For a scintillating-fiber array fast-neutron radiography system,a point-spread-function computing model was introduced,and the simulation code was developed. The results of calculation show that fast-neutron radiograp...For a scintillating-fiber array fast-neutron radiography system,a point-spread-function computing model was introduced,and the simulation code was developed. The results of calculation show that fast-neutron radiographs vary with the size of fast neutron sources,the size of fiber cross-section and the imaging geometry. The results suggest that the following qualifications are helpful for a good point spread function: The cross-section of scintillating fibers not greater than 200 μm×200 μm,the size of neutron source as small as a few millimeters,the distance between the source and the scintillating fiber array greater than 1 m,and inspected samples placed as close as possible to the array. The results give suggestions not only to experiment considerations but also to the estimation of spatial resolution for a specific system.展开更多
This paper proposes a new method of aperture synthetizing in digital holography based on the principle of holography.In the new method aperture synthetizing is achieved by reconstructing each sub-hologram respectively...This paper proposes a new method of aperture synthetizing in digital holography based on the principle of holography.In the new method aperture synthetizing is achieved by reconstructing each sub-hologram respectively,firstly,moving each reconstructed wave field referred to the benchmark reconstructed wave field according to the relationship between spacial motion and frequency shift,and finally splicing them by using superposition. Two different recording ways,using plane wave to record and using spherical wave to record,are analyzed,and their moving formula is deduced,too.Simulation and experiment are done. The results show that in comparison with the traditional method of aperture synthetizing in digital holography,the new method can decrease calculation and save reconstructed time obviously which has better applicability.展开更多
3,4-Bis（4＇-aminofurazano-3＇）furoxan（DATF）, one of a new generation of high energy density materials, shows lots of interesting properties such as lower sensitivity, excellent thermal stability and superior deton...3,4-Bis（4＇-aminofurazano-3＇）furoxan（DATF）, one of a new generation of high energy density materials, shows lots of interesting properties such as lower sensitivity, excellent thermal stability and superior detonation perfor- mance in chemistry and physics. In this paper, on-line infrared（IR） spectroscopy was used to monitor the synthesis process of DATF. The concentration profiles and IR spectra of the components were determined by analyzing the IR data via principal component analysis（PCA）, evolving factor analysis（EFA） and multivariate curve resolution-alternating least squares（MCR-ALS）. The geometric configurations of reactant, intermediates and product were optimized with the density functional theory（DFT） at B3LYP/6-3 l＋G（d, p） level. Their vibrational frequencies and IR spectra were obtained on the basis of vibrational analysis. The result obtained by the chemometric resolution methods agreed well with that obtained by quantum chemical calculation method, which demonstrated the reliability of the proposed chemometric resolution methods. The unstable intermediate 3-amino-4-oxycyanofurazan（AOF） was confirmed via comparing the IR spectra resloved by chemometric resolution methods with those calculated by B3LYP/6-3 l＋G（d,p） and analyzed by MCR-ALS. Finally, the possible synthesis mechanism of DATF was deduced by analyzing the above IR spectra.展开更多
基金Supported by the Foundation of Double-Hundred Talents of China Academy of Engineering Physics (Grant No. 2004R0301)
文摘For a scintillating-fiber array fast-neutron radiography system,a point-spread-function computing model was introduced,and the simulation code was developed. The results of calculation show that fast-neutron radiographs vary with the size of fast neutron sources,the size of fiber cross-section and the imaging geometry. The results suggest that the following qualifications are helpful for a good point spread function: The cross-section of scintillating fibers not greater than 200 μm×200 μm,the size of neutron source as small as a few millimeters,the distance between the source and the scintillating fiber array greater than 1 m,and inspected samples placed as close as possible to the array. The results give suggestions not only to experiment considerations but also to the estimation of spatial resolution for a specific system.
基金Project supported by the National Natural Science Foundation of China (Grant Nos 60747001,60877070 and 60467003)
文摘This paper proposes a new method of aperture synthetizing in digital holography based on the principle of holography.In the new method aperture synthetizing is achieved by reconstructing each sub-hologram respectively,firstly,moving each reconstructed wave field referred to the benchmark reconstructed wave field according to the relationship between spacial motion and frequency shift,and finally splicing them by using superposition. Two different recording ways,using plane wave to record and using spherical wave to record,are analyzed,and their moving formula is deduced,too.Simulation and experiment are done. The results show that in comparison with the traditional method of aperture synthetizing in digital holography,the new method can decrease calculation and save reconstructed time obviously which has better applicability.
基金Supported by the National Natural Science Foundation of China（No.21175106） and the Specialized Research Fund for the Doctoral Program of Higher Education, China（No.20126101110019）.
文摘3,4-Bis（4＇-aminofurazano-3＇）furoxan（DATF）, one of a new generation of high energy density materials, shows lots of interesting properties such as lower sensitivity, excellent thermal stability and superior detonation perfor- mance in chemistry and physics. In this paper, on-line infrared（IR） spectroscopy was used to monitor the synthesis process of DATF. The concentration profiles and IR spectra of the components were determined by analyzing the IR data via principal component analysis（PCA）, evolving factor analysis（EFA） and multivariate curve resolution-alternating least squares（MCR-ALS）. The geometric configurations of reactant, intermediates and product were optimized with the density functional theory（DFT） at B3LYP/6-3 l＋G（d, p） level. Their vibrational frequencies and IR spectra were obtained on the basis of vibrational analysis. The result obtained by the chemometric resolution methods agreed well with that obtained by quantum chemical calculation method, which demonstrated the reliability of the proposed chemometric resolution methods. The unstable intermediate 3-amino-4-oxycyanofurazan（AOF） was confirmed via comparing the IR spectra resloved by chemometric resolution methods with those calculated by B3LYP/6-3 l＋G（d,p） and analyzed by MCR-ALS. Finally, the possible synthesis mechanism of DATF was deduced by analyzing the above IR spectra.
