Reduction of halogenated dinitro-triphenyl ethers over Fe-HCl gave halogenated diamino-triphenyl ethers in 77.0-94.0%.The reaction were fast and easy to operate while water was used as a proton-donator and ethanol was...Reduction of halogenated dinitro-triphenyl ethers over Fe-HCl gave halogenated diamino-triphenyl ethers in 77.0-94.0%.The reaction were fast and easy to operate while water was used as a proton-donator and ethanol was used as a solvent.展开更多
Halobenzene substituted by strong withdrawing-electron group was condensed with dihydroxy-benzene in non-protonic polar solvent and in the present of alkali metal carbonate,six bis(nitrophenoxy)-Benzene were synthesiz...Halobenzene substituted by strong withdrawing-electron group was condensed with dihydroxy-benzene in non-protonic polar solvent and in the present of alkali metal carbonate,six bis(nitrophenoxy)-Benzene were synthesized in good yields and good qualities by series of conditional tests.展开更多
文摘Reduction of halogenated dinitro-triphenyl ethers over Fe-HCl gave halogenated diamino-triphenyl ethers in 77.0-94.0%.The reaction were fast and easy to operate while water was used as a proton-donator and ethanol was used as a solvent.
文摘Halobenzene substituted by strong withdrawing-electron group was condensed with dihydroxy-benzene in non-protonic polar solvent and in the present of alkali metal carbonate,six bis(nitrophenoxy)-Benzene were synthesized in good yields and good qualities by series of conditional tests.
