A new fully automatic ^40Ar/^39Ar laboratory with a Thermo Scientific ARGUS VI mass spectrometer has been established in China University of Geosciences （Wuhan）. We designed and developed a mini efficient preparatio...A new fully automatic ^40Ar/^39Ar laboratory with a Thermo Scientific ARGUS VI mass spectrometer has been established in China University of Geosciences （Wuhan）. We designed and developed a mini efficient preparation system （80 mL）, a CO2 laser for heating samples, a crusher for extracting fluid inclusions within K-poor minerals and an air reservoir （31 L） and pipette （0.1 mL） system. The ARGUS VI mass spectrometer is operated by the Qtegra Noble Gas software, which can control the peripheral accessories, such as pneumatic valves, CO2 laser and crusher through a PeriCon （peripheral controller）. The experimental procedures of atmospheric argon ana- lyses, ^40Ar/^39Ar dating by laser stepwise heating and by progressive crushing in vacuo, can be fully automatically performed. The weighted mean of atmospheric ^40Ar/^36Ar ratios is 302.22＋0.03 （1σ, MSWD=0.74, n=200）, indicating that air reservoir and pipette system and the whole instrument sys- tem are very stable. This laboratory is a successful pioneer example in China to establish a new no- ble gas laboratory with self-made peripheral accessories expect for the mass spectrometer.展开更多
Laser rock spallation is a rock removal process that utilizes laser induced thermal stress to fracture and cause a break through the rock by creating small fragments before melting of the rock. In this paper we invest...Laser rock spallation is a rock removal process that utilizes laser induced thermal stress to fracture and cause a break through the rock by creating small fragments before melting of the rock. In this paper we investigated the effects of CO2 laser irradiation on limestone of Iran Sarvak formation. Since the limestone included heavy and light oil, we studied the amount of laser beam absorption by this oils for determining thermal fractured during the laser drilling laboratory process. In order to characterize this limestone spectrophotometry (from UV to NIR), scanning electron microscopy (SEM) have been used.展开更多
基金financially supported by the National Natural Science Foundation of China (Nos. 41503053, 41630315, 41688103, and 91128203)
文摘A new fully automatic ^40Ar/^39Ar laboratory with a Thermo Scientific ARGUS VI mass spectrometer has been established in China University of Geosciences （Wuhan）. We designed and developed a mini efficient preparation system （80 mL）, a CO2 laser for heating samples, a crusher for extracting fluid inclusions within K-poor minerals and an air reservoir （31 L） and pipette （0.1 mL） system. The ARGUS VI mass spectrometer is operated by the Qtegra Noble Gas software, which can control the peripheral accessories, such as pneumatic valves, CO2 laser and crusher through a PeriCon （peripheral controller）. The experimental procedures of atmospheric argon ana- lyses, ^40Ar/^39Ar dating by laser stepwise heating and by progressive crushing in vacuo, can be fully automatically performed. The weighted mean of atmospheric ^40Ar/^36Ar ratios is 302.22＋0.03 （1σ, MSWD=0.74, n=200）, indicating that air reservoir and pipette system and the whole instrument sys- tem are very stable. This laboratory is a successful pioneer example in China to establish a new no- ble gas laboratory with self-made peripheral accessories expect for the mass spectrometer.
文摘Laser rock spallation is a rock removal process that utilizes laser induced thermal stress to fracture and cause a break through the rock by creating small fragments before melting of the rock. In this paper we investigated the effects of CO2 laser irradiation on limestone of Iran Sarvak formation. Since the limestone included heavy and light oil, we studied the amount of laser beam absorption by this oils for determining thermal fractured during the laser drilling laboratory process. In order to characterize this limestone spectrophotometry (from UV to NIR), scanning electron microscopy (SEM) have been used.
