The synthesis of Helional[1205-17-0]was reported.It involves the hydrogenation of piperonylenepropanal[6974-47-6]from Cinnamomum petrophilum leaves oil catalyzed by 5% Pd/C,without a solvent at 120℃and 0.6-1.0 MPa,an...The synthesis of Helional[1205-17-0]was reported.It involves the hydrogenation of piperonylenepropanal[6974-47-6]from Cinnamomum petrophilum leaves oil catalyzed by 5% Pd/C,without a solvent at 120℃and 0.6-1.0 MPa,and the yield was 98.2%.GC-MS and HNMR was used to characterize the product.展开更多
文摘The synthesis of Helional[1205-17-0]was reported.It involves the hydrogenation of piperonylenepropanal[6974-47-6]from Cinnamomum petrophilum leaves oil catalyzed by 5% Pd/C,without a solvent at 120℃and 0.6-1.0 MPa,and the yield was 98.2%.GC-MS and HNMR was used to characterize the product.