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用高效液相色谱法考察表面活性剂在油层中的色谱分离 被引量:4
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作者 陈权生 李之平 +1 位作者 赵文强 韩炜2 《分析测试技术与仪器》 CAS 2000年第1期34-38,共5页
强化采油中常用的表面活性剂石油磺酸盐在通过油层时会发生色谱分离作用 ,其完整性受到破坏 ,从而影响与原油界面的活性。采用高效液相色谱法 (HPLC) ,通过测定磺酸盐色谱分离因子 ,定量地描述石油磺酸盐在岩心多孔介质的色谱分离程度... 强化采油中常用的表面活性剂石油磺酸盐在通过油层时会发生色谱分离作用 ,其完整性受到破坏 ,从而影响与原油界面的活性。采用高效液相色谱法 (HPLC) ,通过测定磺酸盐色谱分离因子 ,定量地描述石油磺酸盐在岩心多孔介质的色谱分离程度。应用该方法可以考察影响色谱分离因子的因素 ,以优化化学驱油配方的设计。该方法具有灵敏度高、可靠。 展开更多
关键词 高效液相色谱法 石油磺酸盐 KPS-2 表面活性剂
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Polyacrylamide hydrogel application in sand control with compressive strength testing 被引量:2
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作者 Mahsa Baghban Salehi Asefe Mousavi Moghadam Samira Zargari MarANDi 《Petroleum Science》 SCIE CAS CSCD 2019年第1期94-104,共11页
Sand production is one of the major problems in sandstone reservoirs. Different mechanical and chemical methods have been proposed to control sand production. In this paper, we propose a chemical method based on using... Sand production is one of the major problems in sandstone reservoirs. Different mechanical and chemical methods have been proposed to control sand production. In this paper, we propose a chemical method based on using polyacrylamide/chromium triacetate hydrogel to investigate sand production in a synthetic sandpack system. To this end, a series of bulk experiments including the bottle test and rheological analysis along with compression tests were conducted. Experimental results indicated that the compressive strength of the sandpack was increased as much as 30 times by injecting 0.5 pore volume of hydrogel. Also, it was found that the increases in cross-linker and polymer concentrations exhibited a positive impact on the compressive strength of the sandpack, mostly by cross-linker concentration(48 psi). Hydrogel with a higher value of cross-linker could retain its viscoelastic properties against the strain which was a maximum of 122% for 0.5 weight ratio of cross-linker/polymer. The presence of salts, in particular divalent cations, has a detrimental effect on the hydrogel stability. The maximum strain value applied on hydrogel in the presence of CaCl_2 was only about 201% as compared to 1010% in the presence of distilled water. Finally, thermogravimetric analysis and its derivative showed that the hydrogel could retain its structure up to 300 °C. The results of this study revealed the potential application of the hydrogel to control sand production. 展开更多
关键词 SAND CONTROL - RHEOLOGY HYDROGEL STRENGTH COMPRESSIVE STRENGTH sandpack
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三元复合体系色谱分离实验研究 被引量:4
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作者 刘凯 岳湘安 +3 位作者 杨长春 苏群 徐金涛 张德鑫 《日用化学工业》 CAS CSCD 北大核心 2014年第12期671-675,共5页
利用填砂管模型进行了三元复合体系的渗流实验,研究了填砂管渗透率及长度对于三元复合体系色谱分离的影响。实验结果表明,在填砂管渗透率和长度不同的条件下,三元复合体系均发生了明显的色谱分离现象。当填砂管渗透率从0.601μm2减小到0... 利用填砂管模型进行了三元复合体系的渗流实验,研究了填砂管渗透率及长度对于三元复合体系色谱分离的影响。实验结果表明,在填砂管渗透率和长度不同的条件下,三元复合体系均发生了明显的色谱分离现象。当填砂管渗透率从0.601μm2减小到0.390μm2时,三元复合体系色谱分离程度增加;当填砂管长度从100 cm增加到240 cm时,三元复合体系色谱分离程度有所增加。说明填砂管渗透率和长度是影响三元复合体系色谱分离的重要因素,且填砂管渗透率的变化对于三元复合体系色谱分离影响程度大于长度。 展开更多
关键词 三元复合体系 色谱分离 填砂管 渗透率
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Thermal oil recovery factors from sandpacks of variable mineralogy
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作者 Viacheslau Y.Kudrashou Hisham A.Nasr-El-Din 《Petroleum Research》 EI 2023年第4期481-489,共9页
S Steam injection is commonly used for production of viscous crude oil.Reservoir rock often contains clay minerals.Reactive nature of steam and clay minerals may lead to formation damage.This work in-vestigates oil re... S Steam injection is commonly used for production of viscous crude oil.Reservoir rock often contains clay minerals.Reactive nature of steam and clay minerals may lead to formation damage.This work in-vestigates oil recovery and changes in petrophysical properties as a function of the mineralogy.Sand-packs with quartz,calcite,feldspar,kaolinite,smectite,and illite were prepared for steam injection experiments.Permeability of the steamed sandpacks was determined using coreflood experiments.Chemical composition of the produced aqueous samples was determined using ICP-OES(inductively coupled plasma-optical emission spectroscopy).Morphology of the rock samples was studied using SEM-EDs(scanning electron microscope-energy dispersive X-ray spectroscopy).Mineralogy and elemental content of the solid samples were determined using XRD(X-ray diffraction)analysis and XRF(X-ray fluorescence)respectively.It was found that aqueous phase samples produced from clay-rich sandpacks tend to have higher pH than samples produced from samples without clay minerals.Oil recovery factors for 100%quartz case was determined to be 65 wt%.Calcite-and feldspar-rich sandpacks produced 56 and 61 wt%of oil respectively.Sandpacks with clay fractions have shown the lowest oil recovery-39,29,and 28 wt%for kaolinite-,smectite-,and illite-rich samples respectively.Mineral dissolution and pre-cipitation were the dominant damaging mechanism for quartz and calcite cases.Feldspar-rich sandpack demonstrated signs of structural destruction of the mineral and fines release.Kaolinite's effect on oil recovery was found to be associated with fines migration.Smectite hydration and swelling in presence of steam was the dominant formation damage effect on the oil production.Steam interaction with illite-rich sandpack caused formation of amorphous silica.This paper presents oil recovery factors as a function of injected pore volume(PV)of steam for sandpacks of different mineralogy.Obtained results characterize petrophysical changes caused by steam interaction with 展开更多
关键词 Steam injection Oilrecovery KAOLINITE SMECTITE Ilite sandpack
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弱凝胶在多孔介质中的运移规律研究 被引量:10
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作者 李洪玺 刘全稳 +1 位作者 王健 李小华 《大庆石油地质与开发》 CAS CSCD 北大核心 2006年第1期88-90,共3页
通过线性填砂模型和透明微观模型实验,研究了弱凝胶在多孔介质中的运移规律和提高采收率的一般特性。线性填砂模型研究发现,弱凝胶在多孔介质中有较强流动性能和传播性能;透明微观模型实验研究发现,弱凝胶优先进入低阻力的大孔道,可拉... 通过线性填砂模型和透明微观模型实验,研究了弱凝胶在多孔介质中的运移规律和提高采收率的一般特性。线性填砂模型研究发现,弱凝胶在多孔介质中有较强流动性能和传播性能;透明微观模型实验研究发现,弱凝胶优先进入低阻力的大孔道,可拉伸变形通过窄小孔道,弱凝胶运移过程受到剪切稀释。弱凝胶的主要作用是驱替,而调剖只是初期或暂时的效果。 展开更多
关键词 弱凝胶 多孔介质 运移规律 填砂模型
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连续管喷砂射孔填砂环空压裂技术的发展现状 被引量:6
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作者 于东兵 胡强法 谭多鸿 《石油机械》 北大核心 2013年第12期112-117,共6页
在简述连续管喷砂射孔填砂环空压裂技术原理与技术特点的基础上,阐述了哈里伯顿公司CobraMax系列技术在直井和水平井中的典型应用以及在煤层气和页岩气压裂中的应用。介绍了填砂技术的3种基本类型及其发展过程,并对诱导砂堵填砂技术及... 在简述连续管喷砂射孔填砂环空压裂技术原理与技术特点的基础上,阐述了哈里伯顿公司CobraMax系列技术在直井和水平井中的典型应用以及在煤层气和页岩气压裂中的应用。介绍了填砂技术的3种基本类型及其发展过程,并对诱导砂堵填砂技术及其发展进行了系统分析。结合国内应用连续管喷砂射孔填砂环空压裂技术的情况,提出了发展建议,指出国内填砂技术与国外主流技术的差距是制约该技术在国内有效应用的主要原因。 展开更多
关键词 连续管 喷砂射孔 填砂封隔 环空压裂 发展现状
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