Filled skutterudite is currently one of the most promising intermediate-temperature thermoelectric(TE)materials,having good thermoelectric transport performance and excellent mechanical properties.For the preparation ...Filled skutterudite is currently one of the most promising intermediate-temperature thermoelectric(TE)materials,having good thermoelectric transport performance and excellent mechanical properties.For the preparation of high-efficiency filled skutterudite TE devices,it is important to have p-and n-type filled skutterudite TE materials with matching performance.However,the current TE properties of p-type Fe-based filled skutterudite materials are worse than n-type filled skutterudite materials.Therefore,how to obtain high-performance p-type Fe-based filled skutterudite materials is the key to preparation of high-efficiency skutterudite-based TE devices.This review summarizes some methods for optimizing the thermal transport performance of p-type filled skutterudite materials at the atomic-molecular and nano-mesoscopic scale that have been used in recent years.These methods include doping,multi-atom filling,and use of low-dimensional structure and of nanocomposite.In addition,the synergistic optimization methods of the electrical and thermal transport parameters and advanced preparation technologies of p-type filled skutterudite materials in recent years are also briefly summarized.These optimizational methods and advanced preparation technologies can significantly improve the TE properties of p-type Fe-based filled skutterudite materials.展开更多
Aiming at the problem that the lattice feature exceeds the view field of the scanning electron microscope(SEM)measuring system,a new lattice measuring method is proposed based on integral imaging technology.When the s...Aiming at the problem that the lattice feature exceeds the view field of the scanning electron microscope(SEM)measuring system,a new lattice measuring method is proposed based on integral imaging technology.When the system works,the SEM measuring system is equivalent to an integral image acquisition system.Firstly,a lattice measuring method is researched based on integral imaging theory.Secondly,the system parameters are calibrated by the VLSI lattice standard.Finally,the value of the lattice standard to be tested is determined based on the calibration parameters and the lattice measuring algorithm.The experimental results show that,compared with the traditional electron microscope measurement method,the relative error of the measured value of the algorithm is maintained within 0.2%,with the same level of measurement accuracy,but it expands the field of view of the electron microscope measurement system,which is suitable for the measurement of samples under high magnification.展开更多
基金This work was supported by the National Natural Science Foundation of China(Grant No.51872006)the Anhui University of Technology High-Level Doctoral Student Training Program(DT17200008).
文摘Filled skutterudite is currently one of the most promising intermediate-temperature thermoelectric(TE)materials,having good thermoelectric transport performance and excellent mechanical properties.For the preparation of high-efficiency filled skutterudite TE devices,it is important to have p-and n-type filled skutterudite TE materials with matching performance.However,the current TE properties of p-type Fe-based filled skutterudite materials are worse than n-type filled skutterudite materials.Therefore,how to obtain high-performance p-type Fe-based filled skutterudite materials is the key to preparation of high-efficiency skutterudite-based TE devices.This review summarizes some methods for optimizing the thermal transport performance of p-type filled skutterudite materials at the atomic-molecular and nano-mesoscopic scale that have been used in recent years.These methods include doping,multi-atom filling,and use of low-dimensional structure and of nanocomposite.In addition,the synergistic optimization methods of the electrical and thermal transport parameters and advanced preparation technologies of p-type filled skutterudite materials in recent years are also briefly summarized.These optimizational methods and advanced preparation technologies can significantly improve the TE properties of p-type Fe-based filled skutterudite materials.
基金supported by the National Key Research and Development Program(No.2019YFB2005503)。
文摘Aiming at the problem that the lattice feature exceeds the view field of the scanning electron microscope(SEM)measuring system,a new lattice measuring method is proposed based on integral imaging technology.When the system works,the SEM measuring system is equivalent to an integral image acquisition system.Firstly,a lattice measuring method is researched based on integral imaging theory.Secondly,the system parameters are calibrated by the VLSI lattice standard.Finally,the value of the lattice standard to be tested is determined based on the calibration parameters and the lattice measuring algorithm.The experimental results show that,compared with the traditional electron microscope measurement method,the relative error of the measured value of the algorithm is maintained within 0.2%,with the same level of measurement accuracy,but it expands the field of view of the electron microscope measurement system,which is suitable for the measurement of samples under high magnification.