The effect of strontium doped Zn-Ca-P(ZCP)coating by chemical conversion technique on the biodegradation of AZ31 alloy was evaluated.The coating formed with 1.5 wt.%Sr and 20 min phosphating time at 50℃ with pH 2.5 c...The effect of strontium doped Zn-Ca-P(ZCP)coating by chemical conversion technique on the biodegradation of AZ31 alloy was evaluated.The coating formed with 1.5 wt.%Sr and 20 min phosphating time at 50℃ with pH 2.5 completely covers the alloy surface.The Sr doped coated sample also showed very low evolved hydrogen gas and pH change than the ZCP coatings suggested that the degradation of the alloy was extremely controlled.The in vitro bioactivity studies in simulated body fluid exhibits deposition of calcium phosphate phases with Ca/P ratio of 1.55 which is close to that of hydroxyapatite,mineral component of bone.Cytotoxicity evaluation with L929 cells showed higher cell viability of the Sr doped coatings compared to ZCP coatings.展开更多
The Mg-6Al-4Zn alloy was fabricated by mechanical alloying(MA)and hot pressing to serve as biodegradable metal implant.The influence of addition of 1%Si(mass fraction)on the microstructure,mechanical properties and bi...The Mg-6Al-4Zn alloy was fabricated by mechanical alloying(MA)and hot pressing to serve as biodegradable metal implant.The influence of addition of 1%Si(mass fraction)on the microstructure,mechanical properties and bio-corrosion behavior of Mg-6Al-1Zn alloy was studied using X-ray diffractometry,transmission electron microscopy,compression test,as well as immersion,electrochemical test and MTT assay.The results showed that the addition of 1%Si to Mg-6Al-1Zn alloy led to the formation of fine Mg2Si phase with polygonal shape,and increased compressive strength,elongation and improved corrosion resistance.Furthermore,the cell viability of Saos-2 cells has been improved by addition of 1%Si to Mg-6Al-1Zn alloy.According to the results,the magnesium ions released in the methylthiazol tetrazolium(MTT)test have not shown any cell toxicity.All these indicated that the addition of 1%Si improved the properties of Mg-6Al-4Zn alloy for using as a biodegradable implant.展开更多
文摘The effect of strontium doped Zn-Ca-P(ZCP)coating by chemical conversion technique on the biodegradation of AZ31 alloy was evaluated.The coating formed with 1.5 wt.%Sr and 20 min phosphating time at 50℃ with pH 2.5 completely covers the alloy surface.The Sr doped coated sample also showed very low evolved hydrogen gas and pH change than the ZCP coatings suggested that the degradation of the alloy was extremely controlled.The in vitro bioactivity studies in simulated body fluid exhibits deposition of calcium phosphate phases with Ca/P ratio of 1.55 which is close to that of hydroxyapatite,mineral component of bone.Cytotoxicity evaluation with L929 cells showed higher cell viability of the Sr doped coatings compared to ZCP coatings.
文摘The Mg-6Al-4Zn alloy was fabricated by mechanical alloying(MA)and hot pressing to serve as biodegradable metal implant.The influence of addition of 1%Si(mass fraction)on the microstructure,mechanical properties and bio-corrosion behavior of Mg-6Al-1Zn alloy was studied using X-ray diffractometry,transmission electron microscopy,compression test,as well as immersion,electrochemical test and MTT assay.The results showed that the addition of 1%Si to Mg-6Al-1Zn alloy led to the formation of fine Mg2Si phase with polygonal shape,and increased compressive strength,elongation and improved corrosion resistance.Furthermore,the cell viability of Saos-2 cells has been improved by addition of 1%Si to Mg-6Al-1Zn alloy.According to the results,the magnesium ions released in the methylthiazol tetrazolium(MTT)test have not shown any cell toxicity.All these indicated that the addition of 1%Si improved the properties of Mg-6Al-4Zn alloy for using as a biodegradable implant.