The yield asymmetry between compression and tension of magnesium alloy Mg-3Al-1Zn（AZ31） with different grain sizes and textures has been studied by tensile and compressive testing of as-cast,as-extruded and equal ch...The yield asymmetry between compression and tension of magnesium alloy Mg-3Al-1Zn（AZ31） with different grain sizes and textures has been studied by tensile and compressive testing of as-cast,as-extruded and equal channel angular pressed（ECAPed） specimens.The significant yield asymmetry（the ratio of yield strength between compression and tension σyc/σyt is ～0.44） was found in as-extruded specimens and the corresponding microstructure evolution during deformation revealed that {10 ˉ 12} tensile twinning is the underlying reason for the large yield asymmetry.Strong texture and grain size are influential factors for large yield asymmetry.The separate contributions of grain size and texture on yield asymmetry were investigated.展开更多
In this work,a high-strength Mg–10Gd–6Y–1.5Zn–0.5Zr(wt.%)alloy was fabricated by successive multi-pass equal channel angular pressing(ECAP).The microstructure and mechanical property of as-cast and ECAP alloys wer...In this work,a high-strength Mg–10Gd–6Y–1.5Zn–0.5Zr(wt.%)alloy was fabricated by successive multi-pass equal channel angular pressing(ECAP).The microstructure and mechanical property of as-cast and ECAP alloys were systematically researched by X-ray diffractometer,scanning electron microscopy,transmission electron microscopy and compression test.The results show that the microstructure of as-cast alloy consists ofα-Mg grains,Mg24Y5 networks,18R blocks,fine 14H lamellas,and fewY-rich particles.After 8 passes ECAP,dynamic recrystallization ofα-Mg is developed and their average grain size decreases to about 1μm.The network Mg_(24)Y_(5) phase at grain boundaries is broken into small particles with average diameter lower than 0.5μm.Moreover,18R blocks are kinked and delaminated,or broken into small particles and blended with Mg24Y5 particles.14H lamellas grow gradually or are dynamically precipitated within certainα-Mg grains.Compression tests indicate that 8p ECAP alloy exhibits excellent mechanical property with compressive strength of 537 MPa and fracture strain of 17.0%.The significant improvement for both strength and ductility of deformed alloy could be ascribed to DRX grains,refined Mg24Y5 particles,18R kinking and dynamical precipitation of 14H.展开更多
Microstructure evolution of processed Mg-Al-Zn alloy by equal channel angularextrusion(ECAE) in semi-solid isothermal treatment was investigated. The results show that withincreasing semi-solid isothermal treatment te...Microstructure evolution of processed Mg-Al-Zn alloy by equal channel angularextrusion(ECAE) in semi-solid isothermal treatment was investigated. The results show that withincreasing semi-solid isothermal treatment temperature, the a phase solid grain size of processedMg-Al-Zn alloy by ECAE increases firstly due to coarsening of a phase solid grains, then decreasesdue to melting of a phase solid grains. With the increase of extrusion passes during ECAE, the aphase solid grain size in the following semi-solid isothermal treatment decreases. The a phase solidgrain size of processed Mg-Al-Zn alloy by ECAE under route B_C is the smallest, while the a phasesolid grain size of processed material by ECAE under route A is the largest. The primary mechanismof spheroid formation depends on the melting of recrystallizing boundaries and diffusion of soluteatoms in the semi-solid state.展开更多
The microstructural evolution of AZ61 magnesium alloy predeformed by equal channel angular extrusion（ECAE） during semisolid isothermal treatment（SSIT） was investigated by means of optical metalloscopy and image an...The microstructural evolution of AZ61 magnesium alloy predeformed by equal channel angular extrusion（ECAE） during semisolid isothermal treatment（SSIT） was investigated by means of optical metalloscopy and image analysis equipment.The process involved application of ECAE to as-cast alloy at 310 ℃ to induce strain prior to heating in the semisolid region for different time lengths.The results show that extrusion pass,isothermal temperature and processing route have an influence on microstructural evolution of predeformed AZ61 magnesium alloy during SSIT.With the increase of extrusion pass,the solid particle size is reduced gradually.When isothermal temperature increases from 530 ℃ to 560 ℃,the average particle size increases from 22 μm to 35 μm.When isothermal temperature is 575 ℃,the average particle size decreases.The particle size of microstructure of AZ61 magnesium alloy predeformed by ECAE at BC during SSIT is the finest.展开更多
A combination of extrusion and equal channel angular pressing （ECAP） was used to deform a plain low carbon steel. This process consists of two successive deformations by extrusion and ECAP in a single die （Ex-ECAP...A combination of extrusion and equal channel angular pressing （ECAP） was used to deform a plain low carbon steel. This process consists of two successive deformations by extrusion and ECAP in a single die （Ex-ECAP）. Cylindrical samples were heated to predefined temperatures （650 and 850 ℃） and then pressed through a die channel with crosshead speed of 10 mm/s. Microstructure and resultant mechanical properties of processed material were studied. The results showed that pressing temperature has a significant effect on the resultant microstructure. While at 650 ℃, the cold worked structure with elongated ferrite grains were obtained, and at 850 ℃ the microstructure consisted of elongated ferrite grains and very fine grains at their boundaries as a consequence of continuous dynamic recrystallization （CDRX） of ferrite phase. Also at 850 ℃, a particular microstructure consisted of cold worked ferrite and static recrystallized grains on shear bands was obtained.展开更多
The influence of equal channel angular pressing on the tension-compression yield asymmetry of extruded Mg-5.3 Zn-0.6 Ca(weight percent)alloy has been investigated.The microstructure was obviously refined by the large ...The influence of equal channel angular pressing on the tension-compression yield asymmetry of extruded Mg-5.3 Zn-0.6 Ca(weight percent)alloy has been investigated.The microstructure was obviously refined by the large strain during the equal channel angular pressing,accompanied with very fine Ca_(2)Mg_(6)Zn_(3) phases with average diameter of 70 nm.The weak tension-compression yield asymmetry after equal channel angular pressing is mainly attributed to the reduced volume fraction of extension twinning during the compression,because the slope(k)of twinning in Hall-Petch relationship is higher than that of dislocation slip,and the twinning deformation is difficult to take place with decreasing grain size.The basal slip is more active in the alloy after equal channel angular pressing,due to the non-basal texture components,which hinders the twinning activation and reduces the yield asymmetry.Furthermore,the presence of fine precipitate restricts the twinning activation,which also contributes to the reduction of yield asymmetry.展开更多
Addition of Al-5Ti-1B alloy to molten aluminum alloys can refine α-Al grains effectively and thereby improve their strength and toughness. TiAl;and TiB;in Al-5Ti-1B alloy are the main secondary-phase particles for re...Addition of Al-5Ti-1B alloy to molten aluminum alloys can refine α-Al grains effectively and thereby improve their strength and toughness. TiAl;and TiB;in Al-5Ti-1B alloy are the main secondary-phase particles for refinement, while the understanding on the effect of their sizes on α-Al grain refinement continues to be fragmented. Therefore, Al-5Ti-1B alloys with various sizes and morphologies of the secondary-phase particles were prepared by equal channel angular pressing（ECAP）. Evolution of the secondary-phase particles during ECAP process and their impact on α-Al grain refinement were studied by X-ray diffraction and scanning electron microscope（SEM）. Results show that during the ECAP process, micro-cracks firstly appeared inside TiAl;particles and then gradually expanded, which resulted in continuous refinement of TiAl;particles. In addition, micro-distribution uniformity of TiB;particles was improved due to the impingement of TiAl;particles to TiB;clusters during deformation. Excessively large sizes of TiAl;particles would reduce the number of effective heterogeneous nucleus and thus resulted in poor grain refinement effectiveness. Moreover, excessively small TiAl;particles would reduce inhibitory factors for grain growth Q and weaken grain refinement effectiveness. Therefore, an optimal size range of 18-22 μm for TiAl;particles was suggested.展开更多
The biomagnesium alloys have been considered to be one of the most potential biodegradable metal materials due to its good mechanical compatibility, biological compatibility, biological security and biodegradable char...The biomagnesium alloys have been considered to be one of the most potential biodegradable metal materials due to its good mechanical compatibility, biological compatibility, biological security and biodegradable characteristics. However, the two major problems of high degradation rates in physiological environment and low mechanical properties prevent the development of biomagnesium alloys. In the present work, the samples of Mg-Zn-Y-Nd alloy were prepared by cyclic extrusion compression （CEC） and equal channel angular pressing （ECAP）. The microstructures, mechanical properties of alloy and its corrosion behavior in simulated body fluid （SBF） were evaluated. The results reveal that Mg-Zn-Y-Nd alloy consists of equiaxial fine grain structure with the homogeneous distribution of micrometer size and nano-sized second phase, which was caused by the dynamic recrystallization during the ECAP and CEC. The corrosion resistance of alloy was improved. The tensile and corrosion resistance were improved, especially the processed alloy exhibit uniform corrosion performances and decreased corrosion rate. This will provide theoretical ground for Mg-Zn-Y-Nd alloy as vascular stent application.展开更多
The microstructure, texture and mechanical property evolution of the extruded Mg-x Y(x = 1, 5 wt.%) alloys during equal channel angular pressing(ECAP) were systematically investigated using an optical microscope, elec...The microstructure, texture and mechanical property evolution of the extruded Mg-x Y(x = 1, 5 wt.%) alloys during equal channel angular pressing(ECAP) were systematically investigated using an optical microscope, electron backscatter diffraction(EBSD) and uniaxial tensile test. The Mg-Y alloys exhibited a weakened basal texture before the ECAP, and the texture was further weakened with the max basal poles dispersed along ~45° between the extrusion direction and the transverse direction after the ECAP. The Mg-5 Y alloys always exhibited a finer grain size comparing to that of Mg-1 Y for the same ECAP process. With a proper ECAP process, both the strength and elongation of Mg-5 Y alloy could be improved simultaneously after the ECAP, i.e., the yield strength(273.9 ± 1.2 MPa), ultimate strength(306.4 ± 3.0 MPa),and elongation(23.9 ± 1.0%) were increased by 10%, 6%, and 72%, respectively, comparing to that before the ECAP. This was considered to be arose from the combined effects of grain refinement, significant improved microstructure homogeneity and solid solution hardening.In addition, it was found that Mg-Y alloy with better comprehensive properties could be obtained by the decreasing-temperature ECAP processes. The yield strength-grain size relationship could be well described by the Hall-Petch relation for all the ECAPed Mg-Y alloys,which was consistent with that the texture changes did not significantly affect the average Schmid factors of basal, prismatic and pyramidal slips for both Mg-Y alloys.展开更多
In this work,two wrought Mg-3.66Al-4.25Ca-0.43 Mn(wt%)alloys with different morphology and distribution of Mg_(2)Ca particles were fabricated by hot extrusion and multi-pass(32)equal channel angular pressing(ECAP).The...In this work,two wrought Mg-3.66Al-4.25Ca-0.43 Mn(wt%)alloys with different morphology and distribution of Mg_(2)Ca particles were fabricated by hot extrusion and multi-pass(32)equal channel angular pressing(ECAP).The as-extruded alloy exhibits a banded microstructure with alternately arranged Mg_(2)Ca particle bands,fine α-Mg dynamically recrystallized(DRX)grain bands,and coarse α-Mg deformed grain bands.The Mg_(2)Ca bands are composed of broken Mg_(2)Ca particles which are aggregated and aligned along extrusion direction.The microstructure of ECAP alloy contains complete α-Mg DRX grains and refined Mg_(2)Ca particles which are dispersedly distributed at grain boundaries.Tensile test results show that the as-extruded alloy possesses high ultimate tensile strength(UTS)of 420 MPa and poor fracture elongation of 7%,while the ECAP alloy exhibits improved toughness with UTS of 347 MPa and fraction elongation of 16%.The higher strength of as-extruded alloy is mainly ascribed to the contribution of coarse deformed grains with strong texture,and its poor toughness is resulted from the formation of Mg_(2)Ca bands within which microcracks could form and extend rapidly.On the contrary,the refined and dispersedly distributed Mg_(2)Ca particles are effective to retard crack initiation and impede crack propagation,thereby enhancing the toughness of ECAP alloy significantly.展开更多
Three-dimensional（3D） geometric models with different comer angles （90° and 120°） and with or without inner round fillets in the bottom die were designed. Some important process parameters were regarded ...Three-dimensional（3D） geometric models with different comer angles （90° and 120°） and with or without inner round fillets in the bottom die were designed. Some important process parameters were regarded as the calculation conditions used in DEFORMTM-3D software, such as stress--strain data of compression test for AZ31 magnesium, temperatures of die and billet, and friction coefficient. Influence of friction coefficient on deformation process was discussed. The results show that reasonable lubrication condition is important to plastic deformation. The change characteristics for distributions of effective stress and strain during an equal channel angular extrusion （ECAE） process with inner angle of 90° and without fillets at outer comer were described. Inhomogeneity index （C） was defined and deformation heterogeneity of ECAE was analyzed from the simulation and experiment results. The deformation homogeneity caused by fillets at outer comer increased compared with the die without fillets. The cumulated maximum strains decrease with increasing the fillets of outer comer in ECAE die and the inner comer angle. The analysis results show that better structures of ECAE die including appropriate outer comer fillet and the inner comer angle of 90° for the die can improve the strain and ensure plastic deformation homogenization to a certain extent. The required extrusion force drops with increasing the fillet made at outer comer in ECAE die. It is demonstrated that the prediction results are in good agreement with experiments and the theoretical calculation and the research conclusions in literatures.展开更多
A new quadrature coded OFDM system is proposed. The transmitted data symbols are grouped in such format that the in phase side and the quadrature side of the symbols are arranged in opposite order. By analysis an...A new quadrature coded OFDM system is proposed. The transmitted data symbols are grouped in such format that the in phase side and the quadrature side of the symbols are arranged in opposite order. By analysis and simulation, the performance of the new system can be improved greatly, as well as the harmful influences on the system owing to frequency offset can be reduced effectively, which can combat the disadvantages of OFDM system.展开更多
According to the ion and molecule coexistence theory, the activity model of Fe-Si-B ternary system was es- tablished, and the influence of ratio ：Csi/XZe, boron content and temperature, etc. on the activity of the me...According to the ion and molecule coexistence theory, the activity model of Fe-Si-B ternary system was es- tablished, and the influence of ratio ：Csi/XZe, boron content and temperature, etc. on the activity of the melt com- pound was investigated. The results show that the FeB activity is high in the liquid iron, when Xsl/XFo is 0. 5 ; the ac- tivity of boron increases with increasing the boron content for different contents of xe and xs, and the activity of boron at the ratio xFo = 0.4 is about one order of magnitude higher than that for the XFo = 0. 8; The activities of the melt compound were also affected by temperature, but the influencing extent was little. The equal activity diagrams of silicon and boron were drawn for the first time according to the model results.展开更多
Two kinds of semi-solid samples of AZ80−0.2Y−0.15Ca(wt.%)(AZ80M)magnesium alloy were prepared by semi-solid isothermal heat treatment of materials with and without equal channel angular pressing(ECAP)process.The micro...Two kinds of semi-solid samples of AZ80−0.2Y−0.15Ca(wt.%)(AZ80M)magnesium alloy were prepared by semi-solid isothermal heat treatment of materials with and without equal channel angular pressing(ECAP)process.The microstructures of initial and semi-solid treated samples were compared and analyzed.The results showed a significant difference in the liquid phase distribution between three-pass ECAP processed(3P)and as-received samples during the isothermal heating process.The semi-solid 3P sample showed a more uniform liquid distribution due to its smaller dihedral angle.Besides,the coarsening processes of solid grains of as-received and 3P samples were dominated by the coalescence and Ostwald ripening mechanism,respectively.The difference of coarsening processes was mainly related to the proportion of the high-angle grain boundaries in materials,which further affected the evolution behavior of the liquid pools.展开更多
基金supported by the National Natural Science Foundation of China under Grant Nos.50471082 and 50571102
文摘The yield asymmetry between compression and tension of magnesium alloy Mg-3Al-1Zn（AZ31） with different grain sizes and textures has been studied by tensile and compressive testing of as-cast,as-extruded and equal channel angular pressed（ECAPed） specimens.The significant yield asymmetry（the ratio of yield strength between compression and tension σyc/σyt is ～0.44） was found in as-extruded specimens and the corresponding microstructure evolution during deformation revealed that {10 ˉ 12} tensile twinning is the underlying reason for the large yield asymmetry.Strong texture and grain size are influential factors for large yield asymmetry.The separate contributions of grain size and texture on yield asymmetry were investigated.
基金the Natural Science Foundation of Jiangsu Province of China(No.BK20160869)the financial support from the Nantong Science and Technology Project(No.GY12015009)+1 种基金the Fundamental Research Funds for the Central Universities(No.2015B01314)the National Natural Science Foundation of China(No.51501039).
文摘In this work,a high-strength Mg–10Gd–6Y–1.5Zn–0.5Zr(wt.%)alloy was fabricated by successive multi-pass equal channel angular pressing(ECAP).The microstructure and mechanical property of as-cast and ECAP alloys were systematically researched by X-ray diffractometer,scanning electron microscopy,transmission electron microscopy and compression test.The results show that the microstructure of as-cast alloy consists ofα-Mg grains,Mg24Y5 networks,18R blocks,fine 14H lamellas,and fewY-rich particles.After 8 passes ECAP,dynamic recrystallization ofα-Mg is developed and their average grain size decreases to about 1μm.The network Mg_(24)Y_(5) phase at grain boundaries is broken into small particles with average diameter lower than 0.5μm.Moreover,18R blocks are kinked and delaminated,or broken into small particles and blended with Mg24Y5 particles.14H lamellas grow gradually or are dynamically precipitated within certainα-Mg grains.Compression tests indicate that 8p ECAP alloy exhibits excellent mechanical property with compressive strength of 537 MPa and fracture strain of 17.0%.The significant improvement for both strength and ductility of deformed alloy could be ascribed to DRX grains,refined Mg24Y5 particles,18R kinking and dynamical precipitation of 14H.
基金Projects(50475029,50605015) supported by the National Natural Science Foundation of China
文摘Microstructure evolution of processed Mg-Al-Zn alloy by equal channel angularextrusion(ECAE) in semi-solid isothermal treatment was investigated. The results show that withincreasing semi-solid isothermal treatment temperature, the a phase solid grain size of processedMg-Al-Zn alloy by ECAE increases firstly due to coarsening of a phase solid grains, then decreasesdue to melting of a phase solid grains. With the increase of extrusion passes during ECAE, the aphase solid grain size in the following semi-solid isothermal treatment decreases. The a phase solidgrain size of processed Mg-Al-Zn alloy by ECAE under route B_C is the smallest, while the a phasesolid grain size of processed material by ECAE under route A is the largest. The primary mechanismof spheroid formation depends on the melting of recrystallizing boundaries and diffusion of soluteatoms in the semi-solid state.
基金Project(51075099) supported by the National Natural Science Foundation of ChinaProject(E201038) supported by Natural Science Foundation of the Heilongjiang Province,China+3 种基金Project(20090460884) supported by the China Postdoctoral Science Foundation Project(SKLSP201121) supported by the Fund of the State Key Laboratory of Solidification Processing in NWPU,ChinaProject (2011RFQXG010) supported by the Harbin City Young Scientists Foundation,ChinaProject(LBH-T1102) supported by the Specially Postdoctoral Science Foundation of Heilongjiang Province,China
文摘The microstructural evolution of AZ61 magnesium alloy predeformed by equal channel angular extrusion（ECAE） during semisolid isothermal treatment（SSIT） was investigated by means of optical metalloscopy and image analysis equipment.The process involved application of ECAE to as-cast alloy at 310 ℃ to induce strain prior to heating in the semisolid region for different time lengths.The results show that extrusion pass,isothermal temperature and processing route have an influence on microstructural evolution of predeformed AZ61 magnesium alloy during SSIT.With the increase of extrusion pass,the solid particle size is reduced gradually.When isothermal temperature increases from 530 ℃ to 560 ℃,the average particle size increases from 22 μm to 35 μm.When isothermal temperature is 575 ℃,the average particle size decreases.The particle size of microstructure of AZ61 magnesium alloy predeformed by ECAE at BC during SSIT is the finest.
文摘A combination of extrusion and equal channel angular pressing （ECAP） was used to deform a plain low carbon steel. This process consists of two successive deformations by extrusion and ECAP in a single die （Ex-ECAP）. Cylindrical samples were heated to predefined temperatures （650 and 850 ℃） and then pressed through a die channel with crosshead speed of 10 mm/s. Microstructure and resultant mechanical properties of processed material were studied. The results showed that pressing temperature has a significant effect on the resultant microstructure. While at 650 ℃, the cold worked structure with elongated ferrite grains were obtained, and at 850 ℃ the microstructure consisted of elongated ferrite grains and very fine grains at their boundaries as a consequence of continuous dynamic recrystallization （CDRX） of ferrite phase. Also at 850 ℃, a particular microstructure consisted of cold worked ferrite and static recrystallized grains on shear bands was obtained.
基金The authors wish to highly acknowledge Prof.L.M.Wang of Changchun Institute of Applied Chemistry,Chinese Academy of Sciences,for his valuable suggestions and discussions.Thanks to the financial aid from the National Science&Technology Pillar Program(Grant No.2012BAE01B04)the National Natural Science Foundation of China(Grant No.51401200)the Natural Science Foundation of Jilin Province(Grant No.20140520099JH).
文摘The influence of equal channel angular pressing on the tension-compression yield asymmetry of extruded Mg-5.3 Zn-0.6 Ca(weight percent)alloy has been investigated.The microstructure was obviously refined by the large strain during the equal channel angular pressing,accompanied with very fine Ca_(2)Mg_(6)Zn_(3) phases with average diameter of 70 nm.The weak tension-compression yield asymmetry after equal channel angular pressing is mainly attributed to the reduced volume fraction of extension twinning during the compression,because the slope(k)of twinning in Hall-Petch relationship is higher than that of dislocation slip,and the twinning deformation is difficult to take place with decreasing grain size.The basal slip is more active in the alloy after equal channel angular pressing,due to the non-basal texture components,which hinders the twinning activation and reduces the yield asymmetry.Furthermore,the presence of fine precipitate restricts the twinning activation,which also contributes to the reduction of yield asymmetry.
基金financial support provided by the National Natural Science Foundation of China(Nos.51674077 and 51474063)
文摘Addition of Al-5Ti-1B alloy to molten aluminum alloys can refine α-Al grains effectively and thereby improve their strength and toughness. TiAl;and TiB;in Al-5Ti-1B alloy are the main secondary-phase particles for refinement, while the understanding on the effect of their sizes on α-Al grain refinement continues to be fragmented. Therefore, Al-5Ti-1B alloys with various sizes and morphologies of the secondary-phase particles were prepared by equal channel angular pressing（ECAP）. Evolution of the secondary-phase particles during ECAP process and their impact on α-Al grain refinement were studied by X-ray diffraction and scanning electron microscope（SEM）. Results show that during the ECAP process, micro-cracks firstly appeared inside TiAl;particles and then gradually expanded, which resulted in continuous refinement of TiAl;particles. In addition, micro-distribution uniformity of TiB;particles was improved due to the impingement of TiAl;particles to TiB;clusters during deformation. Excessively large sizes of TiAl;particles would reduce the number of effective heterogeneous nucleus and thus resulted in poor grain refinement effectiveness. Moreover, excessively small TiAl;particles would reduce inhibitory factors for grain growth Q and weaken grain refinement effectiveness. Therefore, an optimal size range of 18-22 μm for TiAl;particles was suggested.
基金Acknowledgements The authors are grateful for the support by National Key Technology R＆D Program of China （Grant No. 2012BAI18B01） and the National Natural Science Foundation of China （Grant No. 51171174）.
文摘The biomagnesium alloys have been considered to be one of the most potential biodegradable metal materials due to its good mechanical compatibility, biological compatibility, biological security and biodegradable characteristics. However, the two major problems of high degradation rates in physiological environment and low mechanical properties prevent the development of biomagnesium alloys. In the present work, the samples of Mg-Zn-Y-Nd alloy were prepared by cyclic extrusion compression （CEC） and equal channel angular pressing （ECAP）. The microstructures, mechanical properties of alloy and its corrosion behavior in simulated body fluid （SBF） were evaluated. The results reveal that Mg-Zn-Y-Nd alloy consists of equiaxial fine grain structure with the homogeneous distribution of micrometer size and nano-sized second phase, which was caused by the dynamic recrystallization during the ECAP and CEC. The corrosion resistance of alloy was improved. The tensile and corrosion resistance were improved, especially the processed alloy exhibit uniform corrosion performances and decreased corrosion rate. This will provide theoretical ground for Mg-Zn-Y-Nd alloy as vascular stent application.
基金supported by the National Natural Science Foundation of China(Nos.51401172 and 51601003)Sichuan Science and Technology Program(2019YJ0238)+1 种基金Fundamental Research Funds for the Central Universities(2682020ZT114)open funding of International Joint Laboratory for Light Alloys(MOE),Chongqing University。
文摘The microstructure, texture and mechanical property evolution of the extruded Mg-x Y(x = 1, 5 wt.%) alloys during equal channel angular pressing(ECAP) were systematically investigated using an optical microscope, electron backscatter diffraction(EBSD) and uniaxial tensile test. The Mg-Y alloys exhibited a weakened basal texture before the ECAP, and the texture was further weakened with the max basal poles dispersed along ~45° between the extrusion direction and the transverse direction after the ECAP. The Mg-5 Y alloys always exhibited a finer grain size comparing to that of Mg-1 Y for the same ECAP process. With a proper ECAP process, both the strength and elongation of Mg-5 Y alloy could be improved simultaneously after the ECAP, i.e., the yield strength(273.9 ± 1.2 MPa), ultimate strength(306.4 ± 3.0 MPa),and elongation(23.9 ± 1.0%) were increased by 10%, 6%, and 72%, respectively, comparing to that before the ECAP. This was considered to be arose from the combined effects of grain refinement, significant improved microstructure homogeneity and solid solution hardening.In addition, it was found that Mg-Y alloy with better comprehensive properties could be obtained by the decreasing-temperature ECAP processes. The yield strength-grain size relationship could be well described by the Hall-Petch relation for all the ECAPed Mg-Y alloys,which was consistent with that the texture changes did not significantly affect the average Schmid factors of basal, prismatic and pyramidal slips for both Mg-Y alloys.
基金supported financially by the Fundamental Research Funds for the Central Universities(B200202131)the National Natural Science Foundation of China(Nos.51901068,51979099 and 51774109)+1 种基金the Nantong Science and Technology Project(No.JC2018109)the Key Research and Development Project of Jiangsu Province(No.BE2017148)。
文摘In this work,two wrought Mg-3.66Al-4.25Ca-0.43 Mn(wt%)alloys with different morphology and distribution of Mg_(2)Ca particles were fabricated by hot extrusion and multi-pass(32)equal channel angular pressing(ECAP).The as-extruded alloy exhibits a banded microstructure with alternately arranged Mg_(2)Ca particle bands,fine α-Mg dynamically recrystallized(DRX)grain bands,and coarse α-Mg deformed grain bands.The Mg_(2)Ca bands are composed of broken Mg_(2)Ca particles which are aggregated and aligned along extrusion direction.The microstructure of ECAP alloy contains complete α-Mg DRX grains and refined Mg_(2)Ca particles which are dispersedly distributed at grain boundaries.Tensile test results show that the as-extruded alloy possesses high ultimate tensile strength(UTS)of 420 MPa and poor fracture elongation of 7%,while the ECAP alloy exhibits improved toughness with UTS of 347 MPa and fraction elongation of 16%.The higher strength of as-extruded alloy is mainly ascribed to the contribution of coarse deformed grains with strong texture,and its poor toughness is resulted from the formation of Mg_(2)Ca bands within which microcracks could form and extend rapidly.On the contrary,the refined and dispersedly distributed Mg_(2)Ca particles are effective to retard crack initiation and impede crack propagation,thereby enhancing the toughness of ECAP alloy significantly.
基金Project(2007CB613700)supported by National Basic Research Program of ChinaProject(2006BAE04B03)supported by Item of Support Plan during the 11th National Five-Year PlanProjects(CST,2007bb4413)supported by National Science Foundation of Chongqing,China
文摘Three-dimensional（3D） geometric models with different comer angles （90° and 120°） and with or without inner round fillets in the bottom die were designed. Some important process parameters were regarded as the calculation conditions used in DEFORMTM-3D software, such as stress--strain data of compression test for AZ31 magnesium, temperatures of die and billet, and friction coefficient. Influence of friction coefficient on deformation process was discussed. The results show that reasonable lubrication condition is important to plastic deformation. The change characteristics for distributions of effective stress and strain during an equal channel angular extrusion （ECAE） process with inner angle of 90° and without fillets at outer comer were described. Inhomogeneity index （C） was defined and deformation heterogeneity of ECAE was analyzed from the simulation and experiment results. The deformation homogeneity caused by fillets at outer comer increased compared with the die without fillets. The cumulated maximum strains decrease with increasing the fillets of outer comer in ECAE die and the inner comer angle. The analysis results show that better structures of ECAE die including appropriate outer comer fillet and the inner comer angle of 90° for the die can improve the strain and ensure plastic deformation homogenization to a certain extent. The required extrusion force drops with increasing the fillet made at outer comer in ECAE die. It is demonstrated that the prediction results are in good agreement with experiments and the theoretical calculation and the research conclusions in literatures.
文摘A new quadrature coded OFDM system is proposed. The transmitted data symbols are grouped in such format that the in phase side and the quadrature side of the symbols are arranged in opposite order. By analysis and simulation, the performance of the new system can be improved greatly, as well as the harmful influences on the system owing to frequency offset can be reduced effectively, which can combat the disadvantages of OFDM system.
基金Item Sponsored by National Key Technology Research and Development Program in 11th Five-Year Plan of China(2009BAB45B05)
文摘According to the ion and molecule coexistence theory, the activity model of Fe-Si-B ternary system was es- tablished, and the influence of ratio ：Csi/XZe, boron content and temperature, etc. on the activity of the melt com- pound was investigated. The results show that the FeB activity is high in the liquid iron, when Xsl/XFo is 0. 5 ; the ac- tivity of boron increases with increasing the boron content for different contents of xe and xs, and the activity of boron at the ratio xFo = 0.4 is about one order of magnitude higher than that for the XFo = 0. 8; The activities of the melt compound were also affected by temperature, but the influencing extent was little. The equal activity diagrams of silicon and boron were drawn for the first time according to the model results.
基金supported by Key Development Project of Sichuan Province(Grant No.2017GZ0399)。
文摘Two kinds of semi-solid samples of AZ80−0.2Y−0.15Ca(wt.%)(AZ80M)magnesium alloy were prepared by semi-solid isothermal heat treatment of materials with and without equal channel angular pressing(ECAP)process.The microstructures of initial and semi-solid treated samples were compared and analyzed.The results showed a significant difference in the liquid phase distribution between three-pass ECAP processed(3P)and as-received samples during the isothermal heating process.The semi-solid 3P sample showed a more uniform liquid distribution due to its smaller dihedral angle.Besides,the coarsening processes of solid grains of as-received and 3P samples were dominated by the coalescence and Ostwald ripening mechanism,respectively.The difference of coarsening processes was mainly related to the proportion of the high-angle grain boundaries in materials,which further affected the evolution behavior of the liquid pools.
