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锍镍试金-等离子体质谱法测定地球化学勘探样品中的铂族元素和金Ⅱ.分析流程空白的降低 被引量:52
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作者 吕彩芬 何红蓼 +3 位作者 周肇茹 支辛辛 李冰 张勤 《岩矿测试》 CAS CSCD 北大核心 2002年第1期7-11,共5页
对锍镍试金富集 -等离子体质谱法测定贵金属流程中的试剂空白进行了检查 ,并对空白主要来源 -捕集剂镍的各种纯化方法作了对比 ,提出了回收试金流程中溶扣后滤液中的镍循环使用。在有效降低空白的基础上 ,满足了化探样品所要求的 0 .0xn... 对锍镍试金富集 -等离子体质谱法测定贵金属流程中的试剂空白进行了检查 ,并对空白主要来源 -捕集剂镍的各种纯化方法作了对比 ,提出了回收试金流程中溶扣后滤液中的镍循环使用。在有效降低空白的基础上 ,满足了化探样品所要求的 0 .0xng/g级检出限 ,对超痕量贵金属标样分析结果与标准值符合。 展开更多
关键词 空白 试剂提纯 铂族元素 锍镍试金 等离子体质谱法 地球化学勘探
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板料成形过程中合理毛坯形状的确定 被引量:21
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作者 罗亚军 张永清 +1 位作者 何丹农 王静怡 《塑性工程学报》 EI CAS CSCD 2001年第3期63-66,共4页
为了提高产品质量和降低生产成本 ,需要合理确定成形件的毛坯形状。在介绍目前几种确定合理毛坯形状方法的基础上 ,提出用形状误差来优化由几何映射法获得的初始毛坯 ,进而确定合理的毛坯形状。以方盒件为例进行了数值模拟和物理模拟 ,... 为了提高产品质量和降低生产成本 ,需要合理确定成形件的毛坯形状。在介绍目前几种确定合理毛坯形状方法的基础上 ,提出用形状误差来优化由几何映射法获得的初始毛坯 ,进而确定合理的毛坯形状。以方盒件为例进行了数值模拟和物理模拟 ,结果表明 ,该方法确定的毛坯成形时避免了成形缺陷 ,而且修边余量小 ,既提高了质量又降低了成本 。 展开更多
关键词 板料成形 毛坯 几何映射法 形状误差 产品质量 滑移线法
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Prospects for Variable Gauge Rolling:Technology,Theory and Application 被引量:26
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作者 LIU Xiang-hua 《Journal of Iron and Steel Research International》 SCIE EI CAS CSCD 2011年第1期1-7,共7页
Variable gauge rolling (VGR) is a new technology to produce flat products with different thicknesses (FDT), which could be used to replace conventional fiat products in order to save metals and reduce structure ma... Variable gauge rolling (VGR) is a new technology to produce flat products with different thicknesses (FDT), which could be used to replace conventional fiat products in order to save metals and reduce structure mass. The method of VGR was introduced for investigating new problems in rolling theory of VGR, and the new formulas for calculating parameters of VGR were proposed. Besides, some results of numerical simulation by finite elemen~ method were described. As an example, the products applications of FDT in bridge construction, ship building and auto manufacturing were presented. Finally, the prospects for VGR and FDT were discussed. 展开更多
关键词 variable gauge rolling longitudinal profile plate tailor rolled blank
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分析化学中检出限问题探讨 被引量:26
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作者 徐金龙 刘中勇 +1 位作者 华斌 史亚晓 《检验检疫学刊》 2012年第6期74-76,共3页
检出限是分析测试的重要指标,检出限通常分为仪器检出限、方法检出限、样品检出限。当以检出限做为分析方法、分析仪器的比较标准时,应正确理解的相关问题和使用注意事项。本文将从检出限的分类、检出限概念及影响因素阐述检出限的重要性。
关键词 检出限 空白 测定下限
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End-Permian catastrophic event of marine acidification by hydrated sulfuric acid:Mineralogical evidence from Meishan Section of South China 被引量:22
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作者 LIANG HandongKey Laboratory of Coal Resources, China University of Mining and Technology, Beijing 100083, China (e-mail: hdl6688@sina.com) 《Chinese Science Bulletin》 SCIE EI CAS 2002年第16期1393-1397,共5页
The event Permian-Triassic boundary (EPTB) is well marked by the famous 'white clay' of bed 25 in Mei-shan Section located in Changxing county, Zhejiang province of China. In this note, the white clay as well ... The event Permian-Triassic boundary (EPTB) is well marked by the famous 'white clay' of bed 25 in Mei-shan Section located in Changxing county, Zhejiang province of China. In this note, the white clay as well as its overlying and underlying sequences is investigated particularly for mineralogical records. The investigation yields three findings that contribute to better understanding the scenario of the EPTB mass extinction. (i) A red goethite-rich microlayer (0.3 mm) is first recognized to be horizontally widespread on the base of the white clay in the section. The microlayer should be considered as a macro geochemical indicator naturally tracing a catastrophic initiation at the EPTB. (ii) An interruption of marine carbonate deposition is discovered due to blank of carbonate minerals in the white clay. The discovery provides significant evidence of a marine acidification event that would occur in the paleo-ocean with marine acidity estimated at pH【4.0 at least and be triggered by the ultimate 展开更多
关键词 mass extinction MARINE ACIDIFICATION hydrated sulfuric acid MEISHAN Section GOETHITE carbonate blank catastrophic event.
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谈氨氮测定时应注意的几点问题 被引量:22
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作者 王朝明 《长春大学学报》 2007年第2期97-99,共3页
纳氏试剂比色法是测定水中氨氮的国家标准方法。标准方法对氨氮的介绍比较详细,测定步骤也较简单,但实际工作中,情况比较复杂,条件较苛刻,实验空白值难以达到要求(A≤0.030),很多具体的因素都影响该方法的灵敏度,也直接影响分析结果的... 纳氏试剂比色法是测定水中氨氮的国家标准方法。标准方法对氨氮的介绍比较详细,测定步骤也较简单,但实际工作中,情况比较复杂,条件较苛刻,实验空白值难以达到要求(A≤0.030),很多具体的因素都影响该方法的灵敏度,也直接影响分析结果的精密度和准确度。根据多年的实际工作经验,将氨氮测定过程中容易出现的问题及注意事项进行了总结。 展开更多
关键词 氨氮 空白 注意事项
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Technology and Experiments of 42CrMo Bearing Ring Forming Based on Casting Ring Blank 被引量:17
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作者 LI Yongtang JU Li +3 位作者 QI Huiping ZHANG Feng CHEN Guozhen WANG Mingli 《Chinese Journal of Mechanical Engineering》 SCIE EI CAS CSCD 2014年第2期418-427,共10页
Bearing ring is the crucial component of bearing. With regard to such problems as material waste, low efficiency and high energy consumption in current process of producing large bearing ring, a new process named "ca... Bearing ring is the crucial component of bearing. With regard to such problems as material waste, low efficiency and high energy consumption in current process of producing large bearing ring, a new process named "casting-rolling compound forming technology" is researched by taking the typical 42CrMo slew bearing as object. Through theoretical analysis, the design criteria of the main casting-rolling forming parameters are put forward at first. Then the constitutive relationship model of as-cast 42CrMo steel and its mathematical model of dynamic recrystallization are obtained according to the results of the hot compression experiment. By a coupled thermal-mechanical finite element model for radial-axial rolling of bearing ring, the fraction of dynamic recrystallization is calculated and recrystallized grains size are predicated. Meanwhile, the effects of the initial rolling temperature and feed rate of idle roll on material microstructure evolution are analyzed. Finally, the industrial rolling experiment is designed and performed, based on the simulation results. In addition, mechanical and metallographic tests are conducted on rolled bearing ring to get the mechanical parameters and metallographic structure. The experimental data and results show that the mechanical properties of bearing ring produced by casting-rolling compound forming technology are up to industrial standard, and a qualified bearing ring can be successfully formed by employing this new technology. Through the study, a process of forming large bearing ring directly by using casting ring blank is obtained, which could provide an effective theoretical guidance for manufacturing large ring parts. It also has an edge in saving material, lowering energy and improving efficiency. 展开更多
关键词 bearing ring 42CrMo casting ring blank casting-rolling compound forming microstructure evolution
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FAST ACCURATE PREDICTION OF BLANK SHAPE IN SHEET METAL FORMING 被引量:14
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作者 LiuYuqi LiZhigang YahYakun 《Acta Mechanica Solida Sinica》 SCIE EI 2004年第1期58-64,共7页
By using the Finite Element Inverse Approach based on the Hill quadratic anisotrop-ically yield criterion and the quadrilateral element, a fast analyzing software-FASTAMP for the sheet metal forming is developed. The ... By using the Finite Element Inverse Approach based on the Hill quadratic anisotrop-ically yield criterion and the quadrilateral element, a fast analyzing software-FASTAMP for the sheet metal forming is developed. The blank shapes of three typical stampings are simulated and compared with numerical results given by the AUTOFORM software and experimental results, respectively. The comparison shows that the FASTAMP can predict blank shape and strain distribution of the stamping more precisely and quickly than those given by the traditional methods and the AUTOFORM. 展开更多
关键词 sheet metal forming Finite Element Inverse Approach blank shape FASTAMP software
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静压作用下重组木坯料形成的力学机理和试验验证 被引量:10
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作者 马岩 金维洙 +2 位作者 孟庆军 李松龄 关小平 《林业科学》 CAS CSCD 北大核心 1996年第2期171-174,共4页
在横观各向同性假设条件下.借用弹性力学的半无限平面体边界上受力作用和圆柱体均布载荷作用的结论,导出静压作用下重组木坯料形成的受力关系式,并用试验验证了这些结论。应用这些理论,可以精确计算重组本木束形成达到临界状态时的... 在横观各向同性假设条件下.借用弹性力学的半无限平面体边界上受力作用和圆柱体均布载荷作用的结论,导出静压作用下重组木坯料形成的受力关系式,并用试验验证了这些结论。应用这些理论,可以精确计算重组本木束形成达到临界状态时的最大应力,并可建立其强度准则。结论还可以用于重组木坯料加工设备的参数确定和丰富木材学的基础理论。 展开更多
关键词 重组木 坯料 木材学
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语言表达的缺位与补位——从“长期以来”与“一直以来”的竞争、互补与融合说起 被引量:13
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作者 周静 杨海明 《语言文字应用》 CSSCI 北大核心 2007年第1期78-85,共8页
汉语“X以来”框架中事件序列表达是有缺位的,事件序列的概约化表达长期缺位,一直用时间序列的概约化表达“长期以来”替代事件序列的概约化表达。“一直以来”是拷贝时间序列概约化表达的结果,是对事件序列缺位的一种补位。补位可以通... 汉语“X以来”框架中事件序列表达是有缺位的,事件序列的概约化表达长期缺位,一直用时间序列的概约化表达“长期以来”替代事件序列的概约化表达。“一直以来”是拷贝时间序列概约化表达的结果,是对事件序列缺位的一种补位。补位可以通过拷贝已有表达形式产生;新形式产生后必然与旧形式进行竞争。 展开更多
关键词 缺位 补位 长期 一直 竞争 融合
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基于有限元逆向法和正向法的板料成形过程中合理毛坯形状的确定 被引量:12
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作者 苗量 陈文琳 李桂兰 《锻压技术》 CAS CSCD 北大核心 2006年第2期15-18,共4页
合理的毛坯形状可以提高板料成形质量,降低成本。有限元逆向法确定简单形状零件的毛坯具有很高的可靠性,但不适合于单独用来确定带有拉深筋及切边余量大的覆盖件拉深成形板料毛坯。本文采用有限元逆向法和正向法结合的方法,确定覆盖件... 合理的毛坯形状可以提高板料成形质量,降低成本。有限元逆向法确定简单形状零件的毛坯具有很高的可靠性,但不适合于单独用来确定带有拉深筋及切边余量大的覆盖件拉深成形板料毛坯。本文采用有限元逆向法和正向法结合的方法,确定覆盖件零件的成形毛坯,并用物理实验验证了其合理性。 展开更多
关键词 毛坯 有限元逆向法 数值模拟 板料成形
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Study on Nonuniform Deformation of Tailor Rolled Blank During Uniaxial Tension 被引量:14
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作者 Hua-Wei Zhang Xiang-Hua Liu +2 位作者 Li-Zhong Liu Ping Hu Jia-Lu Wu 《Acta Metallurgica Sinica(English Letters)》 SCIE EI CAS CSCD 2015年第9期1198-1204,共7页
The deformation characteristics of tailor rolled blank (TRB) in the course of uniaxial tension were studied by means of analysis, test and simulation. The mechanical analytical model of TRB during uniaxial tension w... The deformation characteristics of tailor rolled blank (TRB) in the course of uniaxial tension were studied by means of analysis, test and simulation. The mechanical analytical model of TRB during uniaxial tension was set up, and the deformation formulae for the thinner side and for the thicker side were derived to quantify the deformation of TRB. On this basis, uniaxial tension tests on TRB and ordinary blanks (the thinner side and the thicker side of TRB) were conducted. Lagrange polynomial interpolation method was adopted to construct the stress-strain fields of unannealed and annealed TRBs for solving TRB material parameters, and then, uniaxial tension simulation on TRB was completed. Deformations and properties of unannealed TRB were compared with those of annealed TRB, and the thinner side and the thicker side were also compared. Finally, the research results were explained by metallurgical structure. The results show that nonuniform deformation happens in TRB during uniaxial tension, and the necking occurs on the thinner side. The agreement of analysis, test and simulation confirms the correctness of the analytical model and the deformation formulae. The findings of this paper can lay the foundation for the future study on TRB stamping formability and provide a way for TRB modeling. 展开更多
关键词 Tailor rolled blank (TRB) Nonuniform deformation Uniaxial tension ANNEALING Metallographical
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Design of Pinion Machine Tool-settings for Spiral Bevel Gears by Controlling Contact Path and Transmission Errors 被引量:12
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作者 曹雪梅 方宗德 +1 位作者 许浩 苏进展 《Chinese Journal of Aeronautics》 SCIE EI CAS CSCD 2008年第2期179-186,共8页
This paper proposes a new approach to design pinion machine tool-settings for spiral bevel gears by controlling contact path and transmission errors. It is based on the satisfaction of contact condition of three given... This paper proposes a new approach to design pinion machine tool-settings for spiral bevel gears by controlling contact path and transmission errors. It is based on the satisfaction of contact condition of three given control points on the tooth surface. The three meshing points are controlled to be on a predesigned straight contact path that meets the pre-designed parabolic function of transmission errors. Designed separately, the magnitude of transmission errors and the orientation of the contact path are subjected to precise control. In addition, in order to meet the manufacturing requirements, we suggest to modify the values of blank offset, one of the pinion machine tool-settings, and redesign pinion ma- chine tool-settings to ensure that the magnitude and the geometry of transmission errors should not be influenced apart from minor effects on the predesigned straight contact path. The proposed approach together with its ideas has been proven by a numerical example and the manufacturing practice of a pair of spiral bevel gears. 展开更多
关键词 spiral bevel gear contact path transmission error blank offset tooth contact analysis
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Fluid Flow and Solidification Simulation in Beam Blank Continuous Casting Process With 3D Coupled Model 被引量:14
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作者 YANG Jian-wei DU Yan-ping +1 位作者 SHI Rong CUI Xiao-chao 《Journal of Iron and Steel Research International》 SCIE EI CAS CSCD 2006年第4期17-21,共5页
Based on turbulent theory, a 3D coupled model of fluid flow and solidification was built using finite difference method and used to study the influence of superheating degree and casting speed on fluid flow and solidi... Based on turbulent theory, a 3D coupled model of fluid flow and solidification was built using finite difference method and used to study the influence of superheating degree and casting speed on fluid flow and solidification, analyze the interaction between shell and molten steel, and compare the temperature distribution under different technological conditions. The results indicate that high superheating degree can lengthen the liquid-core depth and make the crack and breakout possible, so suitable superheating should be controlled within 35℃ according to the simulation results. Casting speed which is one of the most important technological parameters of improving production rate, should be controlled between 0. 85 m/min and 1.05 m/min and the caster has great potential in the improvement of blank quality. 展开更多
关键词 beam blank continuous casting flow field temperature distribution coupled model SOLIDIFICATION
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均布载荷辗压重组木坯料的强度准则建立初探 被引量:8
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作者 马岩 金维洙 +2 位作者 蔡立新 张宁 耿绍辉 《东北林业大学学报》 CAS CSCD 北大核心 1993年第6期56-60,共5页
采用横观各向同性假设,对均布载荷辗压方式下,重组木网状坯料的形成静力学强度准则进行了初步探讨。重组木的坯料要求将间伐材等沿径向与切向压溃,而纵向纤维不断。因此,必须准确地确定加压数值。本文以复合材料力学建立判据,其分析结... 采用横观各向同性假设,对均布载荷辗压方式下,重组木网状坯料的形成静力学强度准则进行了初步探讨。重组木的坯料要求将间伐材等沿径向与切向压溃,而纵向纤维不断。因此,必须准确地确定加压数值。本文以复合材料力学建立判据,其分析结果将高于传统木材力学的分析方法。 展开更多
关键词 重组木 均布载荷 强度 坯料
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当代汉语新兴词族的形成机制与衍生动因——基于“X女郎”词族的个案分析 被引量:11
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作者 彭晓 杨文全 《语言文字应用》 CSSCI 北大核心 2009年第3期98-104,共7页
本文以当代汉语词库中的一组新兴词族"X女郎"为考察对象,探讨了它们的形成机制与语用动因。就其形成机制而言,"X女郎"首先模拟了原型词"邦女郎"的语义、语用关联框架,伴随着"X"的泛化与"... 本文以当代汉语词库中的一组新兴词族"X女郎"为考察对象,探讨了它们的形成机制与语用动因。就其形成机制而言,"X女郎"首先模拟了原型词"邦女郎"的语义、语用关联框架,伴随着"X"的泛化与"女郎"一词的去范畴化,在汉语中拷贝生成出一个"X女郎";随后,"X女郎"凝固为一个能产的词语模。而它的衍生动因则涉及语言内部与语用两方面因素。 展开更多
关键词 上位词 下位词 缺位 补位 去范畴化 词语模
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Recent Development on Theory and Application of Variable Gauge Rolling, a Review 被引量:12
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作者 Xianghua Liu Qilin Zhao Lizhong Liu 《Acta Metallurgica Sinica(English Letters)》 SCIE EI CAS CSCD 2014年第3期483-493,共11页
Variable gauge rolling (VGR) is a new technology for producing the materials which have the advantage of lightweight due to optimized thickness according to load distribution. The new progresses in the theoretical r... Variable gauge rolling (VGR) is a new technology for producing the materials which have the advantage of lightweight due to optimized thickness according to load distribution. The new progresses in the theoretical research and application of VGR are reviewed in this paper. Two basic equations, VGR-f and VGR-s, were deduced. The former is a new differential equation of force equilibrium, and the latter is a new form of formula for the law of mass conservation. Both of them provide a new base for the development of VGR analysis. As the examples of VGR's application, tailor rolled blank (TRB) and longitudinal profile (LP) plate are introduced. Now TRBs are only produced in Germany and China, and have been used in the automotive manufacturing to play an important role in lightweight design. LP plates have been used in shipbuilding and bridge construction, and promised a bright prospect in reducing construction weight. In addition, new technologies and applications of VGR emerge constantly. Tailor welded strips and tailor rolled strips with variable thickness across the width can be used for progressive die and roll forming. The 3D profiled blank can be obtained by two-step rolling process. Tailor tubes witli the variable wail thickness are an efficient way to reduce the weight. The blank with tailored thickness and mechanical property is also under development. Above products based on the tailored ideas provide a new materials-warehouse for the designers to select so as to meet the needs of weight reducing and material saving. 展开更多
关键词 Variable gauge rolling Tailor rolled blank Longitudinal profile plate Material saving Weight reducing
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平面设计中的空白意蕴 被引量:12
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作者 岳继平 《艺术与设计(理论版)》 2007年第1X期27-29,共3页
平面设计中的空白作为一种空符号,在设计中有着重要的作用,在标识设计中它作为“阴”的一面直接影响着标志含义的表达,而在招贴设计中,余白的运用可以使画面充满透气感,让整体构图充满活力,在包装设计中,大量余白的运用是产品高档次的... 平面设计中的空白作为一种空符号,在设计中有着重要的作用,在标识设计中它作为“阴”的一面直接影响着标志含义的表达,而在招贴设计中,余白的运用可以使画面充满透气感,让整体构图充满活力,在包装设计中,大量余白的运用是产品高档次的象征。 展开更多
关键词 余白 标志 招贴
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关于硝酸银滴定法测定氯离子方法的改进 被引量:12
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作者 康少芝 《吉林水利》 2010年第10期8-9,17,共3页
水中的氯离子对我们的生产、生活有很大的影响,其检测分析方法很多。在选用硝酸银滴定法时,针对国家标准方法在实际检测工作中的运用进行了改进。并根据多年积累的实际工作经验,提出了自己的见解,对基层实验室氯离子的检测分析有一定的... 水中的氯离子对我们的生产、生活有很大的影响,其检测分析方法很多。在选用硝酸银滴定法时,针对国家标准方法在实际检测工作中的运用进行了改进。并根据多年积累的实际工作经验,提出了自己的见解,对基层实验室氯离子的检测分析有一定的借鉴意义。 展开更多
关键词 硝酸银滴定法 氯离子 空白 测定
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Forming defects in aluminum alloy hot stamping of side-door impact beam 被引量:12
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作者 周靖 王宝雨 +2 位作者 林建国 傅垒 马闻宇 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2014年第11期3611-3620,共10页
The forming defects, including thinning, rupture, wrinkling and springback, usually arising in producing a side-door impact beam, were investigated by trial and numerical simulation. A temperature-related constitutive... The forming defects, including thinning, rupture, wrinkling and springback, usually arising in producing a side-door impact beam, were investigated by trial and numerical simulation. A temperature-related constitutive model specific to the temperature range from 350 °C to 500 °C was established and used for the numerical simulation. The trial and numerical simulation were conducted to clarify the quantitative characteristics of forming defects and to analyze the effects of process parameters on the forming defects. Results show that the rupture situation is ameliorated and the springback is eliminated in the aluminum alloy hot stamping. The wrinkling severity decreases with increasing blank holder force (BHF), but the BHF greater than 15 kN causes the rupture at the deepest drawing position of workpiece. The forming defects are avoided with lubricant in the feasible ranges of process parameters: the BHF of 3 to 5 kN and the stamping speed of 50 to 200 mm/s. 展开更多
关键词 aluminum alloy hot stamping forming defects numerical simulation blank holder force
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