Thermal decomposition reaction mechanism of the precursor gel made by sol gel process for nano crystalline BaTiO3 was studied by TG DTG and FTIR techniques.The reaction proceeded in three stages:solvents removing,orga...Thermal decomposition reaction mechanism of the precursor gel made by sol gel process for nano crystalline BaTiO3 was studied by TG DTG and FTIR techniques.The reaction proceeded in three stages:solvents removing,organic ligands decomposing,and amorphous solid BaTiO3 forming.The differential and intergral mechanism functions and activation energy for the third stage were obtained by calculation and comparson.展开更多
文摘换能元作为微机电系统(Micro Electro-Mechanical Systems,MEMS)火工品的核心部件,是MEMS火工品安全性和可靠性的重要影响因素,对整个武器系统的影响也是不可忽视的。文中从换能元的基底和电阻材料研究、结构设计等角度,综述了近年来MEMS火工品换能元的最新发展研究。介绍了MEMS火工品换能元的两大关键技术:MEMS火工品换能元的设计制备方法以及换能元性能参数的测试表征。指出:具有微型化、集成化、多功能化和高可靠性的MEMS火工品换能元是未来研究的热点。为M EM S火工品换能元的设计研究提供理论支撑,应加强微尺度下的热散失特性以及桥区电阻特性研究。认为复合含能薄膜桥换能元是MEMS火工品换能元的一个重要发展方向。
文摘Thermal decomposition reaction mechanism of the precursor gel made by sol gel process for nano crystalline BaTiO3 was studied by TG DTG and FTIR techniques.The reaction proceeded in three stages:solvents removing,organic ligands decomposing,and amorphous solid BaTiO3 forming.The differential and intergral mechanism functions and activation energy for the third stage were obtained by calculation and comparson.
