系统评价。结果:对基础滚圆空白微丸的处方和工艺进行了优化,载药增重119. 3%,薄膜包衣增重3%和5%,吸湿率分别降低了12. 90%和15. 47%,同时起到了掩盖苦味的作用。结论:本文制备的小儿化斑消疹微丸外形美观、质量稳定,可有效减小药物吸湿性并掩盖其苦味。 展开更多
关键词 空白微丸 液体层积 流化包衣 粉体学 吸湿性
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液相等离子喷涂羟基磷灰石涂层性能与工艺的研究 被引量:1
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作者 苏尧 黄涛 +1 位作者 刘晓光 吴方 《生物骨科材料与临床研究》 CAS 2013年第3期15-18,23,68,共6页
目的通过对液相等离子喷涂羟基磷灰石涂层工艺和涂层理化性能的研究,摸索出最优的液相等离子喷涂工艺参数。方法采用正交试验的方法对喷涂功率、蠕动泵速(传送速率)、喷涂距离及雾化压力这四个关键的工艺参数进行优化,以涂层厚度和结晶... 目的通过对液相等离子喷涂羟基磷灰石涂层工艺和涂层理化性能的研究,摸索出最优的液相等离子喷涂工艺参数。方法采用正交试验的方法对喷涂功率、蠕动泵速(传送速率)、喷涂距离及雾化压力这四个关键的工艺参数进行优化,以涂层厚度和结晶度为考察目标进行正交试验分析,并对涂层进行了X射线衍射、傅立叶转换红外光谱及扫描电镜观察等理化性能表征。结果 XRD分析表明各组样品的主相均为HA相,部分样品含有少量的TCP相和CaO;FTIR分析表明每组样品都含有少量的CO32-基团,部分样品的OH-基团发生了脱落;SEM观测表明3#样品呈颗粒状松散堆积,结合强度低,其余样品均呈现出较好的扁平化;正交分析表明各因素对涂层性能的影响大小顺序为:喷涂距离>雾化压力>泵速>功率,并得到了最佳的工艺参数组合。结论液相等离子喷涂羟基磷灰石涂层的最佳工艺参数组合为:功率(45kw)+泵速(8)+喷涂距离(10cm)+雾化压力(0.14mPa)。 展开更多
关键词 液相等离子喷涂 羟基磷灰石涂层 正交实验 工艺优化
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