The ceramic composites of sodium bismuth titanate with reduce graphene oxide NBT/rGO of different compositions were fabricated by solid state sintering method and characterized. In this work, the graphene oxide (GO) a...The ceramic composites of sodium bismuth titanate with reduce graphene oxide NBT/rGO of different compositions were fabricated by solid state sintering method and characterized. In this work, the graphene oxide (GO) and reduce graphene oxide (rGO) was successfully synthesized by Hummer’s modified method which is confirmed by FTIR and XRD results. The reduce graphene oxide used as 2D filler in piezoelectric creamic material. The crystalline structure of NBT/rGO composite was confirmed by X-ray diffraction with rhombohedral symmetry. The dispersion of rGO in the ceramic can be detect by the optical microcopy images. The electrical conductivity of sodium bismuth titanate shows increase at higher values of frequency and conductivity nanocomposites of different wt% were start decreases up to certain value of frequency. The broadening of peaks in frequency explicit plots of electrical conductivity with the help of LCR Meter (Impedance Capacitance and Resistance). The crystalline size of reduced graphene oxide and NBT is calculated by Scherrer’s formula of XRD peaks.展开更多
A higher value of the dielectric constant of h-BN makes it quite favourable material in energy storing device. The variation in dielectric constant was observed as a function of thickness. In this research work multil...A higher value of the dielectric constant of h-BN makes it quite favourable material in energy storing device. The variation in dielectric constant was observed as a function of thickness. In this research work multilayers of Hexagonal Boron Nitride (h-BN) was fabricated by using the Chemical exfoliation method. Two solvents Dimethylformamide (DMF) and Isopropyl Alcohol (IPA) were used for the exfoliation of h-BN. Successful sonication of hexagonal boron nitride led to the formation of Boron Nitride nanosheets (BNNs). The stable dispersibility of h-BN in Dimethylformamide and Isopropyl Alcohol was confirmed by UV Visible Spectroscopy, X-ray diffraction (XRD) and Scanning electron microscopy (SEM) confirm the mono crystallite structure (002) and nanoflakes like morphology of h-BN respectively. This appropriate strategy offered a feasible route to produce multilayer of hexagonal boron nitride. After the successful fabrication of h-BN multilayers its dielectric properties were calculated by using LCR meter. Profilometer revealed the variation in thickness and value of Dielectric constant was calculated by using its formula.展开更多
文摘The ceramic composites of sodium bismuth titanate with reduce graphene oxide NBT/rGO of different compositions were fabricated by solid state sintering method and characterized. In this work, the graphene oxide (GO) and reduce graphene oxide (rGO) was successfully synthesized by Hummer’s modified method which is confirmed by FTIR and XRD results. The reduce graphene oxide used as 2D filler in piezoelectric creamic material. The crystalline structure of NBT/rGO composite was confirmed by X-ray diffraction with rhombohedral symmetry. The dispersion of rGO in the ceramic can be detect by the optical microcopy images. The electrical conductivity of sodium bismuth titanate shows increase at higher values of frequency and conductivity nanocomposites of different wt% were start decreases up to certain value of frequency. The broadening of peaks in frequency explicit plots of electrical conductivity with the help of LCR Meter (Impedance Capacitance and Resistance). The crystalline size of reduced graphene oxide and NBT is calculated by Scherrer’s formula of XRD peaks.
文摘A higher value of the dielectric constant of h-BN makes it quite favourable material in energy storing device. The variation in dielectric constant was observed as a function of thickness. In this research work multilayers of Hexagonal Boron Nitride (h-BN) was fabricated by using the Chemical exfoliation method. Two solvents Dimethylformamide (DMF) and Isopropyl Alcohol (IPA) were used for the exfoliation of h-BN. Successful sonication of hexagonal boron nitride led to the formation of Boron Nitride nanosheets (BNNs). The stable dispersibility of h-BN in Dimethylformamide and Isopropyl Alcohol was confirmed by UV Visible Spectroscopy, X-ray diffraction (XRD) and Scanning electron microscopy (SEM) confirm the mono crystallite structure (002) and nanoflakes like morphology of h-BN respectively. This appropriate strategy offered a feasible route to produce multilayer of hexagonal boron nitride. After the successful fabrication of h-BN multilayers its dielectric properties were calculated by using LCR meter. Profilometer revealed the variation in thickness and value of Dielectric constant was calculated by using its formula.
