Self-lubrication is one of the smart material properties required for producing components with enhanced wear resistance and low coefficient of friction.Bidirectional(BD)satin weave polyacrylonitrile(PAN)based carbon ...Self-lubrication is one of the smart material properties required for producing components with enhanced wear resistance and low coefficient of friction.Bidirectional(BD)satin weave polyacrylonitrile(PAN)based carbon fiber(Cf)fabric preform was successfully infiltrated with Al 6061 alloy by squeeze infiltration process.The infiltrated composite shows uniform distribution of carbon fibers in the matrix with the elimination of porosities,fiber damage and close control on the formation of deleterious aluminum carbide(Al4C3)phase.Cf/Al composite exhibits remarkable wear resistance compared to unreinforced alloy due to the formation of self-lubricating tribolayer on the pin surface,which intercepts the contact of matrix metal to counter surface.The BD carbon fiber enhanced the hardness and compressive strength of the composite by restraining the plastic flow behavior of matrix.High resolution transmission electron microscopy shows the presence of Al2O3 and MgAl2O4 spinel,confirmed by EDS and SAD pattern,at the composite interface.The composite shows a lower density of 2.16 g/cm^3 which is a major ad vantage for weight reduction compared to the monolithic alloy(2.7 g/cm^3).展开更多
This paper studies the microstructure variation induced by super-absorbent polymer(SAP)to understand the mechanism of macroscopic strength improvement of stabilized soil.The fabric changes of cement elime stabilized s...This paper studies the microstructure variation induced by super-absorbent polymer(SAP)to understand the mechanism of macroscopic strength improvement of stabilized soil.The fabric changes of cement elime stabilized soil were analyzed with respect to the variation of SAP content,water content,lime content and curing time,using mercury intrusion porosimetry(MIP)tests.It can be observed that the delimitation pore diameter between inter-and intra-aggregate pores was 0.2 mm for the studied soil,determined through the intrusion/extrusion cycles.Experimental results showed that fabric in both inter-and intra-aggregate pores varied significantly with SAP content,lime content,water content and curing time.Two main changes in fabric due to SAP are identified as:(1)an increase in intra-aggregate pores(<0.2 mm)due to the closer soilecementelime cluster space at higher SAP content;and(2)a decrease in inter-aggregate pores represented by a reduction in small-pores(0.2e2 mm)due to the lower pore volume of soil mixture after water absorption by SAP,and a slight increase in large-pores(>2 mm)due to the shrinkage of SAP particle during the freezeedry process of MIP test.Accordingly,the strength gain due to SAP for cementelime stabilized soil was mainly due to a denser fabric with less interaggregate pores.The cementitious products gradually developed over time,leading to an increase in intra-aggregate pores with an increasing proportion of micro-pores(0.006e0.2 mm).Meanwhile,the inter-aggregate pores were filled by cementitious products,resulting in a decrease in total void ratio.Hence,the strength development over time is attributable to the enhancement of cementation bonding and the refinement of fabric due to the increasing cementitious compounds.展开更多
The effects of fibre/matrix bonding, fabric density, fibre volume fraction and bundle size on microstructure, mechanical properties and failure mechanisms in carbon fibre reinforced composites （plastic and carbon mat...The effects of fibre/matrix bonding, fabric density, fibre volume fraction and bundle size on microstructure, mechanical properties and failure mechanisms in carbon fibre reinforced composites （plastic and carbon matrix） have been investigated. The microstructure of unloaded and cracked samples was studied by optical microscopy and scanning electron microscopy （SEM）, respectively whereas the mechanical behaviour was examined by 3- point bending experiments. Exclusively one type of experimental resole type phenolic resin was applied. A strong fibre/matrix bonding, which is needed for high strength of carbon fibre reinforced plastic （CFRP） materials leads to severe composite damages during the pyrolysis resulting in low strength, brittle failure and a very low utilisation of the fibres strain to failure in C/C composites. Inherent fabric parameters such as an increasing fabric density or bundle size or a reduced fibre volume fraction introduce inhomogenities to the CFRP＇s microstructure. Results are lower strength and stiffness whereas the strain to failure increases or remains unchanged. Toughness is almost not affected. In C/C composites inhomogenities due to a reduced bundle size reduce strain to failure, strength, stiffness and toughness. Vice versa a declining fibre volume fraction leads to exactly the opposite behaviour. Increasing the fabric density （weight per unit area） causes similar effects as in CFRPs.展开更多
The rheology of rocks at depth remains a key point in earth sciences. Deformation of high-temperature–highpressure rocks from the subduction zone has not been fully studied; in particular, the deformation behavior of...The rheology of rocks at depth remains a key point in earth sciences. Deformation of high-temperature–highpressure rocks from the subduction zone has not been fully studied; in particular, the deformation behavior of eclogites remains poorly understood. This research is focused on the microstructure and fabric of retrograded eclogites from the Hongqiyingzi Complex in Chicheng, north Hebei, China, based on photomicrography, scanning electron microscopy(SEM) and electron backscattered diffraction(EBSD) analysis. The analytical results show that plastic deformation occurred in the garnets during exhumation, but they do not show an obvious lattice preferred orientation(LPO). This can be interpreted as being caused by the simultaneous activation of multiple slip systems in the garnets during deformation by dislocation creep. The plagioclases have a special fabric; the(001) LPO presents a maximum in Z direction which can be correlated with a new [100](001) slip system. The misorientation angle distribution(MAD) of the plagioclases in the deformed retrograded garnet augens shows a special bimodal distribution with peaks in both a low-angle range(<40?) and a high-angle range(>140?). In the retrograded garnet augens(i.e. "white eye socket" garnets) the maximum peak moves from a high-angle range to a low-angle range when we analyze only those plagioclases surrounding the residual garnet porphyroclast. Deformation behavior is controlled by the crystallographic orientation of the host grain and the grain boundary sliding process. Hornblendes in different layers and the retrograded garnet augens show almost the same strong LPO patterns, which are correlated with the [001](010) slip system; and MAD diagrams show a peak in a low-angle range(<40?). Integrating recent studies on metamorphism and geochronology, we argue that ductile deformation occurred during the exhumation periods together with retrograded metamorphism.展开更多
在德国Alfred-Wegener极地与海洋研究所用自动组构分析仪G50测试了东天山庙儿沟冰芯(43°03'19″N,94°19'21″E,4 512 m a.s.l.;2005年钻取,长58.7 m)冰微构造和组构,分析其特征并解释其所蕴含的意义。冰微构造和组构...在德国Alfred-Wegener极地与海洋研究所用自动组构分析仪G50测试了东天山庙儿沟冰芯(43°03'19″N,94°19'21″E,4 512 m a.s.l.;2005年钻取,长58.7 m)冰微构造和组构,分析其特征并解释其所蕴含的意义。冰微构造和组构随深度的演变总体相似于其他中国山地冰川冰的观测结果,同时展示了其季节性特征。部分样品的测试结果有所波动,可能是样品在运输和存储过程中的热力学性质发生改变所致。组构型反应的力场较为简单,主要为中下部的单轴压应力作用。正常晶粒生长、多边形化作用和应变导致的边界迁移再结晶不能解释其在某一深段占据主导,而可能是三者共同作用于所有冰芯深部。展开更多
文摘Self-lubrication is one of the smart material properties required for producing components with enhanced wear resistance and low coefficient of friction.Bidirectional(BD)satin weave polyacrylonitrile(PAN)based carbon fiber(Cf)fabric preform was successfully infiltrated with Al 6061 alloy by squeeze infiltration process.The infiltrated composite shows uniform distribution of carbon fibers in the matrix with the elimination of porosities,fiber damage and close control on the formation of deleterious aluminum carbide(Al4C3)phase.Cf/Al composite exhibits remarkable wear resistance compared to unreinforced alloy due to the formation of self-lubricating tribolayer on the pin surface,which intercepts the contact of matrix metal to counter surface.The BD carbon fiber enhanced the hardness and compressive strength of the composite by restraining the plastic flow behavior of matrix.High resolution transmission electron microscopy shows the presence of Al2O3 and MgAl2O4 spinel,confirmed by EDS and SAD pattern,at the composite interface.The composite shows a lower density of 2.16 g/cm^3 which is a major ad vantage for weight reduction compared to the monolithic alloy(2.7 g/cm^3).
基金the China Postdoctoral Science Foundation(Grant Nos.2016M600396 and 2017T100355)the Fundamental Research Funds for the Central Universities of China(Grant No.B200204001)Jiangsu Natural Resources Science and Technology Fund(Grant No.KJXM2019025)are also acknowledged.
文摘This paper studies the microstructure variation induced by super-absorbent polymer(SAP)to understand the mechanism of macroscopic strength improvement of stabilized soil.The fabric changes of cement elime stabilized soil were analyzed with respect to the variation of SAP content,water content,lime content and curing time,using mercury intrusion porosimetry(MIP)tests.It can be observed that the delimitation pore diameter between inter-and intra-aggregate pores was 0.2 mm for the studied soil,determined through the intrusion/extrusion cycles.Experimental results showed that fabric in both inter-and intra-aggregate pores varied significantly with SAP content,lime content,water content and curing time.Two main changes in fabric due to SAP are identified as:(1)an increase in intra-aggregate pores(<0.2 mm)due to the closer soilecementelime cluster space at higher SAP content;and(2)a decrease in inter-aggregate pores represented by a reduction in small-pores(0.2e2 mm)due to the lower pore volume of soil mixture after water absorption by SAP,and a slight increase in large-pores(>2 mm)due to the shrinkage of SAP particle during the freezeedry process of MIP test.Accordingly,the strength gain due to SAP for cementelime stabilized soil was mainly due to a denser fabric with less interaggregate pores.The cementitious products gradually developed over time,leading to an increase in intra-aggregate pores with an increasing proportion of micro-pores(0.006e0.2 mm).Meanwhile,the inter-aggregate pores were filled by cementitious products,resulting in a decrease in total void ratio.Hence,the strength development over time is attributable to the enhancement of cementation bonding and the refinement of fabric due to the increasing cementitious compounds.
文摘The effects of fibre/matrix bonding, fabric density, fibre volume fraction and bundle size on microstructure, mechanical properties and failure mechanisms in carbon fibre reinforced composites （plastic and carbon matrix） have been investigated. The microstructure of unloaded and cracked samples was studied by optical microscopy and scanning electron microscopy （SEM）, respectively whereas the mechanical behaviour was examined by 3- point bending experiments. Exclusively one type of experimental resole type phenolic resin was applied. A strong fibre/matrix bonding, which is needed for high strength of carbon fibre reinforced plastic （CFRP） materials leads to severe composite damages during the pyrolysis resulting in low strength, brittle failure and a very low utilisation of the fibres strain to failure in C/C composites. Inherent fabric parameters such as an increasing fabric density or bundle size or a reduced fibre volume fraction introduce inhomogenities to the CFRP＇s microstructure. Results are lower strength and stiffness whereas the strain to failure increases or remains unchanged. Toughness is almost not affected. In C/C composites inhomogenities due to a reduced bundle size reduce strain to failure, strength, stiffness and toughness. Vice versa a declining fibre volume fraction leads to exactly the opposite behaviour. Increasing the fabric density （weight per unit area） causes similar effects as in CFRPs.
基金supported by the National Natural Science Foundation of China(Grant No.41430207)the National Basic Research Program of China(Grant No.2013CB429804)the Special Fund for Basic Research of Central Universities(Grant No.310827161010)
文摘The rheology of rocks at depth remains a key point in earth sciences. Deformation of high-temperature–highpressure rocks from the subduction zone has not been fully studied; in particular, the deformation behavior of eclogites remains poorly understood. This research is focused on the microstructure and fabric of retrograded eclogites from the Hongqiyingzi Complex in Chicheng, north Hebei, China, based on photomicrography, scanning electron microscopy(SEM) and electron backscattered diffraction(EBSD) analysis. The analytical results show that plastic deformation occurred in the garnets during exhumation, but they do not show an obvious lattice preferred orientation(LPO). This can be interpreted as being caused by the simultaneous activation of multiple slip systems in the garnets during deformation by dislocation creep. The plagioclases have a special fabric; the(001) LPO presents a maximum in Z direction which can be correlated with a new [100](001) slip system. The misorientation angle distribution(MAD) of the plagioclases in the deformed retrograded garnet augens shows a special bimodal distribution with peaks in both a low-angle range(<40?) and a high-angle range(>140?). In the retrograded garnet augens(i.e. "white eye socket" garnets) the maximum peak moves from a high-angle range to a low-angle range when we analyze only those plagioclases surrounding the residual garnet porphyroclast. Deformation behavior is controlled by the crystallographic orientation of the host grain and the grain boundary sliding process. Hornblendes in different layers and the retrograded garnet augens show almost the same strong LPO patterns, which are correlated with the [001](010) slip system; and MAD diagrams show a peak in a low-angle range(<40?). Integrating recent studies on metamorphism and geochronology, we argue that ductile deformation occurred during the exhumation periods together with retrograded metamorphism.
文摘在德国Alfred-Wegener极地与海洋研究所用自动组构分析仪G50测试了东天山庙儿沟冰芯(43°03'19″N,94°19'21″E,4 512 m a.s.l.;2005年钻取,长58.7 m)冰微构造和组构,分析其特征并解释其所蕴含的意义。冰微构造和组构随深度的演变总体相似于其他中国山地冰川冰的观测结果,同时展示了其季节性特征。部分样品的测试结果有所波动,可能是样品在运输和存储过程中的热力学性质发生改变所致。组构型反应的力场较为简单,主要为中下部的单轴压应力作用。正常晶粒生长、多边形化作用和应变导致的边界迁移再结晶不能解释其在某一深段占据主导,而可能是三者共同作用于所有冰芯深部。
基金Jiangsu Provincial College Students' Innovation and Entrepreneurship Training Program-University Enterprise Cooperation Fund Project(201610285113H)The Nantong Municipal People's Government Funding Project-2015G Leading Edge&Key Technology Innovation Plan-Industrial Innovation Project(H1508)
