The TiO 2 powder was prepared by a stearic acid gel method. XRD characterization indicated that the crystal form was anatase. The grain size, given out by Sherrer formula, is 19 nm. With polystyrene dissolved in tolue...The TiO 2 powder was prepared by a stearic acid gel method. XRD characterization indicated that the crystal form was anatase. The grain size, given out by Sherrer formula, is 19 nm. With polystyrene dissolved in toluene as binder, TiO 2 adhered to the glassfibre substrate. By this method, the powder was immobilized and the crystal form, grain size and photocatalysis activities were well maintained. Photocatalysis degradation properties were investigated by putting the TiO 2 immobilization film in the methyl orange aqueous system. The results indicated that the differences of degradation rate between the TiO 2 immobilization film and powder were not obvious, which made waste water treatment using photocatalysis degradation technique possible in the practical application. [WT5HZ]展开更多
A convenient and economic method for preparing highly ordered MCM 41 was studied in an open vessel by using waterglass as the silicon source. XRD, nitrogen adsorption and TEM show that the product has a highly ordered...A convenient and economic method for preparing highly ordered MCM 41 was studied in an open vessel by using waterglass as the silicon source. XRD, nitrogen adsorption and TEM show that the product has a highly ordered structure and the hexagonal arrangements of uniformly size pores distribution.展开更多
文摘The TiO 2 powder was prepared by a stearic acid gel method. XRD characterization indicated that the crystal form was anatase. The grain size, given out by Sherrer formula, is 19 nm. With polystyrene dissolved in toluene as binder, TiO 2 adhered to the glassfibre substrate. By this method, the powder was immobilized and the crystal form, grain size and photocatalysis activities were well maintained. Photocatalysis degradation properties were investigated by putting the TiO 2 immobilization film in the methyl orange aqueous system. The results indicated that the differences of degradation rate between the TiO 2 immobilization film and powder were not obvious, which made waste water treatment using photocatalysis degradation technique possible in the practical application. [WT5HZ]
文摘A convenient and economic method for preparing highly ordered MCM 41 was studied in an open vessel by using waterglass as the silicon source. XRD, nitrogen adsorption and TEM show that the product has a highly ordered structure and the hexagonal arrangements of uniformly size pores distribution.