摘要
在微波辐射下,选用结晶三氯化铁为催化剂,用微型实验法,成功快速地合成了β-萘甲醚,得出了最佳合成条件,获得了较好的收率.此法操作简单,热能利用率高,无污染等优点,是有机合成的一个新途径.并用测熔点和红外光谱对产品质量进行了鉴定.
Crystal irontrichloride was chosen as katalyst at microave irradiation. β-methoxynaphthalene was synthesized successfully at very rapid speed by subminiature experiment method, which optimal synthetical conditions and better yield were gained from. This method is easy for operation without pollution and heat is used in efficiency by the method. So this method is a new approach for organic synthesis. IR spectra and melting point were also used to identify the product.
出处
《西华师范大学学报（自然科学版）》
2005年第3期302-304,共3页
Journal of China West Normal University(Natural Sciences)
关键词
β-萘甲醚
微波辐射
微型
合成
β-methoxynaphthalene
microwave irradiation
minitype
synthesis
